Organic Structure Determination

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Organic Structure Determination Using 2-D NMR Spectroscopy

Jeffrey H. Simpson
Organic Structure Determination Using 2 D NMR Spectroscopy Book PDF

Author : Jeffrey H. Simpson
Publisher : Academic Press
Page : 591 pages
File Size : 48,5 Mb
Release : 2011-12-30
Category : Science
ISBN : 9780123849700

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Organic Structure Determination Using 2-D NMR Spectroscopy by Jeffrey H. Simpson Pdf

"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--

Tables of Spectral Data for Structure Determination of Organic Compounds

Ernö Pretsch,T. Clerc,J. Seibl,W. Simon
Tables of Spectral Data for Structure Determination of Organic Compounds Book PDF

Author : Ernö Pretsch,T. Clerc,J. Seibl,W. Simon
Publisher : Springer Science & Business Media
Page : 325 pages
File Size : 43,6 Mb
Release : 2013-06-29
Category : Science
ISBN : 9783662224557

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Tables of Spectral Data for Structure Determination of Organic Compounds by Ernö Pretsch,T. Clerc,J. Seibl,W. Simon Pdf

Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.

Structure Determination of Organic Compounds

Ernö Pretsch,Philippe Bühlmann,Christian Affolter
Structure Determination of Organic Compounds Book PDF

Author : Ernö Pretsch,Philippe Bühlmann,Christian Affolter
Publisher : Springer Science & Business Media
Page : 444 pages
File Size : 53,6 Mb
Release : 2000
Category : Science
ISBN : 3540678158

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Structure Determination of Organic Compounds by Ernö Pretsch,Philippe Bühlmann,Christian Affolter Pdf

Table -- Combination tables -- 13C NMR spectroscopy -- 1H NMR specroscopy -- IR spectroscopy -- Mass spectrometry -- UV/Vis spectroscopy.

Problems in Organic Structure Determination

Roger G. Linington,Philip G. Williams,John B. MacMillan
Problems in Organic Structure Determination Book PDF

Author : Roger G. Linington,Philip G. Williams,John B. MacMillan
Publisher : CRC Press
Page : 774 pages
File Size : 45,5 Mb
Release : 2015-10-14
Category : Science
ISBN : 9781498719636

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Problems in Organic Structure Determination by Roger G. Linington,Philip G. Williams,John B. MacMillan Pdf

With extensive detailed spectral data, it contains a variety of problems designed by renowned authors to develop proficiency in organic structure determination. It presents a concept-based learning platform, introducing key concepts sequentially and reinforcing them with problems that exemplify the complexities and underlying principles that govern each concept.

Determination of Organic Structures by Physical Methods

E. A. Braude,F. C. Nachod
Determination of Organic Structures by Physical Methods Book PDF

Author : E. A. Braude,F. C. Nachod
Publisher : Elsevier
Page : 825 pages
File Size : 45,5 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483275727

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Determination of Organic Structures by Physical Methods by E. A. Braude,F. C. Nachod Pdf

Determination of Organic Structures by Physical Methods, Volume 1 focuses on the processes, methodologies, principles, and approaches involved in the determination of organic structures by physical methods, including infrared light absorption, thermodynamic properties, Raman spectra, and kinetics. The selection first elaborates on the phase properties of small molecules, equilibrium and dynamic properties of large molecules, and optical rotation. Discussions focus on simple acyclic compounds, carbohydrates, steroids, diffusion, viscosity, osmotic pressure, sedimentation velocity, melting and boiling points, and molar volume. The book then examines ultraviolet and visible light absorption, infrared light absorption, Raman spectra, and the theory of magnetic susceptibility. Concerns cover applications to the study of organic compounds, applications to the determination of structure, determination of thermodynamic properties, and experimental methods and evaluation of data. The text ponders on wave-mechanical theory, reaction kinetics, and dissociation constants, including dissociation of molecular addition compounds, principles of reaction kinetics, and valence-bond treatment of aromatic systems. The selection is a valuable source of data for researchers interested in the determination of organic structures by physical methods.

Organic Spectroscopic Structure Determination

Douglass F. Taber
Organic Spectroscopic Structure Determination Book PDF

Author : Douglass F. Taber
Publisher : Oxford University Press, USA
Page : 276 pages
File Size : 51,6 Mb
Release : 2007
Category : Science
ISBN : STANFORD:36105123313830

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Organic Spectroscopic Structure Determination by Douglass F. Taber Pdf

Organic Spectroscopic Structure Determination is designed as a first introduction to the elucidation of molecular structures. It consists of four sections that engage the imagination of the student. Taber has arranged the material in such a way that the students can work the problems and learn the procedures on their own, minimizing the time taken in lecture. The first section includes three chapters of instruction on the methods of organic spectroscopy. The second consists of fifty problems with just data sets of spectroscopic data. The third includes fifty problems that show starting materials and reaction conditions, with spectroscopic data for the product. The final section features tables of spectroscopic data.

Challenges in Molecular Structure Determination

Manfred Reichenbächer,Jürgen Popp
Challenges in Molecular Structure Determination Book PDF

Author : Manfred Reichenbächer,Jürgen Popp
Publisher : Springer Science & Business Media
Page : 500 pages
File Size : 55,9 Mb
Release : 2012-03-23
Category : Science
ISBN : 9783642243899

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Challenges in Molecular Structure Determination by Manfred Reichenbächer,Jürgen Popp Pdf

Taking a problem-based approach, the authors provide a practice-oriented and systematic introduction to both organic and inorganic structure determination by spectroscopic methods. This includes mass spectrometry, vibrational spectroscopies, UV/VIS spectroscopy and NMR as well as applying combinations of these methods. The authors show how to elucidate chemical structures with a minimal number of spectroscopic techniques. Readers can train their skills by more than 400 problems with varying degree of sophistication. Interactive Powerpoint-Charts are available as Extra Materials to support self-study.

Determination of Organic Structures by Physical Methods V4

F.C. Nachod
Determination of Organic Structures by Physical Methods V4 Book PDF

Author : F.C. Nachod
Publisher : Elsevier
Page : 396 pages
File Size : 50,5 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780323152341

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Determination of Organic Structures by Physical Methods V4 by F.C. Nachod Pdf

Determination of Organic Structures by Physical Methods, Volume 4 is a seven-chapter text that discusses the refinements of some established physical methods for organic structure determination. Each chapter of this book examines specific physical method, including high-field and pulsed NMR, nuclear magnetic double resonance spectroscopy, and 15N, 13C, and 31P nuclear magnetic resonance. The historical developments, principles, instrumentation, and applications to organic chemistry of these methods are discussed. This work will be of value to organic and analytical chemists and researchers.

Organic Structure Analysis

Phillip Crews,Jaime Rodríguez,Marcel Jaspars
Organic Structure Analysis Book PDF

Author : Phillip Crews,Jaime Rodríguez,Marcel Jaspars
Publisher : Oxford University Press, USA
Page : 664 pages
File Size : 42,5 Mb
Release : 2010
Category : Medical
ISBN : STANFORD:36105133005210

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Organic Structure Analysis by Phillip Crews,Jaime Rodríguez,Marcel Jaspars Pdf

The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods. FEATURES * Focus on Structure: Opens with structural elements and then considers the characteristics, advantages, and disadvantages of spectroscopic methods. Includes coverage of the steps used in determining a molecular structure, the limitations to organic structure determination by spectroscopic methods, and an "Organic Structure Analyses Gone Bad" table (all unique to this text) * Practical Organization: Presents the most commonly used methods first, beginning with an overview of strategies, followed by the use of NMR, and then moving on to mass spectrometry, infrared, and ultraviolet * Innovative Real-World Problem-Solving Approach: Follows the actual information flow used by chemists to solve molecular structures, as opposed to the standard methods-based approach of other texts * Unique Chapter (12) Featuring 51 Structure-Solving Problems: Each problem emphasizes a different method; the problems increase in difficulty throughout the chapter, successively building on students' knowledge and requiring them to integrate multiple methods to identify molecules. NEW TO THE SECOND EDITION * Coverage of the Latest Instrumental and Computational Advances: Examines the use of modern instruments, data processing, and computer-assisted structure elucidation techniques * Updated and Expanded Treatment of NMR (Chapters 2-5): An extensively revised Chapter 5 discusses multi-pulse 1D and 2D NMR methods, 1D TOCSY and 1D NOESY sequences, and using NOESY and ROESY in determining relative stereochemistry and solution conformation. * Additional Coverage of Mass Spectrometry: A new chapter (7) expands the discussion of mass spectrometry to three chapters (6-8). Topics include cutting-edge MS instrumentation and new information on tandem MS techniques, combining NMR with MS, large-molecule MS, chemo-informatics, and more. * More Exercises and Improved Spectra: The second edition includes 25% more problems than the previous edition (279 total). In addition, many of the spectra, including all of those presented in Chapters 11 and 12, have been reprocessed or reacquired for greater clarity.

Structure Elucidation in Organic Chemistry

Maria-Magdalena Cid,Jorge Bravo
Structure Elucidation in Organic Chemistry Book PDF

Author : Maria-Magdalena Cid,Jorge Bravo
Publisher : John Wiley & Sons
Page : 552 pages
File Size : 41,8 Mb
Release : 2015-01-05
Category : Science
ISBN : 9783527664634

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Structure Elucidation in Organic Chemistry by Maria-Magdalena Cid,Jorge Bravo Pdf

Intended for advanced readers, this is a review of all relevant techniques for structure analysis in one handy volume. As such, it provides the latest knowledge on spectroscopic and related techniques for chemical structure analysis, such as NMR, optical spectroscopy, mass spectrometry and X-ray crystallography, including the scope and limitation of each method. As a result, readers not only become acquainted with the techniques, but also the advantages of the synergy between them. This enables them to choose the correct analytical method for each problem, saving both time and resources. Special emphasis is placed on NMR and its application to absolute configuration determination and the analysis of molecular interactions. Adopting a practical point of view, the author team from academia and industry guarantees both solid methodology and applications essential for structure determination, equipping experts as well as newcomers with the tools to solve any structural problem.

Structure Determination from Powder Diffraction Data

William I. F. David
Structure Determination from Powder Diffraction Data Book PDF

Author : William I. F. David
Publisher : OUP Oxford
Page : 358 pages
File Size : 41,6 Mb
Release : 2002
Category : Language Arts & Disciplines
ISBN : 9780198500919

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Structure Determination from Powder Diffraction Data by William I. F. David Pdf

Our understanding of the properties of materials, from drugs and proteins to catalysts and ceramics, is almost always based on structural information. This book describes the new developments in the realm of powder diffraction which make it possible for scientists to obtain such information even from polycrystalline materials. Written and edited by experts active in the field, and covering both the fundamental and applied aspects of structure solution from powder diffraction data, this book guides both novices and experienced practitioners alike through the maze of possibilities.

Organic Structures from Spectra

L. D. Field,S. Sternhell,John R. Kalman
Organic Structures from Spectra Book PDF

Author : L. D. Field,S. Sternhell,John R. Kalman
Publisher : Unknown
Page : 304 pages
File Size : 40,9 Mb
Release : 1995-12-26
Category : Science
ISBN : STANFORD:36105018313846

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Organic Structures from Spectra by L. D. Field,S. Sternhell,John R. Kalman Pdf

Offers a realistic approach to solving problems used by organic chemists. Covering all the major spectroscopic techniques, it provides a graded set of problems that develop and consolidate students' understanding of organic spectroscopy. This edition contains more elementary problems and a modern approach to NMR spectra.

Spectrometric Identification of Organic Compounds

Robert Milton Silverstein,Francis X. Webster,David J. Kiemle
Spectrometric Identification of Organic Compounds Book PDF

Author : Robert Milton Silverstein,Francis X. Webster,David J. Kiemle
Publisher : Unknown
Page : 0 pages
File Size : 44,7 Mb
Release : 2005
Category : Organic compounds
ISBN : 0471429139

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Spectrometric Identification of Organic Compounds by Robert Milton Silverstein,Francis X. Webster,David J. Kiemle Pdf

Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist

Organic Chemistry

Robert V. Hoffman
Organic Chemistry Book PDF

Author : Robert V. Hoffman
Publisher : John Wiley & Sons
Page : 400 pages
File Size : 50,5 Mb
Release : 2004-11-26
Category : Science
ISBN : 9780471648727

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Organic Chemistry by Robert V. Hoffman Pdf

Ideal for those who have previously studies organic chemistry butnot in great depth and with little exposure to organic chemistry ina formal sense. This text aims to bridge the gap betweenintroductory-level instruction and more advanced graduate-leveltexts, reviewing the basics as well as presenting the more advancedideas that are currently of importance in organic chemistry. * Provides students with the organic chemistry background requiredto succeed in advanced courses. * Practice problems included at the end of each chapter.

Organic Structures from Spectra

L. D. Field,S. Sternhell,J. R. Kalman
Organic Structures from Spectra Book PDF

Author : L. D. Field,S. Sternhell,J. R. Kalman
Publisher : John Wiley & Sons
Page : 512 pages
File Size : 40,6 Mb
Release : 2013-02-18
Category : Science
ISBN : 9781118325452

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Organic Structures from Spectra by L. D. Field,S. Sternhell,J. R. Kalman Pdf

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: • includes more than 250 new spectra and more than 25 completely new problems; • now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C H Correlation spectroscopy, HMBC, NOESY and TOCSY); • has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; • contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents Preface Introduction Ultraviolet Spectroscopy Infrared Spectroscopy Mass Spectrometry Nuclear Magnetic Resonance Spectroscopy 2DNMR Problems Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”. Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”