A Handbook Of Derivatives For Mass Spectrometry

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A Handbook of Derivatives for Mass Spectrometry

Vladimir Zaikin,John M. Halket
A Handbook of Derivatives for Mass Spectrometry Book PDF

Author : Vladimir Zaikin,John M. Halket
Publisher : IM Publications
Page : 545 pages
File Size : 41,7 Mb
Release : 2009
Category : Derivatization
ISBN : 9781901019094

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A Handbook of Derivatives for Mass Spectrometry by Vladimir Zaikin,John M. Halket Pdf

Chemical derivatisation of functional groups has proved popular since the beginning of organic mass spectrometry as a means to enhance the stability and volatility of the analytes as well as facilitating structure elucidation. This book provides comprehensive information on the wide range of derivatisation methods. Each chapter looks at a particular area of derivatisation and includes extensive references to the literature for further research where necessary. There are nearly 1800 references, which, as well as full bibliographic information, include chapter/paper titles where appropriate and Digital Object Identifiers (DOIs) to allow easy retrieval of the online version of the referenced publication. The emergence of atmospheric pressure ionisation and other soft ionisation techniques has not diminished the interest in such chemical techniques, as witnessed by the many chemical tags used in quantitative proteomics (Chapter 9). The last two chapters, a substantial part of the book, deal with derivatisation for use with soft ionisation of both small and large molecules. Chapters Silylation Acylation Alkylation (Arylation) Cyclic derivatives Monofunctional compounds Polyfunctional compounds On-line derivatisation/degradation Soft ionisation—small molecules Soft ionisation—large molecules

Handbook of Derivatives for Chromatography

Karl Blau,John M. Halket
Handbook of Derivatives for Chromatography Book PDF

Author : Karl Blau,John M. Halket
Publisher : John Wiley & Sons
Page : 406 pages
File Size : 49,5 Mb
Release : 1993-08-20
Category : Science
ISBN : UOM:39015026874803

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Handbook of Derivatives for Chromatography by Karl Blau,John M. Halket Pdf

A practical handbook of derivatives and an invaluable reference source for chemists using chromatography for derivatization. Since publication of the first edition in 1977, there have been many developments in chemical derivatization which have gone hand-in-hand with advances in chromatography. This handbook will be of use not only in core chemistry but also in food analysis, clinical and biochemical analysis, toxicological, environmental and forensic testing and refining.

Handbook of Analytical Derivatization Reactions

Daniel R. Knapp
Handbook of Analytical Derivatization Reactions Book PDF

Author : Daniel R. Knapp
Publisher : John Wiley & Sons
Page : 772 pages
File Size : 48,7 Mb
Release : 1979-09-10
Category : Science
ISBN : 047103469X

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Handbook of Analytical Derivatization Reactions by Daniel R. Knapp Pdf

Brings together practical information previously available only innumerous separate sources. Handbook of Analytical DerivationReactions begins with an overview of analytical derivatizationwith a section on apparatus. Describes analytical derivatizationmethods organized according to the sample to be derivatized.Discussion of methods includes derivative type, reagent, sampletype, reaction, and typical procedure with comments and referencesfor each.

Gas Chromatography and Mass Spectrometry: A Practical Guide

O. David Sparkman,Zelda Penton,Fulton G. Kitson
Gas Chromatography and Mass Spectrometry A Practical Guide Book PDF

Author : O. David Sparkman,Zelda Penton,Fulton G. Kitson
Publisher : Academic Press
Page : 632 pages
File Size : 40,8 Mb
Release : 2011-05-17
Category : Science
ISBN : 0080920152

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Gas Chromatography and Mass Spectrometry: A Practical Guide by O. David Sparkman,Zelda Penton,Fulton G. Kitson Pdf

The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. Covers the practical instruction necessary for successful operation of GC/MS equipment Reviews the latest advances in instrumentation, ionization methods, and quantitation Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner A true benchtop reference A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) Quick References to data interpretation Ready source for information on new analyses

Chemical Ionization Mass Spectrometry

Alex. G. Harrison
Chemical Ionization Mass Spectrometry Book PDF

Author : Alex. G. Harrison
Publisher : Routledge
Page : 222 pages
File Size : 50,5 Mb
Release : 2018-05-11
Category : Science
ISBN : 9781351461535

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Chemical Ionization Mass Spectrometry by Alex. G. Harrison Pdf

The only comprehensive guide to CIMS applications in structural elucidation and analytical studies Chemical Ionization Mass Spectrometry, 2nd Edition, provides a comprehensive, up-to-date review of CIMS applications in structural elucidation and quantitative analytical studies. For the benefit of readers without a background in gaseous ion chemistry, a thorough review is presented in Chapter 2. Other chapters discuss such topics as reagent ion systems within the context of the thermochemistry and kinetics of the ionization process, including reactions and the type of information obtained; isotopic exchange reactions; stereochemical effects in chemical ionization; and reactive ion/molecule collisions in quadrupole cells. Chemical ionization mass spectra of 13 classes of compounds are discussed in detail to illustrate the influence of different functional groups on the spectra observed. Chemical Ionization Mass Spectrometry, 2nd Edition will be a valuable reference for anyone interested in mass spectrometry and gaseous ion chemistry in general.

Mass Spectrometry Handbook

Mike S. Lee
Mass Spectrometry Handbook Book PDF

Author : Mike S. Lee
Publisher : John Wiley & Sons
Page : 1362 pages
File Size : 55,8 Mb
Release : 2012-05-08
Category : Science
ISBN : 9780470536735

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Mass Spectrometry Handbook by Mike S. Lee Pdf

Due to its enormous sensitivity and ease of use, mass spectrometry has grown into the analytical tool of choice in most industries and areas of research. This unique reference provides an extensive library of methods used in mass spectrometry, covering applications of mass spectrometry in fields as diverse as drug discovery, environmental science, forensic science, clinical analysis, polymers, oil composition, doping, cellular research, semiconductor, ceramics, metals and alloys, and homeland security. The book provides the reader with a protocol for the technique described (including sampling methods) and explains why to use a particular method and not others. Essential for MS specialists working in industrial, environmental, and clinical fields.

Mass Spectrometry

Reg Davis,Martin Frearson
Mass Spectrometry Book PDF

Author : Reg Davis,Martin Frearson
Publisher : John Wiley & Sons
Page : 630 pages
File Size : 48,8 Mb
Release : 1987
Category : Science
ISBN : UOM:49015001473082

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Mass Spectrometry by Reg Davis,Martin Frearson Pdf

Mass spectrometry has undergone a great deal of development as an empirical subject and many useful approaches to the analysis and identification of organic molecules have been developed without a detailed understanding of theory of ion behaviour. This is also the way in which the subject is usually approached and it is the tack adopted here. That does not mean to say that an understanding of ion behaviour is not important - it is, but that understanding is still being developed and this book is designed for those wishing to use mass spectrometry now.

Mass Spectrometry of Inorganic and Organometallic Compounds

William Henderson,J. Scott McIndoe
Mass Spectrometry of Inorganic and Organometallic Compounds Book PDF

Author : William Henderson,J. Scott McIndoe
Publisher : John Wiley & Sons
Page : 272 pages
File Size : 45,6 Mb
Release : 2005-07-15
Category : Science
ISBN : 9780470014301

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Mass Spectrometry of Inorganic and Organometallic Compounds by William Henderson,J. Scott McIndoe Pdf

This is the first modern book to treat inorganic and organometallic mass spectrometry simultaneously. It is textbook and handbook in one; as a textbook it introduces the techniques and gives hints on how to apply the various techniques, as a handbook it lists all available ionization techniques for just about any given compound. The book also includes non-mathematical explanations of how modern MS instruments work Mass Spectrometry of Inorganic and Organometallic Compounds will inspire the synthetic inorganic and organometallic chemist with the confidence to apply some of the new techniques to their characterization problems.

Mass Spectrometry

Jürgen H Gross
Mass Spectrometry Book PDF

Author : Jürgen H Gross
Publisher : Springer
Page : 968 pages
File Size : 42,5 Mb
Release : 2017-06-13
Category : Science
ISBN : 9783319543987

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Mass Spectrometry by Jürgen H Gross Pdf

This book offers a balanced mixture of practice-oriented information and theoretical background as well as numerous references, clear illustrations, and useful data tables. Problems and solutions are accessible via a special website. This new edition has been completely revised and extended; it now includes three new chapters on tandem mass spectrometry, interfaces for sampling at atmospheric pressure, and inorganic mass spectrometry.

Basic Gas Chromatography-Mass Spectrometry

F.W. Karasek,R.E. Clement
Basic Gas Chromatography Mass Spectrometry Book PDF

Author : F.W. Karasek,R.E. Clement
Publisher : Unknown
Page : 222 pages
File Size : 53,5 Mb
Release : 1988-02
Category : Science
ISBN : UOM:39015014899663

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Basic Gas Chromatography-Mass Spectrometry by F.W. Karasek,R.E. Clement Pdf

The book begins by covering the basic principles of both gas chromatography (GC) and mass spectrometry (MS) to the extent necessary to understand and deal with the data generated in a GC-MS analysis. The focus then turns to the particular requirements created by a direct combination of these two techniques into a single instrumentation system. The data generated and their use are covered in detail. The role of the computer and its specific software receives special attention, especially in the matter of compound identification via mass spectral search techniques. GC-MS-computer instrumentation has reached such a plateau of excellence today that the present commercial systems will not be obsolete for a long time to come. Therefore, a detailed description of these systems is not only informative but is also pertinent to the subject matter of this book. Finally, representative applications and results obtained with GC-MS-computer techniques are presented and chosen in such a way as to permit extrapolation of specific applications to similar problems encountered by the reader. To aid the reader in mastering the subject matter and increase understanding, interpretation problems and suggested readings are included. The format is instructional, informative and application-oriented with material presented in such a way as to be useful to a broad spectrum of people. The book serves as a text in its own right. The software package Gas Chromatography-Mass Spectrometry: A Knowledge Base, by F.A. Settle, Jr. and M.A. Pleva provides rapid access to a wealth of current information in the GC-MS field. Its three diskettes (51/4 inch) allow the user three ways to access: the index mode, the tree mode and a keyword search mode. The package may be purchased separately and is available for the IBM-PC and compatibles. The software provides a valuable supplement to the book.

Practical Mass Spectrometry

Brian S. Middleditch
Practical Mass Spectrometry Book PDF

Author : Brian S. Middleditch
Publisher : Springer Science & Business Media
Page : 394 pages
File Size : 50,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781461329824

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Practical Mass Spectrometry by Brian S. Middleditch Pdf

It has been estimated that more than 8090 of the world's scientists who have ever lived are still alive today. It would not be unreasonable to suggest that more than 95% of those who have ever used a mass spectrometer are not only alive but are still actively employed. Most have never had any formal training in the subject since, with a few notable exceptions, universities have only recently begun to offer courses in mass spectrometry. We have written this book for the student of modern mass spectro metry: it is for the novice who wished to know what the instruments can do and how the techniques can be applied. There are other books on the market which delve into the history of mass spectrometry and go deeply into the mathematical theory and instrumentation. There are yet more books which guide one through the art of interpreting spectra. We have deliberately avoided these topics so that the reader is confronted only with the basic principles and is allowed a taste of the applications. One of the best methods of deVeloping a useful textbook is to teach a course based upon its content. This is what we did. We met in Houston in 1976 to teach a course on "Perspectives in Mass Spectrometry" and to coordinate our writing. The authors of five of the chapters met again in St.

Handbook of GC-MS

Hans-Joachim Hübschmann
Handbook of GC MS Book PDF

Author : Hans-Joachim Hübschmann
Publisher : John Wiley & Sons
Page : 880 pages
File Size : 52,5 Mb
Release : 2015-04-22
Category : Science
ISBN : 9783527674336

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Handbook of GC-MS by Hans-Joachim Hübschmann Pdf

The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses. As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories in environmental, food, pharmaceutical and clinical analysis. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application. For this new edition the work has been now extended to two volumes, reflecting the latest developments in the technique and related instrumentation, while also incorporating several new examples of applications in many fields. The first two editions were very well received, making this handbook a must-have in all analytical laboratories using GC-MS.

Metabolomics, Metabonomics and Metabolite Profiling

William J. Griffiths
Metabolomics Metabonomics and Metabolite Profiling Book PDF

Author : William J. Griffiths
Publisher : Royal Society of Chemistry
Page : 336 pages
File Size : 47,7 Mb
Release : 2008
Category : Medical
ISBN : 9780854042999

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Metabolomics, Metabonomics and Metabolite Profiling by William J. Griffiths Pdf

In this comprehensive resource the Editor draws together experts from the field and provides an insightful introduction into the technology and methodology.

Introduction to Mass Spectrometry

J. Throck Watson,O. David Sparkman
Introduction to Mass Spectrometry Book PDF

Author : J. Throck Watson,O. David Sparkman
Publisher : John Wiley & Sons
Page : 972 pages
File Size : 51,5 Mb
Release : 2013-07-09
Category : Science
ISBN : 9781118681589

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Introduction to Mass Spectrometry by J. Throck Watson,O. David Sparkman Pdf

Completely revised and updated, this text provides an easy-to-read guide to the concept of mass spectrometry and demonstrates its potential and limitations. Written by internationally recognised experts and utilising "real life" examples of analyses and applications, the book presents real cases of qualitative and quantitative applications of mass spectrometry. Unlike other mass spectrometry texts, this comprehensive reference provides systematic descriptions of the various types of mass analysers and ionisation, along with corresponding strategies for interpretation of data. The book concludes with a comprehensive 3000 references. This multi-disciplined text covers the fundamentals as well as recent advance in this topic, providing need-to-know information for researchers in many disciplines including pharmaceutical, environmental and biomedical analysis who are utilizing mass spectrometry

Organic Mass Spectrometry in Art and Archaeology

Prof Maria Perla Colombini,Prof Francesca Modugno
Organic Mass Spectrometry in Art and Archaeology Book PDF

Author : Prof Maria Perla Colombini,Prof Francesca Modugno
Publisher : John Wiley & Sons
Page : 508 pages
File Size : 52,9 Mb
Release : 2009-07-28
Category : Science
ISBN : 9780470741924

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Organic Mass Spectrometry in Art and Archaeology by Prof Maria Perla Colombini,Prof Francesca Modugno Pdf

Offers an overview of the analysis of art and archaeological materials using techniques based on mass spectrometry Illustrates basic principles, procedures and applications of mass spectrometric techniques. Fills a gap in the field of application on destructive methods in the analysis of museum objects Edited by a world-wide respected specialists with extensive experience of the GC/MS analysis of art objects Such a handbook has been long-awaited by scientists, restorers and other experts in the analysis of art objects