Calorimetric Methods For The Characterization Of Porous Materials

Author : Juan Carlos Moreno-Piraján,Liliana Giraldo Gutiérrez,Fernando Gómez-Granados,Diana Cristina Hernández-Monje
Publisher : Elsevier
Page : 265 pages
File Size : 43,6 Mb
Release : 2024-04-01
Category : Science
ISBN : 9780443137976

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Calorimetric Methods for the Characterization of Porous Materials by Juan Carlos Moreno-Piraján,Liliana Giraldo Gutiérrez,Fernando Gómez-Granados,Diana Cristina Hernández-Monje Pdf

Calorimetric Methods for the Characterization of Porous Materials presents calorimetric methods used in the characterization of porous materials using chemical thermodynamics. Among these materials, catalysts, supports and adsorbents (such as Activated Carbon, Metal-Organic-Frameworks, SBA-15, Zeolites, Graphene, Graphite, Carbon Foams) are presented. In addition, the use of calorimetry in the study of catalytic reactions in different phases is explored—applicable to air and wastewater treatment, clean and renewable energies, green chemistry, as well as energy production and storage (Carbon dioxide, methane and hydrogen at high pressure). Chapters summarize basic concepts of thermodynamics and kinetics alongside experimental techniques such as thermal analysis and calorimetry. In addition, information is given about different calorimetric methods that can be used in studies aimed at characterizing the physicochemical properties of adsorbents, supports and solid catalysts, as well as the processes related to the adsorption-desorption phenomena of the reactants and/or products of catalytic reactions. Addresses the problems involved with the chemical thermodynamics of porous materials, with a significant practical element explaining experimental parameters and how to perform calculations Presents, in detail, the main instrumental calorimetric methods, including those that must be carefully considered to avoid experimental errors Demonstrates, step-by-step, how to perform calculations using data obtained from instrumentation to achieve reliable results Provides novel explanations on how to use calorimetry in catalyst characterization Allows readers to broaden the spectrum of the application of calorimetry in the study of materials

Author : Juan Carlos Moreno Piraján
Publisher : BoD – Books on Demand
Page : 126 pages
File Size : 47,8 Mb
Release : 2018-07-18
Category : Science
ISBN : 9781789234381

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Calorimetry by Juan Carlos Moreno Piraján Pdf

Today, calorimetry is considered an art (although some consider it a tool) that studies the energy changes that occur during a change of state. This allows physicochemical analysis to study in detail the thermodynamic systems and to evaluate the different variables that establish the characteristics of the system itself. This book illustrates how the reader can use this technique in a wide spectrum of applications.

Author : KK Unger,F. Rodríguez-Reinoso,Jean Rouquerol,Kenneth S.W. Sing
Publisher : Elsevier
Page : 781 pages
File Size : 53,5 Mb
Release : 1991-04-19
Category : Science
ISBN : 0080887481

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Characterization of Porous Solids II by KK Unger,F. Rodríguez-Reinoso,Jean Rouquerol,Kenneth S.W. Sing Pdf

The Second IUPAC Symposium on the Characterization of Porous Solids (COPS-II) provided the opportunity for detailed discussion and appraisal of the most important techniques currently used for the characterization of porous materials, especially those of technological importance. The 82 selected papers and reviews contained in this volume are mainly concerned with the theoretical and experimental aspects of adsorption, fluid penetration, small-angle scattering and spectroscopic methods with their application in the study of adsorbents, catalysts, constructional materials, etc. Particular attention is given to the characterization of carbons, oxides, zeolites, clays, cement and polymers. The wide range of materials and techniques described in this book provide a useful and comprehensive reference source for academic and industrial scientists and technologists.

Author : Mizutani Tadashi
Publisher : BoD – Books on Demand
Page : 644 pages
File Size : 55,8 Mb
Release : 2011-01-14
Category : Science
ISBN : 9789533079806

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Application of Thermodynamics to Biological and Materials Science by Mizutani Tadashi Pdf

Progress of thermodynamics has been stimulated by the findings of a variety of fields of science and technology. The principles of thermodynamics are so general that the application is widespread to such fields as solid state physics, chemistry, biology, astronomical science, materials science, and chemical engineering. The contents of this book should be of help to many scientists and engineers.

Author : Anonim
Publisher : World Scientific
Page : 1495 pages
File Size : 41,6 Mb
Release : 2020-10-20
Category : Science
ISBN : 9789811223242

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Handbook Of Porous Materials: Synthesis, Properties, Modeling And Key Applications (In 4 Volumes) by Anonim Pdf

This four-volume handbook gives a state-of-the-art overview of porous materials, from synthesis and characterization and simulation all the way to manufacturing and industrial applications. The editors, coming from academia and industry, are known for their didactic skills as well as their technical expertise. Coordinating the efforts of 37 expert authors in 14 chapters, they construct the story of porous carbons, ceramics, zeolites and polymers from varied viewpoints: surface and colloidal science, materials science, chemical engineering, and energy engineering. Volumes 1 and 2 cover the fundamentals of preparation, characterisation, and simulation of porous materials. Working from the fundamentals all the way to the practicalities of industrial production processes, the subjects include hierarchical materials, in situ and operando characterisation using NMR, X-Ray scattering and tomography, state-of-the-art molecular simulations of adsorption and diffusion in crystalline nanoporous materials, as well as the emerging areas of bio-artificing and drug delivery. Volume 3 focuses on porous materials in industrial separation applications, including adsorption separation, membrane separation, and osmotic distillation. Finally, and highly relevant to tomorrow's energy challenges, Volume 4 explains the energy engineering aspects of applying porous materials in supercapacitors, fuel cells, batteries, electrolysers and sub-surface energy applications.The text contains many high-quality colourful illustrations and examples, as well as thousands of up-to-date references to peer-reviewed articles, reports and websites for further reading. This comprehensive and well-written handbook is a must-have reference for universities, research groups and companies working with porous materials.Related Link(s)

Author : Anonim
Publisher : Unknown
Page : 404 pages
File Size : 50,5 Mb
Release : 2010-11-05
Category : Electronic
ISBN : 9781848264274

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MEMBRANE PROCESSES - Volume I by Anonim Pdf

Membrane Processes is a component of Encyclopedia of Water Sciences, Engineering and Technology Resources in the global Encyclopedia of Life Support Systems (EOLSS), which is an integrated compendium of twenty one Encyclopedias. These volumes discuss matters of great relevance to our world on desalination which is a critically important as clearly the only possible means of producing fresh water from the sea for many parts of the world. The two volumes present state-of-the art subject matter of various aspects of Membrane Processes such as: History And Current Status Of Membrane Desalination Processes; Membrane Science And Reclamation; Membrane Characterization; Principles And Practices Of Reverse Osmosis; Reverse Osmosis: Introduction; Hollow-Fiber Membranes; Preparation And Characterization Of Ionexchange Membranes; Preparation And Characterization Of Micro- And Ultrafiltration Membranes; Membrane Distillation; Desalination By Membrane Distillation; Pervaporation;Dialysis And Diffusion Dialysis; Donnan Dialysis; Modeling And Calculation Of Pressure-Driven Membrane Processes; Survey Of Theoretical Approaches To Modeling; Pressure-Driven Membrane. Processes(Submodels For Transport In Phases); Reverse Osmosis Process And System Design; Practical Aspects Of Large-Scale Reverse Osmosis Applications; Health, Safety And Environmental Considerations; Membrane Separation Technologies; Concentration Of Liquid Foods; Mass Transfer Operation–Membrane Separations; Mass Transfer Operations: Hybrid Membrane Processes; Recent Advances In Membrane Science And Technology In Seawater Desalination – With Technology Development In The Middle East And Singapore. These volumes are aimed at the following five major target audiences: University and College Students Educators, Professional Practitioners, Research Personnel and Policy and Decision Makers

Author : G Q Max Lu,Xiu Song Zhao
Publisher : World Scientific
Page : 911 pages
File Size : 51,9 Mb
Release : 2004-11-22
Category : Technology & Engineering
ISBN : 9781783261796

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Nanoporous Materials: Science And Engineering by G Q Max Lu,Xiu Song Zhao Pdf

Porous materials are of scientific and technological importance because of the presence of voids of controllable dimensions at the atomic, molecular, and nanometer scales, enabling them to discriminate and interact with molecules and clusters. Interestingly the big deal about this class of materials is about the “nothingness” within — the pore space. International Union of Pure and Applied Chemistry (IUPAC) classifies porous materials into three categories — micropores of less than 2 nm in diameter, mesopores between 2 and 50 nm, and macropores of greater than 50 nm. In this book, nanoporous materials are defined as those porous materials with pore diameters less than 100 nm.Over the last decade, there has been an ever increasing interest and research effort in the synthesis, characterization, functionalization, molecular modeling and design of nanoporous materials. The main challenges in research include the fundamental understanding of structure-property relations and tailor-design of nanostructures for specific properties and applications. Research efforts in this field have been driven by the rapid growing emerging applications such as biosensor, drug delivery, gas separation, energy storage and fuel cell technology, nanocatalysis and photonics. These applications offer exciting new opportunities for scientists to develop new strategies and techniques for the synthesis and applications of these materials.This book provides a series of systematic reviews of the recent developments in nanoporous materials. It covers the following topics: (1) synthesis, processing, characterization and property evaluation; (2) functionalization by physical and/or chemical treatments; (3) experimental and computational studies on fundamental properties, such as catalytic effects, transport and adsorption, molecular sieving and biosorption; (4) applications, including photonic devices, catalysis, environmental pollution control, biological molecules separation and isolation, sensors, membranes, hydrogen and energy storage, etc./a

Author : Anonim
Publisher : Elsevier
Page : 808 pages
File Size : 55,8 Mb
Release : 2002-11-14
Category : Science
ISBN : 0080528910

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Characterization of Porous Solids VI by Anonim Pdf

This book contains 99 of the papers that were presented at the 6th in the series of Symposia on Characterization of Porous Solids held in Alicante, Spain, May 2002. Written by leading international specialists in the subject, the contributions represent an up-to-date and authoritative account of recent developments around the world in the major methods used to characterize porous solids. The book is a useful work of reference for anyone interested in characterizing porous solids, such as MCM-41 mesoporous materials, pillared clays, etc. Papers on pore structure determination using gas adsorption feature strongly, together with papers on small angle scattering methods, mercury porosimetry, microcalorimetry, scanning probe microscopies, and image analysis.

Author : Prashant Kesharwani,Kamalinder K. Singh
Publisher : Academic Press
Page : 674 pages
File Size : 45,9 Mb
Release : 2021-11-06
Category : Technology & Engineering
ISBN : 9780128209189

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Nanoparticle Therapeutics by Prashant Kesharwani,Kamalinder K. Singh Pdf

Nanoparticle therapeutics: Production Technologies, Types of Nanoparticles, and Regulatory Aspects employs unique principles for applications in cell-based therapeutics, diagnostics and mechanistics for the study of organ physiology, disease etiology and drug screening of advanced nanoparticles and nanomaterials. The book focuses on the extrapolation of bioengineering tools in the domain of nanotechnology and nanoparticles therapeutics, fabrication, characterization and drug delivery aspects. It acquaints scientists and researchers on the experiential and experimental aspects of nanoparticles and nanotechnology to equip their rational application in various fields, especially in differential diagnoses and in the treatment of diverse diseased states. This complete resource provides a holistic understanding of the principle behind formation, characterization, applications, regulations and toxicity of nanoparticles employing myriad principles of nanotechnology. Investigators, pharmaceutical researchers, and advanced students working on technology advancement in the areas of designing targeted therapies, nanoscale imaging systems and diagnostic modalities in human diseases where nanoparticles can be used as a critical tool for technology advancement in drug delivery systems will find this book useful. Brings together the novel applications of nanotechnology in biological fields Explores perspectives on technologies through highly organized tables, illustrative figures and flow charts Addresses key multidisciplinary challenges faced by nanotechnologists to foster collaboration among biologists, chemists, physicists, engineers and clinicians

Author : H. Kral,Jean Rouquerol,Kenneth S.W. Sing,KK Unger
Publisher : Elsevier
Page : 644 pages
File Size : 54,7 Mb
Release : 1988-04-01
Category : Technology & Engineering
ISBN : 0080960731

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Characterization of Porous Solids by H. Kral,Jean Rouquerol,Kenneth S.W. Sing,KK Unger Pdf

The importance of porosity has long been recognized by scientists and engineers. Porous solids are widely encountered in industry and everyday life and their behaviour, e.g. chemical reactivity, adsorptive capacity, and catalytic activity is dependent on their pore structure. A considerable amount of work on porous solids has been undertaken both in academic and in industrial laboratories. However, all this activity is in urgent need of a critical appraisal. To undertake this task, a number of leading experts in the field of adsorption, porosimetry, X-ray and neutron scattering, optical and electron microscopy, calorimetry and fluid permeation, were brought together at the 1987 IUPAC (COPS I) Symposium. This proceedings volume provides an up-to-date overall review of the theoretical foundations for modelling and characterizing porous systems. It deals with most of the techniques in current use as applied to both model systems and porous solids of industrial importance. The reader will find the description and discussion of a number of novel techniques as well as a critical appraisal and comparison of the more established methods. All those concerned with the characterization of porous solids in academic and industrial laboratories will find much to interest them in this volume. It should be on the bookshelf of applied research centres involved in adsorption, catalysis, purification of gases and liquids, pigments, fillers, building materials, etc.

Author : Andrew J. Milling
Publisher : CRC Press
Page : 432 pages
File Size : 55,6 Mb
Release : 1999-08-03
Category : Science
ISBN : 0824773365

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Surface Characterization Methods by Andrew J. Milling Pdf

"Outlines the scientific basis and experimental methods for a broad sample of surface analysis techniques, drawing heavily from established principles of physical and analytical chemistry. Sketches a simple low-cost method of tracking particles in three dimensions."

Author : Abhijit Chatterjee
Publisher : CRC Press
Page : 354 pages
File Size : 55,6 Mb
Release : 2010-05-17
Category : Science
ISBN : 9781420082753

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Structure Property Correlations for Nanoporous Materials by Abhijit Chatterjee Pdf

Nanoporous materials are critical to various fields of research, including ion exchange, separation, catalysis, sensor applications, biological molecular isolation, and purification. In addition, they offer new opportunities in such areas as inclusion chemistry, guest-host synthesis, and molecular manipulations and reactions at the nanoscale. In St

Author : Yuriy L. Zub,Vadim G. Kessler
Publisher : Springer Science & Business Media
Page : 505 pages
File Size : 53,6 Mb
Release : 2008-07-01
Category : Technology & Engineering
ISBN : 9781402085147

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Sol-Gel Methods for Materials Processing by Yuriy L. Zub,Vadim G. Kessler Pdf

Sol-gel processing is a soft-chemistry method to obtain functional materials at low temperatures. This route can be used to produce very sophisticated nanomaterials and to tailor the materials to very specific applications. Adsorption and detection of pollutants, water purification and soil remediation represent challenging fields of application that can be exploited by sol-gel materials. In this volume several contributions from invited speakers and participants at the NATO advanced research workshop on "Sol-gel approaches to materials for pollution control, water purification and soil remediation", which has been held in Kiev, Ukraine on October 2007, are reported. The book offers a wide and updated overview of the most advanced sol-gel methods for materials processing and at the same time presents several case studies concerning possible solutions for environmental issues. General articles on sol-gel from the invited speakers and focused research articles allow getting inside sol-gel applications on this very important field.

Author : Aline Auroux,Ljiljana Damjanović-Vasilić
Publisher : Walter de Gruyter GmbH & Co KG
Page : 412 pages
File Size : 41,5 Mb
Release : 2023-07-03
Category : Technology & Engineering
ISBN : 9783110590449

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Thermal Analysis and Calorimetry by Aline Auroux,Ljiljana Damjanović-Vasilić Pdf

Author : Arthur W. Chester,E.G. Derouane
Publisher : Springer Science & Business Media
Page : 372 pages
File Size : 44,9 Mb
Release : 2009-10-03
Category : Science
ISBN : 9781402096785

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Zeolite Characterization and Catalysis by Arthur W. Chester,E.G. Derouane Pdf

The idea for putting together a tutorial on zeolites came originally from my co-editor, Eric Derouane, about 5 years ago. I ?rst met Eric in the mid-1980s when he spent 2 years working for Mobil R&D at our then Corporate lab at Princeton, NJ. He was on the senior technical staff with projects in the synthesis and characterization of new materials. At that time, I managed a group at our Paulsboro lab that was responsible for catalyst characterization in support of our catalyst and process development efforts, and also had a substantial group working on new material synthesis. Hence, our interests overlapped considerably and we met regularly. After Eric moved back to Namur (initially), we maintained contact, and in the 1990s, we met a number of times in Europe on projects of joint interest. It was after I retired from ExxonMobil in 2002 that we began to discuss the tutorial concept seriously. Eric had (semi-)retired and lived on the Algarve, the southern coast of Portugal. In January 2003, my wife and I spent 3 weeks outside of Lagos, and I worked parts of most days with Eric on the proposed content of the book. We decided on a comprehensive approach that ultimately amounted to some 20+ chapters covering all of zeolite chemistry and catalysis and gave it the title Zeolite Chemistry and Catalysis: An integrated Approach and Tutorial.