Classical Split And Splitless Injection In Capillary Gas Chromatography

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Split and Splitless Injection for Quantitative Gas Chromatography

Author : Konrad Grob
Publisher : John Wiley & Sons
Page : 480 pages
File Size : 53,8 Mb
Release : 2008-11-21
Category : Science
ISBN : 9783527612888

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Split and Splitless Injection for Quantitative Gas Chromatography by Konrad Grob Pdf

This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography

Gas Chromatography with Glass Capillary Columns

Author : Walter Jennings
Publisher : Elsevier
Page : 193 pages
File Size : 44,5 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780323141062

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Gas Chromatography with Glass Capillary Columns by Walter Jennings Pdf

Gas Chromatography with Glass Capillary Columns describes glass capillary technology and the selection, installation, evaluation, and use of glass open tubular columns for gas chromatography. Discussions are organized around the glass capillary column; column coating and installation; inlet systems; measurement of column efficiency; temperature programming and carrier flow; and retention behavior. Column selection and stability and sample preparation are also covered. This text is comprised of 13 chapters; the first of which introduces the reader to the practical considerations involved in the selection, installation, evaluation, and use of high-resolution open tubular glass capillary columns, along with the theory of the chromatographic process. The discussion then turns to the influence of operating parameters and storage conditions on the interrelated forces involved in coating glass capillary columns; the dynamic and static techniques of column coating; and design defects in the inlet system caused by excessive volume and dead space. The chapters that follow focus on general considerations in column attachment, measurement of column efficiency, and retention behavior of carrier gas, along with the operating temperature of the column, the choice of carrier gas, and carrier gas velocity. This book also looks at the factors that affect column stability, materials of restricted volatility, and some applications of glass capillary gas chromatography. This reference material is intended primarily for students and researchers interested in gas chromatography with glass capillary columns.

Capillary Gas Chromatography

Author : David W. Grant
Publisher : John Wiley & Sons
Page : 316 pages
File Size : 47,8 Mb
Release : 2009
Category : Electronic
ISBN : 8126519622

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Capillary Gas Chromatography by David W. Grant Pdf

Chromatographic Analysis of Pharmaceuticals

Author : John A. Adamovics
Publisher : Routledge
Page : 542 pages
File Size : 50,8 Mb
Release : 2017-09-29
Category : Science
ISBN : 9781351460859

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Chromatographic Analysis of Pharmaceuticals by John A. Adamovics Pdf

Updated and revised throughout. Second Edition explores the chromatographic methods used for the measurement of drugs, impurities, and excipients in pharmaceutical preparations--such as tablets, ointments, and injectables. Contains a 148-page table listing the chromatographic data of over 1300 drugs and related substances--including sample matrix analyzed, sample handling procedures, column packings, mobile phase, mode of detection, and more.

Handbook of GC/MS

Author : Hans-Joachim Hübschmann
Publisher : John Wiley & Sons
Page : 735 pages
File Size : 47,7 Mb
Release : 2008-12-03
Category : Science
ISBN : 9783527314270

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Handbook of GC/MS by Hans-Joachim Hübschmann Pdf

This is the first comprehensive reference work for GC/MS now in its second edition. It offers broad coverage, from sample preparation to the evaluation of MS-Data, including library searches. Fundamentals, techniques, and applications are described. A large part of the book is devoted to numerous examples for GC/MS-applications in environmental, food, pharmaceutical and clinical analysis. These proven examples come from the daily practice of various laboratories. The book also features a glossary of terms and a substance index that helps the reader to find information for his particular analytical problem. The author presents in a consistent and clear style his experience from numerous user workshops which he has organized. This is a thoroughly revised and updated English edition based on an edition which was highly successful in Germany.

Modern Practice of Gas Chromatography

Author : Robert L. Grob, PhD,Eugene F. Barry
Publisher : John Wiley & Sons
Page : 1059 pages
File Size : 44,6 Mb
Release : 2004-08-04
Category : Science
ISBN : 9780471651154

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Modern Practice of Gas Chromatography by Robert L. Grob, PhD,Eugene F. Barry Pdf

The bible of gas chromatography-offering everything the professional and the novice need to know about running, maintaining, and interpreting the results from GC Analytical chemists, technicians, and scientists in allied disciplines have come to regard Modern Practice of Gas Chomatography as the standard reference in gas chromatography. In addition to serving as an invaluable reference for the experienced practitioner, this bestselling work provides the beginner with a solid understanding of gas chromatographic theory and basic techniques. This new Fourth Edition incorporates the most recent developments in the field, including entirely new chapters on gas chromatography/mass spectrometry (GC/MS); optimization of separations and computer assistance; high speed or fast gas chromatography; mobile phase requirements: gas system requirements and sample preparation techniques; qualitative and quantitative analysis by GC; updated information on detectors; validation and QA/QC of chromatographic methods; and useful hints for good gas chromatography. As in previous editions, contributing authors have been chosen for their expertise and active participation in their respective areas. Modern Practice of Gas Chromatography, Fourth Edition presents a well-rounded and comprehensive overview of the current state of this important technology, providing a practical reference that will greatly appeal to both experienced chomatographers and novices.

Recent Advances in Capillary Gas Chromatography

Author : Wolfgang Bertsch,Walter Jennings,Rudolf E. Kaiser
Publisher : Unknown
Page : 614 pages
File Size : 47,9 Mb
Release : 1981
Category : Science
ISBN : UOM:39015016083712

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Recent Advances in Capillary Gas Chromatography by Wolfgang Bertsch,Walter Jennings,Rudolf E. Kaiser Pdf

Chemical Analysis of Food: Techniques and Applications

Author : Yolanda Picó
Publisher : Academic Press
Page : 814 pages
File Size : 48,9 Mb
Release : 2012-07-18
Category : Science
ISBN : 9780123848628

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Chemical Analysis of Food: Techniques and Applications by Yolanda Picó Pdf

"The book contains twenty three chapters written by experts on the subject, is structured in two parts: the first one describes the role of the latest developments in analytical and bioanalytical techniques, and the second one deals with the most innovative applications and issues in food analysis. The two first introductory chapters about sampling technique, from basic one to the most recent advances, which is still a food challenge because is responsible of the quality and assurance of the analysis, and on data analysis and chemometrics are followed by a review of the most recently applied techniques in process (on-line) control and in laboratories for the analysis of major or minor compounds of food. These techniques ranged from the non-invasive and non-destructive ones, such as infrared spectroscopy, magnetic resonance and ultrasounds, to emerging areas as nanotechnology, biosensors and electronic noses and tongues, including those already well-established in food analysis, such as chromatographic and electrophoretic techniques. These chapters also include two important tools for solving problems in chemical and biological analysis such as mass spectrometry and molecular-based techniques"--Provided by publisher.

Handbook of GC-MS

Author : Hans-Joachim Hübschmann
Publisher : John Wiley & Sons
Page : 880 pages
File Size : 45,6 Mb
Release : 2015-04-27
Category : Science
ISBN : 9783527674329

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Handbook of GC-MS by Hans-Joachim Hübschmann Pdf

The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses. As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories in environmental, food, pharmaceutical and clinical analysis. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application. For this new edition the work has been now extended to two volumes, reflecting the latest developments in the technique and related instrumentation, while also incorporating several new examples of applications in many fields. The first two editions were very well received, making this handbook a must-have in all analytical laboratories using GC-MS.

Instrumental Methods in Food and Beverage Analysis

Author : D.L.B. Wetzel,G. Charalambous
Publisher : Elsevier
Page : 629 pages
File Size : 43,7 Mb
Release : 1998-05-29
Category : Technology & Engineering
ISBN : 0080534759

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Instrumental Methods in Food and Beverage Analysis by D.L.B. Wetzel,G. Charalambous Pdf

Advances in instrumentation and applied instrumental analysis methods have allowed scientists concerned with food and beverage quality, labeling, compliance, and safety to meet ever increasing analytical demands. Texts dealing with instrumental analysis alone are usually organized by the techniques without regard to applications. The biannual review issue of Analytical Chemistry under the topic of Food Analysis is organized by the analyte such as N and protein, carbohydrate, inorganics, enzymes, flavor and odor, color, lipids, and vitamins. Under 'flavor and odor' the subdivisions are not along the lines of the analyte but the matrix (e.g. wine, meat, dairy, fruit) in which the analyte is being determined. In "Instrumentation in Food and Beverage Analysis" the reader is referred to a list of 72 entries entitled "Instrumentation and Instrumental Techniques" among which molecular spectroscopy, chromatographic and other sophisticated separations in addition to hyphenated techniques such as GS-Mass spectrometry. A few of the entries appear under a chapter named for the technique. Most of the analytical techniques used for determination, separations and sample work prior to determination are treated in the context of an analytical method for a specific analyte in a particular food or beverage matrix with which the author has a professional familiarity, dedication, and authority. Since, in food analysis in particular, it is usually the food matrix that presents the research analytical chemist involved with method development the greatest challenge.