Mixing And Crystallization

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Mixing and Crystallization

Bhaskar Sen Gupta,Shaliza Ibrahim
Mixing and Crystallization Book PDF

Author : Bhaskar Sen Gupta,Shaliza Ibrahim
Publisher : Springer Science & Business Media
Page : 333 pages
File Size : 41,8 Mb
Release : 2013-03-14
Category : Science
ISBN : 9789401722902

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Mixing and Crystallization by Bhaskar Sen Gupta,Shaliza Ibrahim Pdf

We are honoured to present this collection of selected papers from the International Conference on Mixing and Crystallization, held at the Tioman Island, Malaysia in April, 1998. We are grateful to the editorial board comprising five eminent researchers in the field of mixing and crystallization for their thoughtful review and suggestions. In order to make this book as current as possible some of the papers have been thoroughly revised, which caused some delay in bringing out this edited version. We received necessary support from the Institute of Post Graduate Studies and Research, the University of Malaya and the Special Research Centre for Multiphase Processes, and the University of Newcastle, Australia in organizing this conference. We are indebted to the Institute of Chemical Engineers, United Kingdom, and the Institution of Engineers, Malaysia for their sponsorship. We would like to thank K.C. Lim, Dr. C. Ramakanth and Ms. Zubaidah for their help at the various stages of editing. We would also like to express our gratitude to Professor Mohd. Ali Hashim and Dr. Nafis Ahmed for their help and encouragement. Finally, I would like to thank Kluwer Academic Publishers for publishing this book. Bhaskar Sen Gupta Shaliza Ibrahim University of Malaya, Kuala Lumpur xi CFD MODELLING OF HYDRODYNAMIC CONDITIONS WITHIN THE WAKE OF MIXING IMPELLER BLADES 1 G.D. RIGByl., G. LANE . AND G.M. EVANSl.

Handbook of Industrial Crystallization

Allan Myerson
Handbook of Industrial Crystallization Book PDF

Author : Allan Myerson
Publisher : Butterworth-Heinemann
Page : 304 pages
File Size : 40,9 Mb
Release : 2002-01-08
Category : Science
ISBN : 0080533515

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Handbook of Industrial Crystallization by Allan Myerson Pdf

Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes. The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the field Covers all aspects of industrial crystallization in a single, complete volume

Crystallization

Wolfgang Beckmann
Crystallization Book PDF

Author : Wolfgang Beckmann
Publisher : John Wiley & Sons
Page : 370 pages
File Size : 47,7 Mb
Release : 2013-01-14
Category : Science
ISBN : 9783527650347

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Crystallization by Wolfgang Beckmann Pdf

Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

Crystallization of Organic Compounds

Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Crystallization of Organic Compounds Book PDF

Author : Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Publisher : John Wiley & Sons
Page : 388 pages
File Size : 47,9 Mb
Release : 2023-07-05
Category : Science
ISBN : 9781119879480

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Crystallization of Organic Compounds by Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley Pdf

Crystallization of Organic Compounds Practical resource covering applications of crystallization principles with methodologies, case studies, and numerous industrial examples for emphasis Based on the authors’ hands-on experiences as process engineers, through the use of case studies and examples of crystallization processes, ranging from laboratory development through manufacturing scale-up, Crystallization of Organic Compounds guides readers through the practical applications of crystallization and emphasizes strategies that have proven to be successful, enabling readers to avoid common pitfalls that can render standard procedures unsuccessful. Most chapters feature multiple examples that guide readers, step by step, through the crystallization of active pharmaceutical ingredients (APIs), including an analysis of the major methods of carrying out crystallization operations, their strengths and potential issues, as well as numerous examples of crystallization processes from development through manufacturing scale. Advancements in the field of crystallization have been integrated throughout the book in the newly revised Second Edition to ensure the content adequately reflects current state-of-the-art industrial know-hows and practice. The new edition also adds chapters addressing downstream operations after the crystallization, including filtration/washing and drying, together with industrial use cases. Crystallization of Organic Compounds includes detailed information on: Solubility and solid behavior, covering phase rule, polymorph, salt/co-crystal, chiral resolution and in-silico solubility prediction; and kinetics, covering seed, supersaturation, nucleation, crystal growth and model-based experimental design Critical issues in the crystallization practice, covering oiling out, seeding/wet-milling, agglomeration/aggregation, mixing scale-up and quality-by-design principles Cooling, anti-solvent, evaporation and reactive crystallization process design, covering batch and continuous operations with industrial examples Special applications, covering crystallization with ultrasound, reaction selectivity enhancement, and computation fluid dynamics, and solid dispersion With highly practical coverage of the subject, Crystallization of Organic Compounds is an essential resource for engineers and chemists involved with the development, scaling, or operation of crystallization process in the pharmaceutical and fine chemical industries, particularly those with degrees in chemical engineering and chemistry.

Crystallization of Organic Compounds

Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Crystallization of Organic Compounds Book PDF

Author : Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Publisher : John Wiley & Sons
Page : 304 pages
File Size : 49,7 Mb
Release : 2009-06-17
Category : Science
ISBN : 9780470447789

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Crystallization of Organic Compounds by Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley Pdf

Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.

Crystallization Process Systems

Alan G. Jones
Crystallization Process Systems Book PDF

Author : Alan G. Jones
Publisher : Butterworth-Heinemann
Page : 362 pages
File Size : 40,6 Mb
Release : 2002-04-24
Category : Science
ISBN : 9780750655200

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Crystallization Process Systems by Alan G. Jones Pdf

Particulate Crystal Characteristics; Fluid-particle Transport Processes; Crystallization Principles and Techniques; Crystal Formation Processes; Crystallizer Design and Operation; Solid-Liquid Separation Processes; Design of Crystallization Process Systems.

Crystallization Technology Handbook

A. Mersmann
Crystallization Technology Handbook Book PDF

Author : A. Mersmann
Publisher : CRC Press
Page : 856 pages
File Size : 42,7 Mb
Release : 2001-05-08
Category : Science
ISBN : 0203908287

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Crystallization Technology Handbook by A. Mersmann Pdf

This handbook facilitates the selection, design and operation of large-scale industrial crystallizers that process crystals with the proper size distribution, shape and purity sought - including cooling, evaporation, drowning-out reaction, melt, and related crystallization techniques. This new edition offers new results on direct-contact cooling crystallization. It lists the properties of over 170 organic and inorganic crystallization systems.

Crystallization of Lipids

Kiyotaka Sato
Crystallization of Lipids Book PDF

Author : Kiyotaka Sato
Publisher : John Wiley & Sons
Page : 540 pages
File Size : 48,7 Mb
Release : 2018-04-23
Category : Technology & Engineering
ISBN : 9781118593929

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Crystallization of Lipids by Kiyotaka Sato Pdf

An authoritative reference that contains the most up-to-date information knowledge, approaches, and applications of lipid crystals Crystallization of Lipids is a comprehensive resource that offers the most current and emerging knowledge, techniques and applications of lipid crystals. With contributions from noted experts in the field, the text covers the basic research of polymorphic structures, molecular interactions, nucleation and crystal growth and crystal network formation of lipid crystals which comprise main functional materials employed in food, cosmetic and pharmaceutical industry. The authors highlight trans-fat alternative and saturated-fat reduction technology to lipid crystallization. These two issues are the most significant challenges in the edible-application technology of lipids, and a key solution is lipid crystallization. The text focuses on the crystallization processes of lipids under various external influences of thermal fluctuation, ultrasound irradiation, shear, emulsification and additives. Designed to be practical, the book’s information can be applied to realistic applications of lipids to foods, cosmetic and pharmaceuticals. This authoritative and up-to-date guide: Highlights cutting-edge research tools designed to help analyse lipid crystallization with the most current and the conventional techniques Offers a thorough review of the information, techniques and applications of lipid crystals Includes contributions from noted experts in the field of lipid crystals Presents cutting-edge information on the topics of trans-fat alterative and saturated-fat reduction technology Written for research and development technologists as well as academics, this important resource contains research on lipid crystals which comprise the main functional materials employed in food, cosmetic and pharmaceutical industry.

Industrial Crystallization

J. Mullin
Industrial Crystallization Book PDF

Author : J. Mullin
Publisher : Springer Science & Business Media
Page : 457 pages
File Size : 43,5 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781461572589

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Industrial Crystallization by J. Mullin Pdf

Industrial Crystallization Symposia have been organized by the Crystallization Research Group at the Czechoslovak Research Institute for Inorganic Chemistry, Usti nad Labem, since 1960. Over the years, the increasing popularity of the unit operation of crystallization has been clearly demonstrated by the steady increase in numbers of both the papers presented and the attendances at the meetings. The 6th Symposium (1-3 September 1975) was organized jointly with the European Federation of Chemical Engineering Working Party on Crystallization, and the 44 papers presented were arranged into four sessions - A: Secondary Nucleation, B: Crystal Growth Kinetics, C: Crystal Habit Modification, D: Crystallizer Design, E: Indus trial Crystallizer Operation and Case Studies. The same groupings are preserved in this edited version of the proceedings. This is the first time that the Industrial Crystallization Symposium papers have appeared in one volume. After the 5th (1972) Symposium, authors we.re encouraged to submit their papers to an international journal specializing in crystallization. However, the results were not altogether satisfactory in that less than one third of the papers presented at the meeting were offered for consideration. This time, therefore, the organizing committee decided to attempt to keep the papers together by making arrangements for their pUblication by Plenum Press.

Industrial Crystallization

Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen
Industrial Crystallization Book PDF

Author : Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen
Publisher : Cambridge University Press
Page : 353 pages
File Size : 50,6 Mb
Release : 2015-07-02
Category : Science
ISBN : 9781107052154

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Industrial Crystallization by Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen Pdf

A comprehensive overview of industrial crystallization, its theory and practice, including recent advances, real world case studies, and worked examples.

Formulation and Analytical Development for Low-Dose Oral Drug Products

Jack Zheng
Formulation and Analytical Development for Low Dose Oral Drug Products Book PDF

Author : Jack Zheng
Publisher : John Wiley & Sons
Page : 506 pages
File Size : 42,5 Mb
Release : 2009-02-09
Category : Medical
ISBN : 9780470056097

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Formulation and Analytical Development for Low-Dose Oral Drug Products by Jack Zheng Pdf

There are unique challenges in the formulation, manufacture, analytical chemistry, and regulatory requirements of low-dose drugs. This book provides an overview of this specialized field and combines formulation, analytical, and regulatory aspects of low-dose development into a single reference book. It describes analytical methodologies like dissolution testing, solid state NMR, Raman microscopy, and LC-MS and presents manufacturing techniques such as granulation, compaction, and compression. Complete with case studies and a discussion of regulatory requirements, this is a core reference for pharmaceutical scientists, regulators, and graduate students.

Industrial Crystallization

Narayan S. Tavare
Industrial Crystallization Book PDF

Author : Narayan S. Tavare
Publisher : Springer Science & Business Media
Page : 550 pages
File Size : 48,6 Mb
Release : 2013-11-11
Category : Science
ISBN : 9781489902337

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Industrial Crystallization by Narayan S. Tavare Pdf

Incorporating all recent developments and applications of crystallization technology, this volume offers a clear account of the field's underlying principles, reviews of past and current research, and provides guidelines for equipment and process design. The book takes a balanced functional approach in its critical survey of research literature, and includes several problems based on real practical situations that illustrate theoretical development. Several new concepts and techniques used in process simulation and identification analysis are featured.

Industrial Crystallization Process Monitoring and Control

Angelo Chianese,Herman J. Kramer
Industrial Crystallization Process Monitoring and Control Book PDF

Author : Angelo Chianese,Herman J. Kramer
Publisher : John Wiley & Sons
Page : 253 pages
File Size : 43,6 Mb
Release : 2012-04-06
Category : Science
ISBN : 9783527645176

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Industrial Crystallization Process Monitoring and Control by Angelo Chianese,Herman J. Kramer Pdf

Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.

14th International Symposium on Industrial Crystallization

Anonim
14th International Symposium on Industrial Crystallization Book PDF

Author : Anonim
Publisher : IChemE
Page : 2454 pages
File Size : 43,5 Mb
Release : 1999
Category : Chemical engineering
ISBN : 9780852954249

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14th International Symposium on Industrial Crystallization by Anonim Pdf

This conference provides a forum for discussion of the advances in the theory and practice of crystallization as it relates to the production of bulk crystalline materials.

Advances in Industrial Mixing

Suzanne M. Kresta,Arthur W. Etchells, III,David S. Dickey,Victor A. Atiemo-Obeng,North American Mixing Forum
Advances in Industrial Mixing Book PDF

Author : Suzanne M. Kresta,Arthur W. Etchells, III,David S. Dickey,Victor A. Atiemo-Obeng,North American Mixing Forum
Publisher : John Wiley & Sons
Page : 1040 pages
File Size : 40,7 Mb
Release : 2015-10-21
Category : Science
ISBN : 9781118944301

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Advances in Industrial Mixing by Suzanne M. Kresta,Arthur W. Etchells, III,David S. Dickey,Victor A. Atiemo-Obeng,North American Mixing Forum Pdf

Advances in Industrial Mixing is a companion volume and update to the Handbook of Industrial Mixing. The second volume fills in gaps for a number of industries that were not covered in the first edition. Significant changes in five of the fundamental areas are covered in entirely updated or new chapters. The original text is provided as a searchable pdf file on the accompanying USB. This book explains industrial mixers and mixing problems clearly and concisely. Gives practical insights by the top professionals in the field, combining industrial design standards with fundamental insight. Details applications in 14 key industries. Six of these are new since the first edition. Provides the professional with information he/she did not receive in school. Five completely rewritten chapters on mixing fundamentals where significant advances have happened since the first edition and seven concise update chapters which summarize critical technical information.