Multidimensional Hplc Of Polymers

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Multidimensional HPLC of Polymers

Harald Pasch,Bernd Trathnigg
Multidimensional HPLC of Polymers Book PDF

Author : Harald Pasch,Bernd Trathnigg
Publisher : Springer Science & Business Media
Page : 291 pages
File Size : 48,9 Mb
Release : 2013-06-12
Category : Technology & Engineering
ISBN : 9783642360800

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Multidimensional HPLC of Polymers by Harald Pasch,Bernd Trathnigg Pdf

This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers. It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.

HPLC of Polymers

Harald Pasch,Bernd Trathnigg
HPLC of Polymers Book PDF

Author : Harald Pasch,Bernd Trathnigg
Publisher : Springer Science & Business Media
Page : 234 pages
File Size : 42,6 Mb
Release : 2012-12-06
Category : Technology & Engineering
ISBN : 9783642582653

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HPLC of Polymers by Harald Pasch,Bernd Trathnigg Pdf

Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

Chromatographic Characterization of Polymers

Theodore Provder
Chromatographic Characterization of Polymers Book PDF

Author : Theodore Provder
Publisher : Unknown
Page : 322 pages
File Size : 47,8 Mb
Release : 1995
Category : Chromatographic analysis
ISBN : UVA:X002240259

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Chromatographic Characterization of Polymers by Theodore Provder Pdf

Presents an overview of the recent developments in the use of hyphenated multidimensional separation and detection techniques for the characterization of polymeric materials. Reports on successful multidimensional chromatographic methods and multiple detector systems. Includes an analysis of compositional heterogeneity in copolymers and blends.

Multidimensional Liquid Chromatography

Steven A. Cohen,Mark R. Schure
Multidimensional Liquid Chromatography Book PDF

Author : Steven A. Cohen,Mark R. Schure
Publisher : John Wiley & Sons
Page : 490 pages
File Size : 44,7 Mb
Release : 2008-05-09
Category : Science
ISBN : 9780470276259

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Multidimensional Liquid Chromatography by Steven A. Cohen,Mark R. Schure Pdf

Multidimensional Liquid Chromatography (MDLC) is a very powerful separation technique for analyzing exceptionally complex samples in one step. This authoritative reference presents a number of recent contributions that help define the current art and science of MDLC. Topics covered include instrumentation, theory, methods development, and applications of MDLC in the life sciences and in industrial chemistry. With the information to help you perform very difficult separations of complex samples, this reference includes chapters contributed by leading experts or teams of experts.

Chromatography of Polymers

Theodore Provder
Chromatography of Polymers Book PDF

Author : Theodore Provder
Publisher : Unknown
Page : 368 pages
File Size : 47,5 Mb
Release : 1999
Category : Science
ISBN : UOM:39015042094097

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Chromatography of Polymers by Theodore Provder Pdf

This book covers recent advances in characterizing polymers by chromatographic techniques and with other types of detectors. It also examines applications of these techniques to the analysis of oligomers and other polymeric techniques.

Liquid Chromatography of Synthetic Polymers

Muhammad Imran Malik,Dusan Berek
Liquid Chromatography of Synthetic Polymers Book PDF

Author : Muhammad Imran Malik,Dusan Berek
Publisher : Springer Nature
Page : 310 pages
File Size : 42,8 Mb
Release : 2023-11-03
Category : Technology & Engineering
ISBN : 9783031348358

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Liquid Chromatography of Synthetic Polymers by Muhammad Imran Malik,Dusan Berek Pdf

This book elucidates the peculiar phenomenon of entropy/enthalpy compensation that takes place in high performance liquid chromatography (HPLC) of polymers. Numerous publications, including some books, are devoted to molecular characterization of synthetic polymers, materials presently produced in large and steadily growing quantities, applying methods of HPLC. A knowledge of the molecular characteristics of polymers is indispensable, not only for their proper applications but also for their recycling and remediation. Polymer scientists generally focus on synthesis and potential applications of polymers while not giving due attention to an important central link, their comprehensive characterization in context of development of structure-property correlations. To fill this gap is one of the aims of the present book. The process of entropy/enthalpy compensation plays a decisive role in the advanced method of polymer characterization such as liquid chromatography at critical conditions, eluent gradient interaction chromatography, and temperature gradient interaction chromatography. All chemists working on any aspect of polymer science will find this book a valuable resource for the development of structure-property correlations.

Additives in Polymers

Jan C. J. Bart
Additives in Polymers Book PDF

Author : Jan C. J. Bart
Publisher : John Wiley & Sons
Page : 836 pages
File Size : 43,5 Mb
Release : 2005-04-08
Category : Technology & Engineering
ISBN : 9780470012055

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Additives in Polymers by Jan C. J. Bart Pdf

This industrially relevant resource covers all established and emerging analytical methods for the deformulation of polymeric materials, with emphasis on the non-polymeric components. Each technique is evaluated on its technical and industrial merits. Emphasis is on understanding (principles and characteristics) and industrial applicability. Extensively illustrated throughout with over 200 figures, 400 tables, and 3,000 references.

Handbook of HPLC

Danilo Corradini
Handbook of HPLC Book PDF

Author : Danilo Corradini
Publisher : CRC Press
Page : 715 pages
File Size : 45,8 Mb
Release : 2016-04-19
Category : Science
ISBN : 9781420016949

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Handbook of HPLC by Danilo Corradini Pdf

High performance liquid chromatography (HPLC) is one of the most widespread analytical and preparative scale separation techniques used for both scientific investigations and industrial and biomedical analysis. Now in its second edition, this revised and updated version of the Handbook of HPLC examines the new advances made in this field since the

Thermal Field-Flow Fractionation of Polymers

Guilaume Greyling,Harald Pasch
Thermal Field Flow Fractionation of Polymers Book PDF

Author : Guilaume Greyling,Harald Pasch
Publisher : Springer
Page : 116 pages
File Size : 41,9 Mb
Release : 2019-02-21
Category : Technology & Engineering
ISBN : 9783030106508

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Thermal Field-Flow Fractionation of Polymers by Guilaume Greyling,Harald Pasch Pdf

This book introduces the reader to thermal field-flow fractionation and discusses its advantages over the fundamental problems associated with traditional column-based analytical techniques commonly used to characterize polymers and macromolecules. The authors discuss the theoretical background, equipment, experimental procedures as well as the recent advances and applications of thermal field-flow fractionation. Complete with several practical examples and troubleshooting guidelines, the book is written for beginners and experienced separation scientists alike and will enable its readers to optimize their experimental conditions for their specific separation needs and problems.

Molecular Characterization of Polymers

Muhammad Imran Malik,Jimmy Mays,Muhammad Raza Shah
Molecular Characterization of Polymers Book PDF

Author : Muhammad Imran Malik,Jimmy Mays,Muhammad Raza Shah
Publisher : Elsevier
Page : 670 pages
File Size : 41,7 Mb
Release : 2021-03-09
Category : Technology & Engineering
ISBN : 9780128225981

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Molecular Characterization of Polymers by Muhammad Imran Malik,Jimmy Mays,Muhammad Raza Shah Pdf

Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material Establishes a strong link between basic principles, characterization techniques, and real-life applications

Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation

Gottfried Glöckner
Gradient HPLC of Copolymers and Chromatographic Cross Fractionation Book PDF

Author : Gottfried Glöckner
Publisher : Springer Science & Business Media
Page : 227 pages
File Size : 45,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642757990

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Gradient HPLC of Copolymers and Chromatographic Cross-Fractionation by Gottfried Glöckner Pdf

"The problems involved in separating complex macromolecules require under standing not only the chromatographic process but also the physicochemical behavior of the solutes." This sentence from the pen of Phyllis R. Brown 1, University of Rhode Island, can certainly be applied to synthetic copolymers whose structure is very complex indeed. Thus it may be forgiven that a book on copolymer HPLC has been written not by a trained chromatographer but by someone from the polymer side. The HPLC of synthetic polymers is often understood to mean only a synonym for size exclusion chromatography. The latter method separates polymers according to the size of the macromolecules and enables the molecular weight distribution of a sample to be evaluated. But as early as 1936, Mark and Saito attempted chromatographic fractionation of cellulose acetate on a charcoal-like adsorbent made from blood. HPLC adsorption chromatography was first applied to copolymer analysis by Teramachi et al. in 1979. Since then, another branch of polymer HPLC has arisen which has the capacity of separating copolymers by composition and enables the chemical composition distribution to be evaluated. The technique requires a suitable elution program and is mainly carried out as gradient elution.

Rubber Analysis

Martin J. Forrest
Rubber Analysis Book PDF

Author : Martin J. Forrest
Publisher : Walter de Gruyter GmbH & Co KG
Page : 358 pages
File Size : 51,6 Mb
Release : 2019-04-01
Category : Technology & Engineering
ISBN : 9783110640281

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Rubber Analysis by Martin J. Forrest Pdf

Rubber analysis plays a vital part in ensuring that manufactured products are fit for purpose. This comprehensive, application-based book with up-to-date referencing covers all important applications and subject area associated with the analysis of rubber compounds and rubber products. Includes characterization of rubber polymers, rubber fumes, identification of extractables and leachables, as well as reverse engineering on compounded products.

Applied Polymer Science

Ulf W. Gedde,Mikael S. Hedenqvist,Minna Hakkarainen,Fritjof Nilsson,Oisik Das
Applied Polymer Science Book PDF

Author : Ulf W. Gedde,Mikael S. Hedenqvist,Minna Hakkarainen,Fritjof Nilsson,Oisik Das
Publisher : Springer Nature
Page : 555 pages
File Size : 52,9 Mb
Release : 2021-10-29
Category : Science
ISBN : 9783030684723

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Applied Polymer Science by Ulf W. Gedde,Mikael S. Hedenqvist,Minna Hakkarainen,Fritjof Nilsson,Oisik Das Pdf

This companion volume to “Fundamental Polymer Science” (Gedde and Hedenqvist, 2019) offers detailed insights from leading practitioners into experimental methods, simulation and modelling, mechanical and transport properties, processing, and sustainability issues. Separate chapters are devoted to thermal analysis, microscopy, spectroscopy, scattering methods, and chromatography. Special problems and pitfalls related to the study of polymers are addressed. Careful editing for consistency and cross-referencing among the chapters, high-quality graphics, worked-out examples, and numerous references to the specialist literature make “Applied Polymer Science” an essential reference for advanced students and practicing chemists, physicists, and engineers who want to solve problems with the use of polymeric materials.

Advanced Separation Techniques for Polyolefins

Harald Pasch,Muhammad Imran Malik
Advanced Separation Techniques for Polyolefins Book PDF

Author : Harald Pasch,Muhammad Imran Malik
Publisher : Springer
Page : 179 pages
File Size : 47,7 Mb
Release : 2014-08-27
Category : Technology & Engineering
ISBN : 9783319086323

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Advanced Separation Techniques for Polyolefins by Harald Pasch,Muhammad Imran Malik Pdf

This Springer Laboratory volume introduces the reader to advanced techniques for the separation and fractionation of polyolefins. It includes detailed information on experimental protocols and procedures, addressing the experimental background of different polyolefin fractionation techniques in great detail. The book summarizes important applications in all major fractionation methods with emphasis on multidimensional analytical approaches. It comprises the most powerful modern techniques, such as high temperature size exclusion chromatography (HT-SEC) for molar mass analysis, temperature rising elution fractionation (TREF) and crystallization analysis fractionation (CRYSTAF) for the analysis of chemical composition and branching, high temperature two-dimensional liquid chromatography (HT-2D-LC), solvent and temperature gradient interaction chromatography (SGIC and TGIC) and crystallization elution fractionation (CEF). Beginners as well as experienced chromatographers will benefit from this concise introduction to a great variety in instrumentation, separation procedures and applications. With detailed descriptions of experimental approaches for the analysis of complex polyolefins, the readers are offered a toolbox to solve simple as well as sophisticated separation tasks. The book starts with an introduction into the molecular complexity of polyolefins - the most widely used synthetic polymers with rapidly growing production capacities. It systematically discusses crystallization based fractionation techniques including TREF, CRYSTAF and CEF and column chromatographic techniques for molar mass, chemical composition and microstructure, as well as the combination of different fractionations in multidimensional experimental setups. This book also includes basic information on the application of high-temperature field-flow fractionation.

Multidimensional Spectroscopy of Polymers

Marek W. Urban
Multidimensional Spectroscopy of Polymers Book PDF

Author : Marek W. Urban
Publisher : Wiley-VCH
Page : 624 pages
File Size : 52,7 Mb
Release : 1995-08-31
Category : Science
ISBN : UOM:39015034891815

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Multidimensional Spectroscopy of Polymers by Marek W. Urban Pdf

Focuses on advances in three areas of multidimensional spectroscopy: NMR, vibrational, and fluorescence. Discusses important areas in polymer analysis, including diffusion, free volume, adhesion, absorption, polymer interactions, and miscibility. Includes introductory chapters as well as chapters covering both theory and application. Valuable material for researchers in polymer science and in analytical laboratories specializing in NMR, FT-IR and fluorescence spectroscopy.