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Spectrometric Identification of Organic Compounds by Robert Milton Silverstein,Francis X. Webster,David J. Kiemle Pdf
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Guide to Spectroscopic Identification of Organic Compounds by Karen Feinstein Pdf
Guide to Spectroscopic Identification of Organic Compounds is a practical "how-to" book with a general problem-solving algorithm for determining the structure of a molecule from complementary spectra or spectral data obtained from MS, IR, NMR, or UV spectrophotometers. Representative compounds are analyzed and examples are solved. Solutions are eclectic, ranging from simple and straightforward to complex. A picture of the relationship of structure to physical properties, as well as to spectral features, is provided. Compounds and their derivatives, structural isomers, straight-chain molecules, and aromatics illustrate predominant features exhibited by different functional groups. Practice problems are also included. Guide to Spectroscopic Identification of Organic Compounds is a helpful and convenient tool for the analyst in interpreting organic spectra. It may serve as a companion to any organic textbook or as a spectroscopy reference; its size allows practitioners to carry it along when other tools might be cumbersome or expensive.
Robert M. Silverstein,Francis X. Webster,David J. Kiemle,David L. Bryce
Author : Robert M. Silverstein,Francis X. Webster,David J. Kiemle,David L. Bryce Publisher : John Wiley & Sons Page : 467 pages File Size : 54,7 Mb Release : 2014-09-29 Category : Science ISBN : 9780470616376
Spectrometric Identification of Organic Compounds by Robert M. Silverstein,Francis X. Webster,David J. Kiemle,David L. Bryce Pdf
First published over 40 years ago, this was the first text on the identification of organic compounds using spectroscopy. This text is now considered to be a classic. This text presents a unified approach to the structure determination of organic compounds based largely on mass spectrometry, infrared (IR) spectroscopy, and multinuclear and multidimensional nuclear magnetic resonance (NMR) spectroscopy. The key strength of this text is the extensive set of practice and real-data problems (in Chapters 7 and 8). Even professional chemists use these spectra as reference data. Spectrometric Identification of Organic Compounds is written by and for organic chemists, and emphasizes the synergistic effect resulting from the interplay of the spectra. This book is characterized by its problem-solving approach with extensive reference charts and tables. The 8th edition of this text maintains its student-friendly writing style - wording throughout has been updated for consistency and to be more reflective of modern usage and methods. Chapter 3 on proton NMR spectroscopy has been overhauled and updated. Also, new information on polymers and phosphorus functional groups has been added to Chapter 2 on IR spectroscopy.
Spectroscopic Identification Of Organic Molecules by Elnagdi Mohamed Hilmy,Sadek Kamal Usef,Mekheimer Ramadan Ahmed H Pdf
Researchers in the fields of organic synthesis, pharmaceutical research as well as cosmetic and agrochemicals industries need to confirm the structures of products they obtain. This was previously a time-consuming a process that took up much time. Spectroscopic methods however, made it easier, and initially R and UV helped chemists conclude structures one way or another. Initially 1D NMR, 2D NMR and sophisticated NMR measurements like COESY and NOESY were of great assistance. We demonstrate principles to conclude structures of our simple molecules, mainly heterocycles of interest for researchers in fields indicated above.However, it is insufficient to only understand the principles, and one should also master problem solving and thinking. We demonstrate simple problems like the utility of coupling constants, NOE, COESY and NOESY and show how firm conclusions are obtained in real life. Most NMR books usually demonstrate these principles utilizing a pit sophisticated examples. The methodology suggested by us is simpler and quite useful for researchers in heterocyclic chemistry where combination of proton and carbon NMR should be dealt together.Our research results previously been used intensively (Cf. citations in Google Scholar) and still draw attention. Students in the fields indicated will find this book of value to sign the spectra of the molecules they synthesize. Researchers in the field of heterocyclic chemistry as well as instructors in the field of structure proof utilizing spectroscopic identification will also find this book of interest.
SPECTROMETRIC IDENTIFICATION OF ORGANIC COMPOUNDS, 6TH ED by Robert Silverstein & Francis Webster Pdf
Market_Desc: Organic and Analytical in the Forensics, Chemical and Pharmaceutical Industries Special Features: · A how-to, hands-on teaching manual· Considerably expanded NMR coverage--NMR spectra can now be interpreted in exquisite detail· New chapters on correlation NMR spectrometry (2-D NMR) and spectrometry of other important nuclei· Uses a problem-solving approach with extensive reference charts and tables· An extensive set of real-data problems offers a challenge to the practicing chemist About The Book: The book provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry.
Spectrometric Identification of Organic Compounds by Robert M. Silverstein,G. Clayton Bassler,Terence C. Morrill Pdf
Teaches the use of the complementary information afforded by four types of spectrometry for identification of organic compounds: mass, infrared, nuclear magnetic resonance, and ultra violet spectrometry. Throughout, the emphasis is on the relationship between chemical structure and spectral response of the molecule. Each chapter includes problems to facilitate student comprehension and demonstrate practical aspects of the material. Also provided are extensive reference material in charts and tables at the end of each chapter, solved problems, and 50 sets of Spectra of Compounds to be identified. In addition to extensive updating, the Fifth Edition includes a new chapter on New Dimensions in NMR Spectrometry.
Tables of Spectral Data for Structure Determination of Organic Compounds by Ernö Pretsch,T. Clerc,J. Seibl,W. Simon Pdf
Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.
Rosaleen J. Anderson,David J. Bendell,Paul W. Groundwater
Author : Rosaleen J. Anderson,David J. Bendell,Paul W. Groundwater Publisher : Royal Society of Chemistry Page : 190 pages File Size : 42,9 Mb Release : 2004 Category : Education ISBN : 0854044760
Organic Spectroscopic Analysis by Rosaleen J. Anderson,David J. Bendell,Paul W. Groundwater Pdf
A unique textbook, aimed at undergraduate students, containing large numbers of spectra, problems and marginal notes, specifically chosen to highlight the points being discussed.
An Introduction to Spectroscopic Methods for the Identification of Organic Compounds by F. Scheinmann Pdf
An Introduction to Spectroscopic Methods for the Identification of Organic Compounds, Volume 2 covers the theoretical aspects and some applications of certain spectroscopic methods for organic compound identification. This book is composed of 10 chapters, and begins with an introduction to the structure determination from mass spectra. The subsequent chapter presents some mass spectrometry seminar problems and answers. This presentation is followed by discussions on the problems concerning the application of UV spectroscopy and electron spin resonance spectroscopy. Other chapters deal with some advances and development in NMR spectroscopy and the elucidation of structural formula of organic compounds by a combination of spectral methods. The final chapter surveys seminar problems and answers in the identification of organic compounds using NMR, IR, UV and mass spectroscopy. This book will prove useful to organic and analytical chemists.
Structural Identification of Organic Compounds with Spectroscopic Techniques by Yong-Cheng Ning Pdf
Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.
Interpretation of Organic Spectra by Yong-Cheng Ning Pdf
Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation.
Spectroscopic Techniques for Organic Chemists by James W. Cooper Pdf
"Spectroscopy has become the organic chemist's most important tool in identifying compounds and studying their interactions. The arsenal of techniques available to the research chemist has, over the years, expanded from the familiar infrared, proton nmr and mass spectroscopy, to include the routine use of carbon-13 nmr spectroscopy and such modern methods of data acquisition as Fourier transform nmr, laser Raman spectroscopy, and UV spectroscopy. This book serves as an introduction to all of the major spectroscopic techniques, using over 200 actual spectra as examples, and providing a substantial number of problems and completely worked-through solutions that demonstrate how spectral techniques are applied to analytical problems. The book represents a significant departure from the scope of general spectroscopy texts. In addition to the usual chapters on infrared, proton nmr and mass spectroscopy, a number of increasingly important techniques have been included for the first time. Chapter 4, for instance, introduces not only the analysis of proton nmr spectra, but also describes iteration of theoretical nmr spectra for a best fit with observed experimental spectra using the popular LAOCOON III program. A complete FORTRAN listing for a conversational pendix I. Chapter 5 presents a non-mathematical description of Fourier transform nmr, including signal averaging, decoupling methods, quadrature detection, and the Fourier transform itself, and Chapter 6 goes on to describe Fourier transform techniques in carbon-13 spectroscopy. Chapter 7 introduces simple Huckel M.O. theory and the SHMO program for calculating the resonance stabilization of various systems, material which lays the groundwork for Chapter 8's discussion of ultraviolet spectroscopy using examples of ways in which energies can be correlated with SHMO parameters. A SHMO timesharing conversational program is listed in Appendix II. Finally, Chapter 10 outlines the organic chemical applications of laser Raman spectroscopy and the functional groups most easily identified using this method. Both organic chemists and graduate and advanced undergraduate students will find in the book's breadth of coverage an ideal introduction to the identification of organic compounds by spectroscopic means."- Publisher.
