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This book provides an in-depth introduction to the sol to gel transition in inorganic and hybrid organic-inorganic systems, one of the most important chemical-physical transitions and the basis of the sol-gel process. Familiarity with the fundamental chemistry and physics of this transition is essential for students in chemistry and materials science through academic and industry researchers working on sol-gel-related applications. The book features a didactic approach, using simple and clear language to explain the sol to gel transition and the accompanying processes. The text is also suitable for use in short courses and workshops for graduate students as well as professionals.
This book provides an in-depth introduction to the sol to gel transition in inorganic and hybrid organic-inorganic systems, one of the most important chemical-physical transitions and the basis of the sol-gel process. Familiarity with the fundamental chemistry and physics of this transition is essential for students in chemistry and materials science through academic and industry researchers working on sol-gel-related applications. The book features a didactic approach, using simple and clear language to explain the sol to gel transition and the accompanying processes. The text is also suitable for use in short courses and workshops for graduate students as well as professionals.This fully revised and updated new edition contains a wealth of new content. In particular, it includes a detailed discussion of the chemistry of transition metal alkoxides and organosilanes, and an extended discussion of the sol to gel transition models.
Explains the correlation between the physical properties and structure of polymer gels This book elucidates in detail the physics of polymer gels and reviews their unique properties that make them attractive for innumerable applications. Geared towards experienced researchers and entrants to the field, it covers rubber elasticity, swelling and shrinking, deformation and fracture of as well as mass transport in polymer gels, enabling the readers to purposefully design polymer gels fit for specific purposes. Divided into two parts, Physics of Polymer Gels starts by explaining the statistical mechanics and scaling of a polymer chains, and that of polymer solutions. It then introduces the structure of polymer gels and explains the rubber elasticity, which predicts the solid-like nature of polymer gels. Next, it describes swelling/deswelling, which can be understood by combining the rubber elasticity and the osmotic pressure of a polymer solution. Large deformation and fracture, and the diffusion of substances in polymer gels, which are essential for practical applications, are also introduced. The last half of the book contains the authors' experimental results using Tetra-PEG gels and provides readers with the opportunity to examine and compare it with the first half in order to understand how to utilize the models to experiments. This title: * Is the first book dedicated to the physics of polymer gels * Describes in detail the properties of polymer gels and their underlying physics, facilitating the development of novel, polymer gel-based applications * Serves as a reference for all relevant polymer gel properties and their underlying physics * Provides a unified treatment of the subject, explaining the physical properties of polymer gels within a common nomenclature framework Physics of Polymer Gels is a must-have book for experienced researchers, such as polymer chemists, materials scientists, organic chemists, physical chemists, and solid-state physicists, as well as for newcomers to the field.
Physical Gels from Biological and Synthetic Polymers by Madeleine Djabourov,Katsuyoshi Nishinari,Simon B. Ross-Murphy Pdf
Presenting a unique perspective on state-of-the-art physical gels, this interdisciplinary guide provides a complete, critical analysis of the field and highlights recent developments. It shows the interconnections between the key aspects of gels, from molecules and structure through to rheological and functional properties, with each chapter focusing on a different class of gel. There is also a final chapter covering innovative systems and applications, providing the information needed to understand current and future practical applications of gels in the pharmaceutical, agricultural, cosmetic, chemical and food industries. Many research teams are involved in the field of gels, including theoreticians, experimentalists and chemical engineers, but this interdisciplinary book collates and rationalises the many different points of view to provide a clear understanding of these complex systems for researchers and graduate students.
Synthesis of Inorganic Materials by Ulrich S. Schubert,Nicola Hüsing Pdf
Introduces readers to the field of inorganic materials, while emphasizing synthesis and modification techniques Written from the chemist's point of view, this newly updated and completely revised fourth edition of Synthesis of Inorganic Materials provides a thorough and pedagogical introduction to the exciting and fast developing field of inorganic materials and features all of the latest developments. New to this edition is a chapter on self-assembly and self-organization, as well as all-new content on: demixing of glasses, non-classical crystallization, precursor chemistry, citrate-gel and Pechini liquid mix methods, ice-templating, and materials with hierarchical porosity. Synthesis of Inorganic Materials, 4th Edition features chapters covering: solid-state reactions; formation of solids from the gas phase; formation of solids from solutions and melts; preparation and modification of inorganic polymers; self-assembly and self-organization; templated materials; and nanostructured materials. There is also an extensive glossary to help bridge the gap between chemistry, solid state physics and materials science. In addition, a selection of books and review articles is provided at the end of each chapter as a starting point for more in-depth reading. -Gives the students a thorough overview of the fundamentals and the wide variety of different inorganic materials with applications in research as well as in industry -Every chapter is updated with new content -Includes a completely new chapter covering self-assembly and self-organization -Written by well-known and experienced authors who follow an intuitive and pedagogical approach Synthesis of Inorganic Materials, 4th Edition is a valuable resource for advanced undergraduate students as well as masters and graduate students of inorganic chemistry and materials science.
Sol-Gel Science by C. Jeffrey Brinker,George W. Scherer Pdf
Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing presents the physical and chemical principles of the sol-gel process. The book emphasizes the science behind sol-gel processing with a chapter devoted to applications. The first chapter introduces basic terminology, provides a brief historical sketch, and identifies some excellent texts for background reading. Chapters 2 and 3 discuss the mechanisms of hydrolysis and condensation for nonsilicate and silicate systems. Chapter 4 deals with stabilization and gelation of sols. Chapter 5 reviews theories of gelation and examines the predicted and observed changes in the properties of a sol in the vicinity of the gel point. Chapter 6 describes the changes in structure and properties that occur during aging of a gel in its pore liquor (or some other liquid). The discussion of drying is divided into two parts, with the theory concentrated in Chapter 7 and the phenomenology in Chapter 8. The structure of dried gels is explored in Chapter 9. Chapter 10 shows the possibility of using the gel as a substrate for chemical reactions or of modifying the bulk composition of the resulting ceramic by performing a surface reaction (such as nitridation) on the gel. Chapter 11 reviews the theory and practice of sintering, describing the mechanisms that govern densification of amorphous and crystalline materials, and showing the advantages of avoiding crystallization before sintering is complete. The properties of gel-derived and conventional ceramics are discussed in Chapter 12. The preparation of films is such an important aspect of sol-gel technology that the fundamentals of film formation are treated at length in Chapter 13. Films and other applications are briefly reviewed in Chapter 14. Materials scientists and researchers in the field of sol-gel processing will find the book invaluable.
Sol-Gel Materials by John D. Wright,Nico A.J.M. Sommerdijk Pdf
Sol-Gel processing methods, first used historically for decorative and constructional materials, were extensively developed in the last century for applications such as glasses, ceramics, catalysts, coatings, composites and fibres. Today they are reaching their full potential, enabling the preparation of new generations of advanced materials not easily accessible by other methods yet using mild, low-energy conditions. The topic is therefore increasingly included in advanced undergraduate, MSc and PhD programmes in the areas of chemistry, physics and materials science. This concise introductory text, written at the advanced undergraduate/first-year postgraduate level, is also suitable as an introduction to the development, mechanisms, chemistry, characterisation methods and applications of the technique. It provides readers with an extensive yet concise grounding in the theory of each area of the subject and details the real and potential applications and the future prospects of sol-gel chemistry.
Introduction to Sol-Gel Processing by Alain C. Pierre Pdf
This book presents a broad, general introduction to the processing of Sol-Gel technologies. This updated volume serves as a general handbook for researchers and students entering the field. This new edition provides updates in fields that have undergone rapid developments, such as Ceramics, Catalysis, Chromatropgraphy, biomaterials, glass science, and optics. It provides a simple, compact resource that can also be used in graduate-level materials science courses.
The Sol-Gel Handbook by David Levy,Marcos Zayat Pdf
This comprehensive three-volume handbook brings together a review of the current state together with the latest developments in sol-gel technology to put forward new ideas. The first volume, dedicated to synthesis and shaping, gives an in-depth overview of the wet-chemical processes that constitute the core of the sol-gel method and presents the various pathways for the successful synthesis of inorganic and hybrid organic-inorganic materials, bio- and bio-inspired materials, powders, particles and fibers as well as sol-gel derived thin films, coatings and surfaces. The second volume deals with the mechanical, optical, electrical and magnetic properties of sol-gel derived materials and the methods for their characterization such as diffraction methods and nuclear magnetic resonance, infrared and Raman spectroscopies. The third volume concentrates on the various applications in the fields of membrane science, catalysis, energy research, biomaterials science, biomedicine, photonics and electronics.
Physical Chemistry and Industrial Application of Gellan Gum by K. Nishinari Pdf
Gellan gum, a microbial polysaccharide, consisting of tetra-saccharide unit, glucose, glucuronic acid, glucose and rhamnose, forms a transparent gel which is heat-resistant in the presence of divalent cations. Since 1989, the collaborative research group was organised in the Research Group of Polymer Gels affiliated to the Society of Polymer Science, Japan, consisting of various laboratories with different disciplines to clarify the mechanism using the common purified sample. This special issue contains 19 papers on the molecular conformation, gel-sol transition, interaction of gellan and water, cations and sugar, based on rheology, NMR, ESR, DSC, light scattering, osmotic pressure, small angle x-ray scattering, dielectric measurement, atomic force microscopy and the industrial application of gellan gum presented at the 4th International Conference on Hydrocolloids - OCUIS '98 by the collaborative group members and by international experts.
Metal Oxide Nanoparticles in Organic Solvents by Markus Niederberger,Nicola Pinna Pdf
Metal Oxide Nanoparticles in Organic Solvents discusses recent advances in the chemistry involved for the controlled synthesis and assembly of metal oxide nanoparticles, the characterizations required by such nanoobjects, and their size and shape depending properties. In the last few years, a valuable alternative to the well-known aqueous sol-gel processes was developed in the form of nonaqueous solution routes. Metal Oxide Nanoparticles in Organic Solvents reviews and compares surfactant- and solvent-controlled routes, as well as providing an overview of techniques for the characterization of metal oxide nanoparticles, crystallization pathways, the physical properties of metal oxide nanoparticles, their applications in diverse fields of technology, and their assembly into larger nano- and mesostructures. Researchers and postgraduates in the fields of nanomaterials and sol-gel chemistry will appreciate this book’s informative approach to chemical formation mechanisms in relation to metal oxides.
Sol-Gel Technologies for Glass Producers and Users by Michel Andre Aegerter,M. Mennig Pdf
Sol-Gel Techniques for Glass Producers and Users provides technological information, descriptions and characterizations of prototypes, or products already on the market, and illustrates advantages and disadvantages of the sol-gel process in comparison to other methods. The first chapter entitled "Wet Chemical Technology" gives a summary of the basic principles of the sol-gel chemistry. The most promising applications are related to coatings. Chapter 2 describes the various "Wet Chemical Coating Technologies" from glass cleaning to many deposition and post-coating treatment techniques. These include patterning of coatings through direct or indirect techniques which have became very important and for which the sol-gel processing is particularly well adapted. Chapter 3 entitled "Bulk Glass Technologies" reports on the preparation of special glasses for different applications. Chapter 4 entitled "Coatings and Materials Properties" describes the properties of the different coatings and the sol-gel materials, fibers and powders. The chapter also includes a section dedicated to the characterization techniques especially applied to sol-gel coatings and products.
Sol--Gel--Optics encompasses numerous schemes for fabricating optical materials from gels -- materials such as bulk optics, optical waveguides, doped oxides for laser and nonlinear optics, gradient refractive index (GRIN) optics, chemical sensors, environmental sensors, and `smart' windows. Sol--Gel--Optics: Processing and Applications provides in-depth coverage of the synthesis and fabrication of these materials and discusses the optics related to microporous, amorphous, crystalline and composite materials. The reader will also find in this book detailed descriptions of new developments in silica optics, bulk optics, waveguides and thin films. Various applications to sensor and device technology are highlighted. For researchers and students looking for novel optical materials, processing methods or device ideas, Sol--Gel--Optics: Processing and Applications surveys a wide array of promising new avenues for further investigation and for innovative applications. (This book is the first in a new subseries entitled `Electronic Materials: Science and Technology).
Gels: Structures, Properties, and Functions by Masayuki Tokita Pdf
This volume includes 28 contributions to the Toyoichi Tanaka Memorial Symposium on Gels which took place at Arcadia Ichigaya on September 10th-12th, 2008. The contributions from leading scientists cover a broad spectrum of topics concerning: Structure and Functional Properties of Gels - Swelling of Gels - Industrial and Biomedical Application. The symposium was held in the style of Faraday Discussions, which stimulated the active discussion. After the symposium, each manuscript was rewritten based on the discussion and the critical review. Since the research on gels is becoming more and more important both for academia and industry, this book will be an essential source of information.
Author : Robert Corriu,Nguyen Trong Anh Publisher : John Wiley & Sons Page : 200 pages File Size : 47,8 Mb Release : 2009-02-18 Category : Science ISBN : 0470742801
Molecular Chemistry of Sol-Gel Derived Nanomaterials by Robert Corriu,Nguyen Trong Anh Pdf
Presenting the wide range of synthetic possibilities opened by sol-gel processes in the field of organic-inorganic materials, Molecular Chemistry of Sol-Gel Derived Nanomaterials discusses the state of the art in the synthesis of the various nanomaterials. The text includes examples of applications, including photoluminescent nanocomposites, grafted nanomaterials for selective separations of ions or isotopes, for cascade syntheses, chelation of transition metals and lanthanides by lamellar structured nanomaterials, and immobilized enzymes on mesoporous nanomaterials. This indispensable text for graduate students, engineers, and scientists concludes with a look toward future developments.