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Analytical Pyrolysis of Natural Organic Polymers

S.C. Moldoveanu

Author : S.C. Moldoveanu
Publisher : Elsevier
Page : 640 pages
File Size : 52,6 Mb
Release : 2020-09-12
Category : Science
ISBN : 9780128235539

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Analytical Pyrolysis of Natural Organic Polymers by S.C. Moldoveanu Pdf

Analytical Pyrolysis of Natural Organic Polymers, Second Edition, Volume 20 describes the methodology of analytical pyrolysis, the results of pyrolysis for a variety of biopolymers, and several practical applications of analytical pyrolysis on natural organic polymers and their composite materials. The book describes the results of pyrolysis for biopolymers and some chemically modified natural organic polymers. In addition, the many applications of analytical pyrolysis are covered in detail, including topics such as polymer detection used in forensic science, structure elucidation of specific polymers, and identification of small molecules present in polymers (anti-oxidants, plasticizers, etc.). Assembles all essential information on the pyrolysis of natural polymers in one volume, together with the techniques and instrumentation used Covers advances and developments over the last 20 years, including discussions on the many different types of apparatus commercially available Includes reference lists in every chapter to guide readers on a path to further study

Analytical Pyrolysis of Synthetic Organic Polymers

Serban C. Moldoveanu

Author : Serban C. Moldoveanu
Publisher : Elsevier
Page : 714 pages
File Size : 45,5 Mb
Release : 2005-01-20
Category : Science
ISBN : 9780080455860

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Analytical Pyrolysis of Synthetic Organic Polymers by Serban C. Moldoveanu Pdf

Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers. The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed. * Includes broad coverage of organic synthetic macromolecules * Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers * Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers

Analytical Pyrolysis of Synthetic Organic Polymers

Serban C. Moldoveanu

Author : Serban C. Moldoveanu
Publisher : Elsevier Science
Page : 714 pages
File Size : 55,5 Mb
Release : 2005-03-17
Category : Science
ISBN : 0444512926

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Analytical Pyrolysis of Synthetic Organic Polymers by Serban C. Moldoveanu Pdf

Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers. The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed. * Includes broad coverage of organic synthetic macromolecules * Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers * Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers

Analytical Pyrolysis of Natural Organic Polymers

S.C. Moldoveanu

Author : S.C. Moldoveanu
Publisher : Elsevier
Page : 510 pages
File Size : 41,5 Mb
Release : 1998-11-11
Category : Science
ISBN : 0080527167

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Analytical Pyrolysis of Natural Organic Polymers by S.C. Moldoveanu Pdf

Analytical pyrolysis is one of the many tools utilized for the study of natural organic polymers. This books describes in three parts the methodology of analytical pyrolysis, the results of pyrolysis for a variety of biopolymers, and several practical applications of analytical pyrolysis on natural organic polymers and their composite materials. Analytical pyrolysis methodology covers two distinct subjects, the instrumentation used for pyrolysis and the analytical methods that are applied for the analysis of the pyrolysis products. A variety of pyrolytic techniques and of analytical instruments commonly coupled with pyrolysis devices are given. The description of the results of pyrolysis for biopolymers and some chemically modified natural organic polymers is the core of the book. The main pyrolysis products of numerous compounds as well as the proposed mechanisms for their pyrolysis are described. In this part an attempt is made to present as much as possible the chemistry of the pyrolytic process of natural organic polymers. The applications of analytical pyrolysis include topics such as polymer detection used for example in forensic science, structure elucidation of specific polymers, and identification of small molecules present in polymers (anti-oxidants, plasticizers, etc.). Also, the degradation during heating is a subject of major interest in many practical applications regarding the physical properties of polymers. The applications to composite polymeric materials are in the fields of classification of microorganisms, study of a variety of biological samples, study of fossil materials, etc. Analytical pyrolysis can also be used for obtaining information on the burning area generate pyrolysates that have complex compositions. Their analysis is important in connection with health issues, environmental problems, and taste of food and cigarettes. Features of this book: • Presents analytical pyrolysis as a uniform subject and not as a conglomerate of scientific papers. • Puts together in an organized manner a large volume of available information in this specific field. • Provides original results which address subjects with relatively scarce information in literature. • Gives original views on subjects such as the parallel between the pyrolytic process and the ion fragmentation in mass spectrometry. • Includes the role of pyrolysis in the burning process. The three parts of the book are covered in 18 chapters, each divided into sections. Some sections are further divided by particular subjects. References are given for each chapter, and an effort has been made to include as much as possible from the available representative information. A few unpublished personal results are also included.

Analytical Pyrolysis

Peter Kusch

Author : Peter Kusch
Publisher : BoD – Books on Demand
Page : 104 pages
File Size : 52,7 Mb
Release : 2019-02-13
Category : Science
ISBN : 9781789849585

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Analytical Pyrolysis by Peter Kusch Pdf

Analytical pyrolysis deals with the structural identification and quantitation of pyrolysis products with the ultimate aim of establishing the identity of the original material and the mechanisms of its thermal decomposition. The pyrolytic process is carried out in a pyrolyzer interfaced with analytical instrumentation such as gas chromatography (GC), mass spectrometry (MS), gas chromatography coupled with mass spectrometry (GC/MS), or with Fourier-transform infrared spectroscopy (GC/FTIR). By measurement and identification of pyrolysis products, the molecular composition of the original sample can often be reconstructed.This book is the outcome of contributions by experts in the field of pyrolysis and includes applications of the analytical pyrolysis-GC/MS to characterize the structure of synthetic organic polymers and lignocellulosic materials as well as cellulosic pulps and isolated lignins, solid wood, waste particle board, and bio-oil. The thermal degradation of cellulose and biomass is examined by scanning electron micrography, FTIR spectroscopy, thermogravimetry (TG), differential thermal analysis, and TG/MS. The calorimetric determination of high heating values of different raw biomass, plastic waste, and biomass/plastic waste mixtures and their by-products resulting from pyrolysis is described.

Analytical Pyrolysis

Peter Kusch

Author : Peter Kusch
Publisher : Unknown
Page : 102 pages
File Size : 44,7 Mb
Release : 2019
Category : Chemistry, Analytic
ISBN : 1789849594

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Analytical Pyrolysis by Peter Kusch Pdf

Analytical pyrolysis deals with the structural identification and quantitation of pyrolysis products with the ultimate aim of establishing the identity of the original material and the mechanisms of its thermal decomposition. The pyrolytic process is carried out in a pyrolyzer interfaced with analytical instrumentation such as gas chromatography (GC), mass spectrometry (MS), gas chromatography coupled with mass spectrometry (GC/MS), or with Fourier-transform infrared spectroscopy (GC/FTIR). By measurement and identification of pyrolysis products, the molecular composition of the original sample can often be reconstructed.This book is the outcome of contributions by experts in the field of pyrolysis and includes applications of the analytical pyrolysis-GC/MS to characterize the structure of synthetic organic polymers and lignocellulosic materials as well as cellulosic pulps and isolated lignins, solid wood, waste particle board, and bio-oil. The thermal degradation of cellulose and biomass is examined by scanning electron micrography, FTIR spectroscopy, thermogravimetry (TG), differential thermal analysis, and TG/MS. The calorimetric determination of high heating values of different raw biomass, plastic waste, and biomass/plastic waste mixtures and their by-products resulting from pyrolysis is described.

Analytical Pyrolysis Handbook

Karen D. Sam,Thomas P. Wampler

Author : Karen D. Sam,Thomas P. Wampler
Publisher : CRC Press
Page : 354 pages
File Size : 53,7 Mb
Release : 2021-03-23
Category : Science
ISBN : 9780429574924

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Analytical Pyrolysis Handbook by Karen D. Sam,Thomas P. Wampler Pdf

Analytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Analytical Pyrolysis Handbook, Third Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a diversity of fields including microbiology, forensic science, industrial research, and environmental analysis. The much-anticipated third edition incorporates recent technological advances that increase the technique’s sensitivity to trace elements, improve its reproducibility, and expand its applicability. The book reviews the types of instrumentation available to perform pyrolysis and offers guidance for interfacing instruments and integrating other analytical techniques, including gas chromatography and mass spectrometry. Fully updated with new sample pyrograms, figures, references, and real-world examples, this edition also highlights new areas of application including cultural materials, forensic analysis, and environmental studies. This book illustrates how the latest advances make pyrolysis a practical, cost-effective, reliable, and flexible alternative for increasingly complex sample analyses. Analytical Pyrolysis Handbook, Third Edition is an essential, one-stop guide for determining if pyrolysis meets application-specific needs as well as performing pyrolysis and handling the data obtained.

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition)

Peter Kusch

Author : Peter Kusch
Publisher : World Scientific
Page : 383 pages
File Size : 54,9 Mb
Release : 2023-08-28
Category : Science
ISBN : 9781800613003

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Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by Peter Kusch Pdf

Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.

Analytical Pyrolysis

Kent J Voorhees

Author : Kent J Voorhees
Publisher : Butterworth-Heinemann
Page : 496 pages
File Size : 40,6 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483192284

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Analytical Pyrolysis by Kent J Voorhees Pdf

Analytical Pyrolysis: Techniques and Applications provides an overview of analytical pyrolysis applied to geochemistry, biology, polymers, and biomass. This book presents a survey of basic phenomena, data analysis, and instrumentation. Organized into 15 chapters, this book begins with an overview of mass spectrometry in developing ion sources that are applicable to materials that either have low volatility, high molecular weight, are thermally unstable or some combination of the three. This text then examines the role of thermal processes in many of the desorption methods. Other chapters consider desorption techniques, which are closely allied to analytical pyrolysis. This book discusses as well the Flash Vacuum Pyrolysis/Field Ionization Mass Spectrometry (FVP/FIMS) technique, which is based on a direct link between the pyrolysis unit and a double focusing mass spectrometer. The final chapter deals with inert atmosphere poly (vinyl chloride) (PVC) thermal decomposition. This book is a valuable resource for chemists and researchers.

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials

Peter Kusch

Author : Peter Kusch
Publisher : World Scientific
Page : 268 pages
File Size : 40,6 Mb
Release : 2018-10-08
Category : Science
ISBN : 9781786345776

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Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by Peter Kusch Pdf

The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.

Pyrolysis of Organic Molecules

Serban C. Moldoveanu

Author : Serban C. Moldoveanu
Publisher : Elsevier
Page : 744 pages
File Size : 42,8 Mb
Release : 2009-09-16
Category : Science
ISBN : 0080932150

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Pyrolysis of Organic Molecules by Serban C. Moldoveanu Pdf

Pyrolysis of Organic Molecules with Applications to Health and Environmental Issues, the 28th volume in the Techniques and Instrumentation in Analytical Chemistry series, gives a systematic and comprehensive description of pyrolysis of non-polymeric organic molecules. Pyrolysis is involved in many practical applications as well as in many common human activities, but harmful compounds can be generated in the process. The study of pyrolysis and of the formation of undesirable compounds as a result of pyrolytic processes is of considerable interest to chemists, chemical engineers, and toxicologists. Pyrolysis results for compounds not previously studied or reported Updated information from a large body of results published on pyrolysis of individual compounds or classes of compounds Information on mechanisms and kinetics of numerous pyrolytic processes

Pyrolysis of Organic Molecules

Serban C. Moldoveanu

Author : Serban C. Moldoveanu
Publisher : Elsevier
Page : 816 pages
File Size : 43,6 Mb
Release : 2018-11-14
Category : Science
ISBN : 9780444640017

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Pyrolysis of Organic Molecules by Serban C. Moldoveanu Pdf

Pyrolysis of Organic Molecules: Applications to Health and Environmental Issues, Second Edition offers a systematic presentation of pyrolysis results for the main classes of non-polymeric organic molecules. It covers a large body of data published on pyrolysis, as well as numerous original contributions to the pyrolysis of compounds not previously studied. This thoroughly revised edition contains new results reported in the literature since the first edition published, including the generation of traces of toxic compounds in various pyrolytic processes; the pyrolysis in the presence of catalysts and solid supports such as alumina, silica, and non-inert metals; and pyrolysis of specific mixtures of compound such as amino acids plus carbohydrates. This new information regarding the pyrolysis of these mixtures has greatly improved the utility of the book, making Pyrolysis of Organic Molecules an essential resource for chemists and chemical engineers involved in processes related to pyrolysis, as well as toxicologists and environmentalists. Presents new information on the pyrolysis of specific compounds Includes data on the mechanisms and kinetics of pyrolytic processes Provides data on the influence of catalysts and solid supports on pyrolytic processes

Horizons in Polymer Research

Robert K. Bregg

Author : Robert K. Bregg
Publisher : Nova Publishers
Page : 214 pages
File Size : 44,5 Mb
Release : 2005
Category : Science
ISBN : 1594544123

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Horizons in Polymer Research by Robert K. Bregg Pdf

Polymers are substances containing a large number of structural units joined by the same type of linkage. These substances often form into a chain-like structure. Starch, cellulose, and rubber all possess polymeric properties. Today, the polymer industry has grown to be larger than the aluminum, copper and steel industries combined. Polymers already have a range of applications that far exceeds that of any other class of material available to man. Current applications extend from adhesives, coatings, foams, and packaging materials to textile and industrial fibers, elastomers, and structural plastics. Polymers are also used for most composites, electronic devices, biomedical devices, optical devices, and precursors for many newly developed high-tech ceramics. This new book presents leading-edge research in this rapidly-changing and evolving field.

Analytical Pyrolysis

C.E.R. Jones

Author : C.E.R. Jones
Publisher : Elsevier
Page : 435 pages
File Size : 42,5 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780444601407

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Analytical Pyrolysis by C.E.R. Jones Pdf

Analytical Pyrolysis presents the Proceedings of the Third International Symposium on Analytical Pyrolysis, held in Amsterdam on September 7-9, 1976. It looks at newly emergent techniques in analytical pyrolysis, including pyrolysis mass spectrometry, gas chromatography, thin-layer chromatography, and pyrolysis-gas liquid chromatography. The book also covers topics ranging from automation and microbiology to forensic science and pharmacology, reproducibility and specificity, biochemistry, laser-induced pyrolysis, pyrolytic reaction mechanisms, and polymers. Comprised of 50 chapters, this book begins with a discussion of automatic analysis of tire rubber blends using computer-linked pyrolysis gas chromatography, thermal procedures in coupling with thin-layer chromatography, the role of pyrolysis-gas liquid chromatography in biomedical studies, and the identification of microorganisms by pyrolysis gas-liquid chromatography. It then examines forensic applications of analytical pyrolysis techniques, structure and degradation behavior of synthetic polymers using pyrolysis in combination with field ion mass spectrometry, determination of polysaccharides in fulvic acids by pyrolysis gas chromatography, and application of Curie-point pyrolysis mass spectrometry in fungal taxonomy. The reader is also introduced to pyrolysis mass spectrometry of model compounds labeled with stable isotopes, the use of pyrolysis/gas chromatography to determine the quality of porous polymers of styrene cross-linked with divinyl benzene, and application of pyrohydrolysis for a rapid and accurate determination of halides in silicate rocks and minerals. This volume will benefit students, researchers, chemists, and scientists working in the field of analytical pyrolysis.

Pyrolysis - GC/MS Data Book of Synthetic Polymers

Shin Tsuge,Hajima Ohtani,Chuichi Watanabe

Author : Shin Tsuge,Hajima Ohtani,Chuichi Watanabe
Publisher : Elsevier
Page : 420 pages
File Size : 52,6 Mb
Release : 2011-08-02
Category : Science
ISBN : 9780444538932

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Pyrolysis - GC/MS Data Book of Synthetic Polymers by Shin Tsuge,Hajima Ohtani,Chuichi Watanabe Pdf

In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample

Analytical Pyrolysis Of Natural Organic Polymers

Analytical Pyrolysis of Natural Organic Polymers by S.C. Moldoveanu Pdf

Analytical Pyrolysis of Synthetic Organic Polymers by Serban C. Moldoveanu Pdf

Analytical Pyrolysis of Synthetic Organic Polymers by Serban C. Moldoveanu Pdf

Analytical Pyrolysis of Natural Organic Polymers by S.C. Moldoveanu Pdf

Analytical Pyrolysis by Peter Kusch Pdf

Analytical Pyrolysis by Peter Kusch Pdf

Analytical Pyrolysis Handbook by Karen D. Sam,Thomas P. Wampler Pdf

Pyrolysis-gas Chromatography/mass Spectrometry Of Polymeric Materials (Second Edition) by Peter Kusch Pdf

Analytical Pyrolysis by Kent J Voorhees Pdf

Pyrolysis-gas Chromatography: Mass Spectrometry Of Polymeric Materials by Peter Kusch Pdf

Pyrolysis of Organic Molecules by Serban C. Moldoveanu Pdf

Pyrolysis of Organic Molecules by Serban C. Moldoveanu Pdf

Horizons in Polymer Research by Robert K. Bregg Pdf

Analytical Pyrolysis by C.E.R. Jones Pdf

Pyrolysis - GC/MS Data Book of Synthetic Polymers by Shin Tsuge,Hajima Ohtani,Chuichi Watanabe Pdf

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