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Author : Horst Friebolin
Publisher : Unknown
Page : 402 pages
File Size : 42,6 Mb
Release : 1993
Category : Nuclear magnetic resonance spectroscopy
ISBN : UOM:39015048776226
Author : Horst Friebolin
Publisher : Unknown
Page : 400 pages
File Size : 51,7 Mb
Release : 1993
Category : Nuclear magnetic resonance spectroscopy
ISBN : UOM:39015049074514
Author : Atta-ur- Rahman
Publisher : Elsevier
Page : 599 pages
File Size : 51,8 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483290713
The field of nuclear magnetic resonance spectroscopy has undergone explosive development during the last decade with the advent of new one- and two-dimensional techniques. The author has had extensive experience in the use of these techniques for the structure elucidation of complex natural products, and in this book he gives a comprehensive, up-to-date and very readable account of these developments. The book's scope is very wide. It starts from fundamental principles of modern NMR spectroscopy, describing the instrumentation and its optimum use, and extends to the latest developments such as inverse measurements. Emphasis is on problem-solving so as to be useful to a large number of organic chemists, biochemists and medicinal chemists. The problems and worked solutions at the end of the chapters will help students to gain proficiency in the application of these new techniques. Those who are learning how to operate modern NMR spectrometers will find particularly useful the description of such basic aspects as shimming, probe tuning, and methods for improvement of resolution and sensitivity.
Author : Horst Friebolin
Publisher : John Wiley & Sons
Page : 452 pages
File Size : 45,7 Mb
Release : 2010-12-28
Category : Science
ISBN : 9783527327829
This is the fifth edition of the highly successful, classic textbook for bachelor and master courses, with over 20 % new material and the contents completely revised and updated. Using a minimum of mathematics, it explains the underlying theory of this most important spectroscopic technique in a thorough, yet readily understandable way, covering instrumentation and interpretation of the spectra. It presents all students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy, as well as NMR imaging, all illustrated by examples for maximum clarity. All the sections include sub-chapters that focus on applications taken from organic, macromolecular, polymer and biochemistry. A must for students and lecturers in chemistry, biochemistry, pharmacy, and life sciences, as well as for spectroscopists.
Author : Harald Günther
Publisher : John Wiley & Sons
Page : 842 pages
File Size : 51,6 Mb
Release : 2013-12-13
Category : Science
ISBN : 9783527674770
Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.
Author : L. D. Field,H. L. Li,A. M. Magill
Publisher : John Wiley & Sons
Page : 328 pages
File Size : 53,7 Mb
Release : 2015-06-15
Category : Science
ISBN : 9781118868942
The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D-NMR spectroscopy. The problems are graded to develop and consolidate a student’s understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one-dimensional NMR spectroscopy Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry Focuses on the most common 2D NMR techniques – including COSY, NOESY, HMBC, TOCSY, CH-Correlation and multiplicity-edited C-H Correlation. Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectra is a logical follow-on from the highly successful “Organic Structures from Spectra” which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Also available: Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra
Author : William R. Croasmun,Robert M. K. Carlson
Publisher : VCH Publishers
Page : 994 pages
File Size : 48,8 Mb
Release : 1994
Category : Science
ISBN : UOM:39015032550876
Author : W. R. Croasmun,Robert M. K. Carlson
Publisher : John Wiley & Sons
Page : 1692 pages
File Size : 50,9 Mb
Release : 1996-12-17
Category : Science
ISBN : 0471185930
Diese Neuauflage behandelt auch die methodischen Fortschritte in der NMR-Spektroskopie, die seit der ersten Auflage gemacht wurden. Dazu gehören die indirekten Nachweismethoden, die die Empfindlichkeit wesentlich gesteigert haben; die drei- und mehrdimensionale NMR mit ihrer erhöhten spektralen Auflösung und Korrelationsvermögen; neue Programme, die die Molekularmechanik und dynamische Rechnungen ausnutzen und mit denen man komplexe zwei- und mehrdimensionale NMR- Spektren genau auswerten kann; und das Gradientenverfahren, das die Untersuchungszeit wesentlich verkürzt. Die Neuauflage behält den bewährten Aufbau der ersten Ausgabe bei: Einführende Kapitel mit Beschreibungen, den Grundlagen der Theorie und den experimentellen Aspekten stehen Anwendungskapiteln voran, die die Breite der Forschungsgebiete und Verbindungsklassen illustrieren. Aus Besprechungen der ersten Auflage: ... mit seinem einzigartigen Inhalt und praktischen Wert wird es seinen Platz auf den Bücherbrettern der meisten NMR-Laboratorien finden. (Journal of Natural Products)
Author : Jeffrey H. Simpson
Publisher : Academic Press
Page : 591 pages
File Size : 40,7 Mb
Release : 2011-12-30
Category : Science
ISBN : 9780123849700
"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--
Author : Neil E. Jacobsen
Publisher : John Wiley & Sons
Page : 648 pages
File Size : 43,5 Mb
Release : 2016-10-21
Category : Science
ISBN : 9781119176886
Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings
Author : Richard R. Ernst,Geoffrey Bodenhausen,Alexander Wokaun
Publisher : Unknown
Page : 0 pages
File Size : 44,7 Mb
Release : 2023
Category : Nuclear magnetic resonance spectroscopy
ISBN : 1383028621
Nuclear magnetic resonance spectroscopy is one of the most powerful and versatile techniques now available for the study of molecular structure and reaction mechanisms. Written by recognised experts in the field, this classic account of modern NMR spectroscopy was heralded on its first publication in 1987 as 'the lasting text of its age'. The text provides a thoroughly comprehensive review of modern NMR techniques and the underlying principles. It describes the study of solutions and solids using one- and two-dimensional spectroscpy, providing both a solid theoretical foundation and a description of practical procedures. The material is presented in an intuitive manner within a rigorous mathematical framework, and is extensively illustrated throughout.
Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 42,8 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Author : Harald Günther
Publisher : John Wiley & Sons
Page : 739 pages
File Size : 55,9 Mb
Release : 2013-11-04
Category : Science
ISBN : 9783527330003
Auch die komplett überarbeitete 3. Auflage dieses bewährten Lehrbuchs überzeugt durch Klarheit, eine didaktisch gelungene Aufbereitung des Stoffes und ein hohes Maß an Praxisbezug. Das komplexe Thema wird mit einem Mindestmaß an Mathematik erklärt - ideal für Studenten, die die Grundlagen der NMR-Spektroskopie verstehen und das Verfahren effizient und präzise anwenden möchten. Die neue Auflage ist vollständig überarbeitet und aktualisiert. So sind rund 25% der Inhalte neu, darunter auch Kapitel zur biologischen NMR-Spektroskopie sowie viele Beispiele aus der organischen Chemie. Daher stellt dieses Fachbuch auch für Studenten in Grund- und Hauptstudium verwandter Fachrichtungen wie der Biochemie, Medizinischen Chemie, Pharmazeutischen Chemie und Materialwissenschaften einen wertvollen Leitfaden dar. Außerdem findet der Leser eine Vielzahl von Übungsaufgaben mit zugehörigen Lösungen.
Author : A.E. Derome
Publisher : Elsevier
Page : 299 pages
File Size : 42,6 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483286426
Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.
Author : L. D. Field
Publisher : Wiley-Blackwell
Page : 128 pages
File Size : 48,9 Mb
Release : 2015-05-18
Category : Electronic
ISBN : 1119073707
The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two–dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D–NMR spectroscopy. The problems are graded to develop and consolidate a students understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra: – Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one–dimensional NMR spectroscopy – Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry – Focuses on the most common 2D NMR techniques including COSY, NOESY, HMBC, TOCSY, CH–Correlation and multiplicity–edited C–H Correlation. – Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectrais a logical follow–on from the highly successful Organic Structures from Spectra which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Organic Structures from 2D NMR Spectra is complimented by the Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra which is a set of step–by–step worked solutions to every problem in the book. While it is absolutely clear that there are many ways to get to the correct solution of any of the problems, the instructors guide contains at least one complete pathway to every one of the questions. In addition, the instructors guide carefully rationalises every peak in every spectrum in relation to the correct structure. The Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra: – Is a complete set of worked solutions to the problems contained in Organic Structures from 2D NMR Spectra. – Provides a step–by–step description of the process to derive structures from spectra as well as annotated 2D spectra indicating the origin of every cross peak. – Highlights common artefacts and re–enforces the important characteristics of the most common techniques 2D NMR techniques including COSY, NOESY, HMBC, TOCSY, CH–Correlation and multiplicity–edited C–H Correlation. This guide is an essential aid to those teachers, lecturers and instructors who use Organic Structures from 2D NMR as a text to teach students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry.