Nuclear Magnetic Resonance Spectroscopy

Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 53,7 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235

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Nuclear Magnetic Resonance Spectroscopy by Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge Pdf

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Author : Heinrich Nöth,Bernd Wrackmeyer
Publisher : Springer Science & Business Media
Page : 474 pages
File Size : 54,6 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642667572

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Nuclear Magnetic Resonance Spectroscopy of Boron Compounds by Heinrich Nöth,Bernd Wrackmeyer Pdf

The revolutionary impetus of the NMR methods in organic chemistry has parallels in the field of boron chemistry. lIB NMR spectroscopy provided a basis for the elucida tion of structures and reactions of the boron hydrides. However, although many studies have been carried out with the higher boranes, carboranes, metalloboranes, etc. , and although certain patterns have emerged, the correlation between the observed chemical shift and the assigned structural unit is still not fully understood. Therefore, predictions in this area are still rather limited, and semiquantitative interpretations are not yet pos sible. Several years ago Eaton and Lipscomb sUpImarized the status in this field in their book "NMR Studies of Boron Hydrides and Related Compounds" and a plethora of new data has accumulated since then. The book also contained material on simple bo rane derivatives, but they were not discussed in any detail. On the other hand many systematic studies, both synthetic and spectroscopic, have been conducted on these simple boron materials in the last decade. Thus a large amount of NMR information is available, not only on lIB but also on 1 H, 1 3 C, and 14 N. However, this information is widely scattered in the literature, and often the data are not discussed at all. It see med appropriate, therefore, to collect these data and to present them in one volume.

Author : Atta-ur-Rahman,M. Iqbal Choudhary
Publisher : Bentham Science Publishers
Page : 289 pages
File Size : 51,5 Mb
Release : 2016-11-22
Category : Science
ISBN : 9781681082875

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Applications of NMR Spectroscopy by Atta-ur-Rahman,M. Iqbal Choudhary Pdf

Applications of NMR Spectroscopy is a book series devoted to publishing the latest advances in the applications of nuclear magnetic resonance (NMR) spectroscopy in various fields of organic chemistry, biochemistry, health and agriculture. The fifth volume of the series features several reviews focusing on NMR spectroscopic techniques for identifying natural and synthetic compounds (polymer and peptide characterization, GABA in tinnitus affected mice), medical diagnosis and therapy (gliomas) and food analysis. The spectroscopic methods highlighted in this volume include high resolution proton magnetic resonance spectroscopy and solid state NMR.

Author : John Henry Nelson
Publisher : Unknown
Page : 488 pages
File Size : 40,8 Mb
Release : 2003
Category : Education
ISBN : STANFORD:36105110252751

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Nuclear Magnetic Resonance Spectroscopy by John Henry Nelson Pdf

This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H andC in depth. It contains extensive reference material and numerous problems, most of which include real spectra. It is written to provide users with the knowledge necessary to choose the most appropriate experiment to obtain the best quality spectra with the ability to fully interpret the data. The book covers basic theory of NMR spectroscopy, spectrum measurement, the chemical shift and examples for selected nuclei, symmetry and NMR spectroscopy, spin-spin coupling and NMR spin systems, typical magnitude of selected coupling constants, nuclear spin relaxation, the nuclear overhauser effect, editing C NMR spectra, two-dimensional NMR spectroscopy, dynamic NMR spectroscopy, lanthanide shift reagents (LSR), NMR of solids. For NMR spectroscopists and analytical chemists.

Author : Mark A. Nanny,R. A. Minear,J. A. Leenheer
Publisher : Oxford University Press, USA
Page : 341 pages
File Size : 49,6 Mb
Release : 1997
Category : Science
ISBN : 9780195097511

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Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry by Mark A. Nanny,R. A. Minear,J. A. Leenheer Pdf

This book demonstrates the usefulness of NMR spectroscopy for a wide variety of applications in environmental science and technology. It contains a wealth of information relating to instrumentation, sample preparation, and data interpretation. The book is divided into three sectionsdiscussing contaminant interaction, solution and condensed-phase characterization, and nutrients and natural organic matter characterization. In addition to these in-depth chapters, an introductory overview provides the basic principles of solution and solid-state NMR spectroscopy. Each sectionalso contains a discussion of advances in each area directly attributable to NMR spectroscopy. A final chapter suggests future directions for the deployment of this powerful technology in environmental science.

Author : Simonpietro Agnello
Publisher : John Wiley & Sons
Page : 500 pages
File Size : 42,5 Mb
Release : 2021-09-08
Category : Technology & Engineering
ISBN : 9781119697329

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Spectroscopy for Materials Characterization by Simonpietro Agnello Pdf

SPECTROSCOPY FOR MATERIALS CHARACTERIZATION Learn foundational and advanced spectroscopy techniques from leading researchers in physics, chemistry, surface science, and nanoscience In Spectroscopy for Materials Characterization, accomplished researcher Simonpietro Agnello delivers a practical and accessible compilation of various spectroscopy techniques taught and used to today. The book offers a wide-ranging approach taught by leading researchers working in physics, chemistry, surface science, and nanoscience. It is ideal for both new students and advanced researchers studying and working with spectroscopy. Topics such as confocal and two photon spectroscopy, as well as infrared absorption and Raman and micro-Raman spectroscopy, are discussed, as are thermally stimulated luminescence and spectroscopic studies of radiation effects on optical materials. Each chapter includes a basic introduction to the theory necessary to understand a specific technique, details about the characteristic instrumental features and apparatuses used, including tips for the appropriate arrangement of a typical experiment, and a reproducible case study that shows the discussed techniques used in a real laboratory. Readers will benefit from the inclusion of: Complete and practical case studies at the conclusion of each chapter to highlight the concepts and techniques discussed in the material Citations of additional resources ideal for further study A thorough introduction to the basic aspects of radiation matter interaction in the visible-ultraviolet range and the fundamentals of absorption and emission A rigorous exploration of time resolved spectroscopy at the nanosecond and femtosecond intervals Perfect for Master and Ph.D. students and researchers in physics, chemistry, engineering, and biology, Spectroscopy for Materials Characterization will also earn a place in the libraries of materials science researchers and students seeking a one-stop reference to basic and advanced spectroscopy techniques.

Author : Harald Günther
Publisher : John Wiley & Sons
Page : 842 pages
File Size : 41,5 Mb
Release : 2013-12-13
Category : Science
ISBN : 9783527674770

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NMR Spectroscopy by Harald Günther Pdf

Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.

Author : Frank A. Bovey,Peter A. Mirau,H. S. Gutowsky
Publisher : Elsevier
Page : 668 pages
File Size : 49,6 Mb
Release : 1988-11-01
Category : Science
ISBN : 9780080916996

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Nuclear Magnetic Resonance Spectroscopy by Frank A. Bovey,Peter A. Mirau,H. S. Gutowsky Pdf

Nuclear Magnetic Resonance Spectroscopy, Second Edition focuses on two-dimensional nuclear magnetic resonance (NMR) spectroscopy, high resolution NMR of solids, water suppression, multiple quantum spectroscopy, and NMR imaging. The selection first takes a look at the fundamental principles and experimental methods. Discussions focus on the NMR phenomenon, dipolar broadening and spin-spin relaxation, nuclear electric quadrupole relaxation, saturation, magnetic shielding and chemical shift, magnetic field, transitions between the nuclear energy levels, and resolution and sensitivity considerations. The manuscript then ponders on chemical shift, coupling of nuclear spins, and nuclear relaxation and chemical rate processes. Topics include spin lattice relaxation, spin-spin relaxation, spin decoupling and associated techniques, and description and analysis of spin systems. The text examines two-dimensional NMR spectroscopy, macromolecules, and NMR of solids, including magic angle spinning, cross polarization, proton dipolar broadening, biopolymers, and chain motion in macromolecules. The selection is a valuable source of data for readers interested in nuclear magnetic resonance spectroscopy.

Author : L. M. Jackman,S. Sternhell
Publisher : Elsevier
Page : 474 pages
File Size : 54,6 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483280943

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Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry by L. M. Jackman,S. Sternhell Pdf

Application of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry, Second Edition covers the theoretical background necessary for the intelligent application of NMR spectroscopy to common problems encountered in organic chemistry. This book is composed of five parts, and begins with introduction to the theory and practice of nuclear magnetic resonance. The succeeding chapter deals with the theory of chemical effects in NMR spectroscopy. These topics are followed by a discussion on the application of chemical shift to organic compound analysis and the principles of the spin-spin coupling .The final chapter considers the applications of time- dependent phenomena in NMR spectroscopy. This book will prove useful to analytical chemists and researchers in the allied fields.

Author : Frank Alden Bovey
Publisher : Unknown
Page : 420 pages
File Size : 51,7 Mb
Release : 1969
Category : Science
ISBN : UOM:39015003714592

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Nuclear Magnetic Resonance Spectroscopy by Frank Alden Bovey Pdf

Nine chapters cover: fundamental principles; experimental methods; the chemical shift; coupling of nuclear spins; nuclear relaxation and chemical rate processes; two-dimensional nuclear magnetic resonance spectroscopy; macromolecules; NMR of solids; special topics. Annotation copyrighted by Book News, Inc., Portland, OR

Author : Teresa Lehmann
Publisher : MDPI
Page : 307 pages
File Size : 49,5 Mb
Release : 2018-06-13
Category : Electronic books
ISBN : 9783038429937

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Nuclear Magnetic Resonance Spectroscopy by Teresa Lehmann Pdf

Nuclear Magnetic Resonance Spectroscopy.

Author : Robin Kingsley Harris
Publisher : Longman Publishing Group
Page : 300 pages
File Size : 49,6 Mb
Release : 1986
Category : Kernmagnetiese resonans-spektroskopie
ISBN : UCSD:31822005882741

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Nuclear Magnetic Resonance Spectroscopy by Robin Kingsley Harris Pdf

Author : T.I. Atta-Ur-Rahman
Publisher : Springer Science & Business Media
Page : 366 pages
File Size : 54,7 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781461248941

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Nuclear Magnetic Resonance by T.I. Atta-Ur-Rahman Pdf

Nuclear magnetic resonance spectroscopy is presently going through an explosive phase of development. This has been brought about largely on account of the advent of Fourier transform NMR spectrometers linked to powerful microcomputers which have opened up a whole new world for structural chemists and biochemists. This is exemplified by a host of publications, especially on new pulse sequences, which continue to provide new exciting modifications for recording two-dimensional NMR. Moreover, NMR is no longer confined to structural chemists but has moved firmly into the area of medicine as a powerful nondestructive body scanning technique. With this background, I felt that there was need for a text which would provide a fairly comprehensive account of the important features of 1 H- and 13C-NMR spectroscopy in one book, as well as make available an up-to-date account of recent developments of new pulse sequences, with particular reference to 2D-NMR spectroscopy. Since this book is written for students of chemistry and biochemistry as well as for biology students who have chemistry as a subsidiary, it was decided to avoid a complex mathematical treatment and to present, as far as possible without oversimplification, a qualitative account of 1 H- and 13C-NMR spectroscopy as it is today. I hope that the book satisfactorily meets these objectives.

Author : Ronald Y. Dong
Publisher : World Scientific
Page : 462 pages
File Size : 46,5 Mb
Release : 2010
Category : Science
ISBN : 9789814273664

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Nuclear Magnetic Resonance Spectroscopy of Liquid Crystals by Ronald Y. Dong Pdf

This edited volume provides an extensive overview of how nuclear magnetic resonance can be an indispensable tool to investigate molecular ordering, phase structure, and dynamics in complex anisotropic phases formed by liquid crystalline materials. The chapters, written by prominent scientists in their field of expertise, provide a state-of-the-art scene of developments in liquid crystal research. The fantastic assortment of shape anisotropy in organic molecules leads to The discoveries of interesting new soft materials made at a rapid rate which not only inject impetus to address the fundamental physical and chemical phenomena, but also the potential applications in memory, sensor and display devices. The review volume also covers topics ranging from solute studies of molecules in nematics and biologically ordered fluids to theoretical approaches in treating elastic and viscous properties of liquid crystals. This volume is aimed at graduate students, novices and experts alike, and provides an excellent reference material for readers interested in the liquid crystal research. it is, indeed, a reference book for every science library to have.

Author : M. Mehring
Publisher : Springer Science & Business Media
Page : 352 pages
File Size : 52,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642687563

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Principles of High Resolution NMR in Solids by M. Mehring Pdf

The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which treats the principles, theo retical foundations and applications of these rather sophisticated experimental techniques. Therefore I wrote a monograph on the subject in 1976. Very soon new ideas led to the developement of "two-dimensional spectroscopy" and "multiple-quantum spectroscopy", topics which were not covered in the first edition of my book. Moreover an exponential growth of literature appeared in this area of research leaving the beginner in an awkward situation of tracing back from a current article to the roots of the experiment.