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Author : Demetrios K. Kyriacou
Publisher : John Wiley & Sons
Page : 184 pages
File Size : 54,9 Mb
Release : 1981
Category : Science
ISBN : UCAL:B4477513
Author : Sigeru Torii
Publisher : Springer Science & Business Media
Page : 475 pages
File Size : 54,5 Mb
Release : 2013-03-09
Category : Science
ISBN : 9784431659242
Among the topics of interest to organic chemists today are the versatility and uniqueness of electrolysis procedures in organic synthesis, as well as the latest advances in methodology, including basic concepts for the design of electrolysis conditions and apparatus. The International Symposium on Electroorganic Synthesis met in Kurashiki, Japan, in September 1997 for lectures on all aspects of current research in the field. This volume comprising the papers from the symposium consists of two parts. Part I, Electrooxidation, includes papers on alcohols and phenols, olefins and aromatics, halogenation, polymers, and electrodes, among others. Included in Part II, Electroreduction, are papers on carbonyl compounds, halogen-containing compounds, reaction with EG bases, and metal complexes. The novel trends presented here will be of special interest to researchers and graduate students in electroorganic chemistry and are a valuable resource for all organic chemists.
Author : Toshio Fuchigami,Mahito Atobe,Shinsuke Inagi
Publisher : John Wiley & Sons
Page : 238 pages
File Size : 45,9 Mb
Release : 2014-11-10
Category : Science
ISBN : 9781118653173
This textbook is an accessible overview of the broad field of organic electrochemistry, covering the fundamentals and applications of contemporary organic electrochemistry. The book begins with an introduction to the fundamental aspects of electrode electron transfer and methods for the electrochemical measurement of organic molecules. It then goes on to discuss organic electrosynthesis of molecules and macromolecules, including detailed experimental information for the electrochemical synthesis of organic compounds and conducting polymers. Later chapters highlight new methodology for organic electrochemical synthesis, for example electrolysis in ionic liquids, the application to organic electronic devices such as solar cells and LEDs, and examples of commercialized organic electrode processes. Appendices present useful supplementary information including experimental examples of organic electrosynthesis, and tables of physical data (redox potentials of various organic solvents and organic compounds and physical properties of various organic solvents).
Author : Tatsuya Shono
Publisher : Springer Science & Business Media
Page : 180 pages
File Size : 40,9 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642694936
Although the first electroorganic reaction used in organic synthesis is probably the famous Kolbe electrolysis published in 1849, no other remarkable reactions have been found until the reductive dimerization of acrylonitrile to adipo nitrile was developed by Dr. M. M. Baizer of Monsanto Co. in 1964. Since then, the electro organic chemistry has been studied extensively with the expectation that it is a new useful tool for finding novel reactions in organic synthesis. The purpose of this book is not to give a comprehensive survey of studies on electrochemical reactions of organic compounds but to show that the electro organic chemistry is indeed useful in organic synthesis. Thus, this book has been written under the following policies. (1) Since this monograph is mainly concerned with organic synthesis, only few studies carried out from the view point of electrochemical, theoretical, or analytical chemistry are mentioned. (2) Since electroorganic chemistry covers a great variety of reactions, the types of reactions described in this book are selected mainly with regard to their application in organic synthesis. Simple transformations of functional groups are only described in particular cases, and also some well established processes such as the Kolbe electrolysis, pinacolic coupling, and hydrodimerization are only briefly mentioned. (3) Since many reports have already been published for each type of these reactions, only a limited number of the relevant papers are cited in this book.
Author : Davood Nematollahi,Saber Alizadeh,Ameneh Amani,Sadegh Khazalpour
Publisher : Elsevier
Page : 352 pages
File Size : 55,6 Mb
Release : 2024-06-04
Category : Science
ISBN : 9780323956673
Practical Aspects of Electroorganic Synthesis presents educational insights into the practical aspects of electrosynthesis methods, providing a variety of examples and techniques. The book covers concepts referred to as "green chemistry" and "sustainable technology." Sections cover direct electrolysis, anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set-up electrochemical experiments. Indirect electrolysis is also covered, including an exploration of catalysts and additives to take on modern electrochemical methods. Finally, the book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products. This book offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques. Discusses complete and up-to-date practical concepts of electrosynthesis methods Provides sound insights into the experimental approaches of electrosynthesis, covering new and novel synthesis techniques Breaks down the fundamentals aspects of electrolysis into three digestible and logical sections
Author : Ralph Roberts,Robert P. Ouellette,Paul N. Cheremisinoff
Publisher : Ann Arbor Science Publishers
Page : 232 pages
File Size : 46,7 Mb
Release : 1982
Category : Electrochemistry, Industrial
ISBN : UCAL:B4125457
Author : John ApSimon
Publisher : John Wiley & Sons
Page : 624 pages
File Size : 54,8 Mb
Release : 2009-09-22
Category : Science
ISBN : 9780470129531
The Vocabulary of Organic Chemistry Milton Orchin, Fred Kaplan,Roger S. Macomber, R. Marshall Wilson & Hans W. ZimmerIdentifies those terms and concepts which now constitute thevocabulary of organic chemists, then defines and explains theseterms and concepts, most often using examples. Organized so thatsubject matter builds successively on increasingly varied andcomplex material. All terms and concepts related to a particulararea are placed together, except for one chapter on name and typereactions, which is alphabetically arranged. The only book of itskind--valuable to students, teachers and chemical professionalsalike. 1980 Protective Groups in Organic Synthesis Theodora W.Greene Provides essential information on transformations of organicmolecules, including instructions and references for the protectionand regeneration of the major organic functional groups: -OH, -NH,-SH, -COOH, and C = O. Covers the best methods of formation andcleavage, properties of protective groups, selection of a group fora particular need. Organization is by functional groups to beprotected, with groups arranged in order of increasing complexityof structure, and with most efficient methods of formation orcleavage described first. Charts show the reactivities of 270 ofthe most commonly used protective groups to 108 reagents, selectedas prototypes for the entire array of reagents available to theorganic chemist. 1981 Basics of Electroorganic Synthesis DemetriosK. Kyriacou A veteran organic electrochemist illuminatesfundamental ideas and principles by means of selected examples fromthe literature and his own research, demonstrating the practicalunity of the field in a clear, concise manner. Describes thegeneral electroorganic reaction and illustrates the general mode ofconcepts and applications in the area of electrosynthesis. Containsa brief survey of electroorganic reactions and coverage of specialtopics and the praxis of electroorganic synthesis. 1981
Author : Norman L. Weinberg,B. V. Tilak
Publisher : John Wiley & Sons
Page : 938 pages
File Size : 55,9 Mb
Release : 1974
Category : Science
ISBN : UOM:49015000655572
Author : Demetrios K. Kyriacou
Publisher : Springer
Page : 250 pages
File Size : 42,5 Mb
Release : 1994
Category : Science
ISBN : UOM:39015032193032
Author : Jiri Volke,Frantisek Liska
Publisher : Springer Science & Business Media
Page : 161 pages
File Size : 42,9 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642786990
This book has been written as an introduction to the electro synthesis of organic compounds, in particular for organic chemists. Both authors assume that the knowledge of electro chemistry of these specialists is rather poor and is usually based only on the remnants of the teaching in the courses on physical and analytical chemistry during their university stud ies. Even with Czech chemists one cannot expect - as it was in the past - the experience obtained in the courses on polaro graphy. This is the reason why it was deemed necessary to write an introductory text to the electro synthesis of organics both as regards the theoretical and the methodological point of view, i. e. the fundamentals, the experimental setup, the application of various working and reference electrodes, the shape and con struction of electrolysis cells, the use of suitable pro tic and aprotic solvents, the experience obtained with various sup porting electrolytes, the separation and isolation of products, as well as the use of inert gases which prevent the interaction of intermediates and of final products with, for example, oxygen or traces of water. - The second part of the book contains a systematic description of preparative organic electrochemical processes, the interpretation of their mechanisms and several prescriptions for synthesizing characteristical groups of com pounds. As a whole the book is not written in an exhaustive way.
Author : L. K. Doraiswamy
Publisher : Oxford University Press
Page : 942 pages
File Size : 52,5 Mb
Release : 2001-02-15
Category : Technology & Engineering
ISBN : 0198025696
This book will formally launch "organic synthesis engineering" as a distinctive field in the armory of the reaction engineer. Its main theme revolves around two developments: catalysis and the role of process intensification in enhancing overall productivity. Each of these two subjects are becoming increasingly useful in organic synthesis engineering, especially in the production of medium and small volume chemicals and enhancing reaction rates by extending laboratory techniques, such as ultrasound, phase transfer catalysts, membrane reactor, and microwaves, to industrial scale production. This volume describes the applications of catalysis in organic synthesis and outlines different techniques of reaction rate and/or selectivity enhancement against a background of reaction engineering principles for both homogeneous and heterogeneous systems.
Author : Frank Marken,Mahito Atobe
Publisher : CRC Press
Page : 227 pages
File Size : 43,5 Mb
Release : 2018-10-11
Category : Science
ISBN : 9780429783838
Modern Electrosynthetic Methods in Organic Chemistry introduces readers to new ways of making materials and compounds using low waste processes, employing energy from electricity rather than chemical reagents. It explores electro-organic synthesis, which offers clean synthesis tools as well as unusual reaction intermediates and reaction types. Despite applications previously remaining niche, due to the advent of microfluidic reactors this book is a must-read for industry professionals and academics alike. It targets specific areas of recent progress and development in the field that show high novelty and potential, at the same time inviting a wider range of applications in green and clean technology. Key Features: Offers clean synthesis tools Targets areas of recent progress and development Addresses the most recent advances in the field
Author : Demetrios K. Kyriacou,Demetrios A. Jannakoudakis
Publisher : Wiley-Interscience
Page : 168 pages
File Size : 52,6 Mb
Release : 1986
Category : Catalysis
ISBN : UCAL:B4476905
A concise introduction to practical electrocatalysis for organic synthesis covering recent trends and applications of modern electroorganic chemistry. Ideal as a quick reference source and initial guide to the new area of electrocatalytic organic synthesis.
Author : Tatsuya Shōno
Publisher : Unknown
Page : 184 pages
File Size : 42,9 Mb
Release : 1991
Category : Science
ISBN : UOM:39015021869196
This book provides the first practical, hands-on approach to electroorganic synthesis. It includes many details of the experimental design of cells, electrodes, electrolytes, and so on, as well as methods and reaction conditions for a large range of chemical transformations. By demonstrating the practicalities and versatility of electroorganic synthesis, this book encourages synthetic chemists to learn electrochemical methods for use in their daily activities.
Author : D.R. Crow
Publisher : Routledge
Page : 276 pages
File Size : 42,5 Mb
Release : 2017-09-06
Category : Science
ISBN : 9781351422086
This introduction to the principles and application of electrochemistry is presented in a manner designed for undergraduates in chemistry and related fields. The author covers the essential aspects of the subject and points the way to further study, his concern being with the overall shape of electrochemistry, its coherence and its wider application. This edition differs from its predecessors in having principles and applications separated, and greater prominence is given to areas such as electrochemical sensors and electroanalytical techniques, of which a number of modern methods were not included in previous editions. A range of numerical problems and outline solutions is provided for each chapter to cover most situations that a student might encounter.