Crystallization Processes And Applications

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Crystallization

Wolfgang Beckmann
Crystallization Book PDF

Author : Wolfgang Beckmann
Publisher : John Wiley & Sons
Page : 370 pages
File Size : 41,5 Mb
Release : 2013-01-14
Category : Science
ISBN : 9783527650347

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Crystallization by Wolfgang Beckmann Pdf

Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

Crystallization: Processes and Applications

Garry Hollis
Crystallization Processes and Applications Book PDF

Author : Garry Hollis
Publisher : Unknown
Page : 0 pages
File Size : 52,9 Mb
Release : 2022-09-13
Category : Electronic
ISBN : 1639891315

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Crystallization: Processes and Applications by Garry Hollis Pdf

A solid material whose constituents such as atoms, molecules, or ions are arranged in a highly ordered microscopic structure is referred to as a crystal. The physical transformation of a liquid, solution, or gas to a crystal is known as crystallization. Crystals are formed by phenomena such as precipitation, freezing, or deposition directly from a gas. The occurrence of crystallization involves two major steps, namely, nucleation and crystal growth. Its most prominent application is salt crystallization which is the most cost-effective way to produce salt. Applications of crystallization involve compound purification and crystal production. The book aims to shed light on some of the unexplored aspects of crystallization and the recent researches in this area. Also included herein is a detailed explanation of the various concepts and applications of this process. This book will serve as a reference to a broad spectrum of readers.

Additives and Crystallization Processes

Keshra Sangwal
Additives and Crystallization Processes Book PDF

Author : Keshra Sangwal
Publisher : John Wiley & Sons
Page : 468 pages
File Size : 52,7 Mb
Release : 2007-09-27
Category : Technology & Engineering
ISBN : 0470517824

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Additives and Crystallization Processes by Keshra Sangwal Pdf

Crystal growth technology involves processes for the production of crystals essential for microelectronics, communication technologies, lasers and energy producing and energy saving technology. A deliberately added impurity is called an additive and in different industries these affect the process of crystal growth. Thus, understanding of interactions between additives and the crystallizing phases is important in different processes found in the lab, nature and in various industries. This book presents a generalized description of the mechanisms of action of additives during nucleation, growth and aggregation of crystals during crystallization and has received endorsement from the President of the International Organization for Crystal Growth. It is the first text devoted to the role of additives in different crystallization processes encountered in the lab, nature and in industries as diverse as pharmaceuticals, food and biofuels. A unique highlight of the book are chapters on the effect of additives on crystal growth processes, since the phenomena discussed is an issue of debate between researchers

Handbook of Industrial Crystallization

Allan Myerson
Handbook of Industrial Crystallization Book PDF

Author : Allan Myerson
Publisher : Butterworth-Heinemann
Page : 304 pages
File Size : 51,8 Mb
Release : 2002-01-08
Category : Science
ISBN : 0080533515

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Handbook of Industrial Crystallization by Allan Myerson Pdf

Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes. The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design. Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the field Covers all aspects of industrial crystallization in a single, complete volume

Advances in Crystallization Processes

Yitzhak Mastai
Advances in Crystallization Processes Book PDF

Author : Yitzhak Mastai
Publisher : BoD – Books on Demand
Page : 672 pages
File Size : 50,5 Mb
Release : 2012-04-27
Category : Science
ISBN : 9789535105817

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Advances in Crystallization Processes by Yitzhak Mastai Pdf

Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. In recent years, a number of new applications have also come to rely on crystallization processes such as the crystallization of nano and amorphous materials. The articles for this book have been contributed by the most respected researchers in this area and cover the frontier areas of research and developments in crystallization processes. Divided into five parts this book provides the latest research developments in many aspects of crystallization including: chiral crystallization, crystallization of nanomaterials and the crystallization of amorphous and glassy materials. This book is of interest to both fundamental research and also to practicing scientists and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia.

Industrial Crystallization Process Monitoring and Control

Angelo Chianese,Herman J. Kramer
Industrial Crystallization Process Monitoring and Control Book PDF

Author : Angelo Chianese,Herman J. Kramer
Publisher : John Wiley & Sons
Page : 253 pages
File Size : 51,8 Mb
Release : 2012-04-16
Category : Science
ISBN : 9783527331734

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Industrial Crystallization Process Monitoring and Control by Angelo Chianese,Herman J. Kramer Pdf

Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.

Crystallization of Organic Compounds

Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Crystallization of Organic Compounds Book PDF

Author : Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Publisher : John Wiley & Sons
Page : 388 pages
File Size : 46,8 Mb
Release : 2023-07-05
Category : Science
ISBN : 9781119879480

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Crystallization of Organic Compounds by Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley Pdf

Crystallization of Organic Compounds Practical resource covering applications of crystallization principles with methodologies, case studies, and numerous industrial examples for emphasis Based on the authors’ hands-on experiences as process engineers, through the use of case studies and examples of crystallization processes, ranging from laboratory development through manufacturing scale-up, Crystallization of Organic Compounds guides readers through the practical applications of crystallization and emphasizes strategies that have proven to be successful, enabling readers to avoid common pitfalls that can render standard procedures unsuccessful. Most chapters feature multiple examples that guide readers, step by step, through the crystallization of active pharmaceutical ingredients (APIs), including an analysis of the major methods of carrying out crystallization operations, their strengths and potential issues, as well as numerous examples of crystallization processes from development through manufacturing scale. Advancements in the field of crystallization have been integrated throughout the book in the newly revised Second Edition to ensure the content adequately reflects current state-of-the-art industrial know-hows and practice. The new edition also adds chapters addressing downstream operations after the crystallization, including filtration/washing and drying, together with industrial use cases. Crystallization of Organic Compounds includes detailed information on: Solubility and solid behavior, covering phase rule, polymorph, salt/co-crystal, chiral resolution and in-silico solubility prediction; and kinetics, covering seed, supersaturation, nucleation, crystal growth and model-based experimental design Critical issues in the crystallization practice, covering oiling out, seeding/wet-milling, agglomeration/aggregation, mixing scale-up and quality-by-design principles Cooling, anti-solvent, evaporation and reactive crystallization process design, covering batch and continuous operations with industrial examples Special applications, covering crystallization with ultrasound, reaction selectivity enhancement, and computation fluid dynamics, and solid dispersion With highly practical coverage of the subject, Crystallization of Organic Compounds is an essential resource for engineers and chemists involved with the development, scaling, or operation of crystallization process in the pharmaceutical and fine chemical industries, particularly those with degrees in chemical engineering and chemistry.

Advanced Topics in Crystallization

Yitzhak Mastai
Advanced Topics in Crystallization Book PDF

Author : Yitzhak Mastai
Publisher : BoD – Books on Demand
Page : 374 pages
File Size : 46,7 Mb
Release : 2015-05-06
Category : Science
ISBN : 9789535121251

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Advanced Topics in Crystallization by Yitzhak Mastai Pdf

In nearly all process industries, crystallization is used at some stage as a method of production, purification or recovery of solid materials. In recent years, a number of new applications have also come to rely on crystallization processes such as the crystallization of nano and amorphous materials. The articles in this book have been contributed by some of the most respected researchers in this area and cover the frontier areas of research and developments in crystallization processes. Divided into three sections, this book provides the latest research developments in many aspects of crystallization including the crystallization of biological macromolecules and pharmaceutical compounds, the crystallization of nanomaterials and the crystallization of amorphous and glassy materials. This book is of interest to both fundamental research and practicing scientists and will prove invaluable to all chemical engineers and industrial chemists in process industries, as well as crystallization workers and students in industry and academia.

Crystallization

Wolfgang Beckmann
Crystallization Book PDF

Author : Wolfgang Beckmann
Publisher : John Wiley & Sons
Page : 370 pages
File Size : 40,8 Mb
Release : 2013-04-01
Category : Science
ISBN : 9783527327621

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Crystallization by Wolfgang Beckmann Pdf

Crystallization is a natural occurring process but also a process abundantly used in the industry. Crystallization can occur from a solution, from the melt or via deposition of material from the gas phase (desublimation). Crystals distinguish themself from liquids, gases and amorphous substances by the long-range order of its building blocks that entail the crystals to be formed of well-defined faces, and give rise to a large number of properties of the solid. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Crystallization is practiced on all scales: from the isolation of the first milligrams of a newly synthesized substance in the research laboratory to isolating products on the mulit-million tonne scale in industry. The book describes the breadth of crystallization operations, from isolation from a reaction broth to purification and finally to tailoring product properties. In the first section of the book, the basic mechanisms - nucleation, growth, attrition and agglomeration are introduced. It ensures an understanding of supersaturation, the driving force of crystallization. Furthermore, the solubility of the substance and its dependences on process conditions and the various techniques of crystallization and their possibilities and limitations are discussed. Last but not least, the first part includes an intensive treatment of polymorphism . The second part builds on the basics, exploring how crystallization processes can be developed, either batch-wise or continuous, from solution or from the melt. A discussion of the purification during crystallization serves as a link between the two sections, where practical aspects and an insight using theoretical concepts are combined. Mixing and its influence on the crystallization as well as the mutual interference of down-stream processes with the crystallization are also treated. Finally, techniques to characterize the crop are discussed. The third part of the book is dedicated to accounts of actual developments and of carried-out crystallizations. Typical pitfalls and strategies to avoid these as well as the design of robust processes are presented.

Crystallization Process Systems

Alan G. Jones
Crystallization Process Systems Book PDF

Author : Alan G. Jones
Publisher : Butterworth-Heinemann
Page : 0 pages
File Size : 48,8 Mb
Release : 2015-01-02
Category : Technology & Engineering
ISBN : 0080993737

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Crystallization Process Systems by Alan G. Jones Pdf

Crystallization Process Systems gives a clear, concise, balanced and up to date presentation of crystallization and solid-liquid separation of crystalline products. It emphasizes the analysis, design, operation and optimization of particulate crystallization processes as systems, in order to assist process engineers and chemists decide on the best, cheapest and most effective production method to use for their application. In addition to providing background on classical crystallization, this book includes modern techniques such as CFD of crystallization systems. It thoroughly covers the impact of mixing on crystallization, and balances theory with the practical aspects of crystallizer design and practical scale-up. Presents a practically oriented approach to developing and implementing the latest crystallization techniques at commercial level. Applications and case studies are supported by a systems approach to showing the reader the relevant fundamentals of particulate crystallization processes for their applications. Emphasis on the design and optimization of the crystallization processing system Offers a more comprehensive approach to the topic than other titles. This will be the first resource to consult when consider design or optimization challenges.

Industrial Crystallization

Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen
Industrial Crystallization Book PDF

Author : Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen
Publisher : Cambridge University Press
Page : 353 pages
File Size : 55,5 Mb
Release : 2015-07-02
Category : Science
ISBN : 9781107052154

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Industrial Crystallization by Alison Lewis,Marcelo Seckler,Herman Kramer,Gerda van Rosmalen Pdf

A comprehensive overview of industrial crystallization, its theory and practice, including recent advances, real world case studies, and worked examples.

Crystallization

J W Mullin
Crystallization Book PDF

Author : J W Mullin
Publisher : Elsevier
Page : 600 pages
File Size : 51,7 Mb
Release : 2001-05-09
Category : Science
ISBN : 9780080530116

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Crystallization by J W Mullin Pdf

Since the first publication of this definitive work nearly 40 years ago, this fourth edition has been completely rewritten. Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. Incorporating all the recent developments and applications of crystallization technology, Crystallization gives clear accounts of the underlying principles, a review of the past and current research themes and guidelines for equipment and process design. This new edition introduces and enlarges upon such subjects as: Control and Separation of polymorphs and chiral crystals Micro- and macro-mixing and the use of computer fluid dynamics Seeding and secondary nucleation in batch crystallization processes Incorporation of upstream and downstream requirements into design procedures for crystallization plant Computer-aided molecular design and its use in crystal habit modifier selection Crystallization provides a comprehensive overview of the subject and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia. Crystallization is written with the precision and clarity of style that is John Mullin's hallmark - a special feature being the large number of appendices that provide relevant physical property data. Covers all new developments and trends in crystallization Comprehensive coverage of subject area

Conceptual Design of Crystallization Processes

Christianto Wibowo,Ka Ming Ng
Conceptual Design of Crystallization Processes Book PDF

Author : Christianto Wibowo,Ka Ming Ng
Publisher : Walter de Gruyter GmbH & Co KG
Page : 367 pages
File Size : 45,6 Mb
Release : 2020-11-23
Category : Technology & Engineering
ISBN : 9781501519901

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Conceptual Design of Crystallization Processes by Christianto Wibowo,Ka Ming Ng Pdf

The book presents, in a unified manner, various crystallization design methods. It discusses in detail the geometric framework for representing complex phase behavior involving multiple solutes, enantiomers, hydrates, compounds, polymorphs, and solid solutions through visualization of high-dimensional phase diagrams. It also describes how the impact of transport processes is accounted for using kinetically controlled process paths.

Advances in Industrial Crystallization

Heike Lorenz,Erik Temmel
Advances in Industrial Crystallization Book PDF

Author : Heike Lorenz,Erik Temmel
Publisher : MDPI
Page : 258 pages
File Size : 45,5 Mb
Release : 2021-06-15
Category : Science
ISBN : 9783036503301

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Advances in Industrial Crystallization by Heike Lorenz,Erik Temmel Pdf

This Special Issue is result of a call for papers of the Section Industrial Crystallization of MDPI’s scientific journal Crystals. It addresses scientists and engineers active in research and process & product development in life-science industries (e.g. pharmaceuticals, fine chemicals and biotechnology products) and bulk chemical applications (e.g. desalination) as well. The contributions comprise several fundamental and application-oriented facets of crystallization providing an overview of industrially relevant subjects in the field. Main issues cover phase equilibria and solid-state behavior of crystalline compounds, crystal shape and size and related measurement techniques. Melt and solution crystallization are considered specifically addressing contemporary aspects of continuous crystallization and process intensification.

Crystallization of Organic Compounds

Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Crystallization of Organic Compounds Book PDF

Author : Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley
Publisher : John Wiley & Sons
Page : 304 pages
File Size : 50,7 Mb
Release : 2009-06-17
Category : Science
ISBN : 9780470447789

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Crystallization of Organic Compounds by Hsien-Hsin Tung,Edward L. Paul,Michael Midler,James A. McCauley Pdf

Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.