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Author : D. Kealey
Publisher : Springer
Page : 92 pages
File Size : 49,9 Mb
Release : 2013-11-27
Category : Science
ISBN : 9781489966353
Author : S.N. Deming,S.L. Morgan
Publisher : Elsevier
Page : 285 pages
File Size : 41,6 Mb
Release : 1987-01-01
Category : Science
ISBN : 0080868304
Now available in a paperback edition is a book which has been described as ``...an exceptionally lucid, easy-to-read presentation... would be an excellent addition to the collection of every analytical chemist. I recommend it with great enthusiasm.'' (Analytical Chemistry). Unlike most current textbooks, it approaches experimental design from the point of view of the experimenter, rather than that of the statistician. As the reviewer in `Analytical Chemistry' went on to say: ``Deming and Morgan should be given high praise for bringing the principles of experimental design to the level of the practicing analytical chemist.''. The book first introduces the reader to the fundamentals of experimental design. Systems theory, response surface concepts, and basic statistics serve as a basis for the further development of matrix least squares and hypothesis testing. The effects of different experimental designs and different models on the variance-covariance matrix and on the analysis of variance (ANOVA) are extensively discussed. Applications and advanced topics (such as confidence bands, rotatability, and confounding) complete the text. Numerous worked examples are presented. The clear and practical approach adopted by the authors makes the book applicable to a wide audience. It will appeal particularly to those with a practical need (scientists, engineers, managers, research workers) who have completed their formal education but who still need to know efficient ways of carrying out experiments. It will also be an ideal text for advanced undergraduate and graduate students following courses in chemometrics, data acquisition and treatment, and design of experiments.
Author : David Harvey
Publisher : McGraw-Hill Science, Engineering & Mathematics
Page : 0 pages
File Size : 42,8 Mb
Release : 2000
Category : Analytical chemistry
ISBN : 0072375477
This introductory text covers both traditional and contemporary topics relevant to analytical chemistry. Its flexible approach allows instructors to choose their favourite topics of discussion from additional coverage of subjects such as sampling, kinetic method, and quality assurance.
Author : Robert L. Pecsok
Publisher : Unknown
Page : 135 pages
File Size : 50,8 Mb
Release : 1968
Category : Analisis quimico
ISBN : 0471676713
Author : Maurice O. Iwunze
Publisher : AuthorHouse
Page : 272 pages
File Size : 54,5 Mb
Release : 2005-08-09
Category : Science
ISBN : 9781468526042
Author : George W. Jr. Latimer
Publisher : Elsevier
Page : 295 pages
File Size : 44,8 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780323157308
Modern Experimental Chemistry provides techniques of qualitative analysis that reinforce experiments on ionic equilibriums. This book includes the determination of water in hydrated salts; identification of an organic compound after determining its molecular weight; and nonaqueous titration of a salt of a weak acid. The calculation of chemical stoichiometry; calculation of thermodynamic properties by determining the change in equilibrium with temperature; and chromium chemistry are also covered. This compilation contains enough experiments for classes which have six hours of laboratory (two 3-hour meetings) per week to last two semesters. This publication is intended for chemistry students as an introductory manual to chemistry laboratory.
Author : Peter C. Meier,Richard E. Zünd
Publisher : John Wiley & Sons
Page : 452 pages
File Size : 54,5 Mb
Release : 2005-03-04
Category : Science
ISBN : 9780471726111
This new edition of a successful, bestselling book continues to provide you with practical information on the use of statistical methods for solving real-world problems in complex industrial environments. Complete with examples from the chemical and pharmaceutical laboratory and manufacturing areas, this thoroughly updated book clearly demonstrates how to obtain reliable results by choosing the most appropriate experimental design and data evaluation methods. Unlike other books on the subject, Statistical Methods in Analytical Chemistry, Second Edition presents and solves problems in the context of a comprehensive decision-making process under GMP rules: Would you recommend the destruction of a $100,000 batch of product if one of four repeat determinations barely fails the specification limit? How would you prevent this from happening in the first place? Are you sure the calculator you are using is telling the truth? To help you control these situations, the new edition: * Covers univariate, bivariate, and multivariate data * Features case studies from the pharmaceutical and chemical industries demonstrating typical problems analysts encounter and the techniques used to solve them * Offers information on ancillary techniques, including a short introduction to optimization, exploratory data analysis, smoothing and computer simulation, and recapitulation of error propagation * Boasts numerous Excel files and compiled Visual Basic programs-no statistical table lookups required! * Uses Monte Carlo simulation to illustrate the variability inherent in statistically indistinguishable data sets Statistical Methods in Analytical Chemistry, Second Edition is an excellent, one-of-a-kind resource for laboratory scientists and engineers and project managers who need to assess data reliability; QC staff, regulators, and customers who want to frame realistic requirements and specifications; as well as educators looking for real-life experiments and advanced students in chemistry and pharmaceutical science. From the reviews of Statistical Methods in Analytical Chemistry, First Edition: "This book is extremely valuable. The authors supply many very useful programs along with their source code. Thus, the user can check the authenticity of the result and gain a greater understanding of the algorithm from the code. It should be on the bookshelf of every analytical chemist."-Applied Spectroscopy "The authors have compiled an interesting collection of data to illustrate the application of statistical methods . . . including calibrating, setting detection limits, analyzing ANOVA data, analyzing stability data, and determining the influence of error propagation."-Clinical Chemistry "The examples are taken from a chemical/pharmaceutical environment, but serve as convenient vehicles for the discussion of when to use which test, and how to make sense out of the results. While practical use of statistics is the major concern, it is put into perspective, and the reader is urged to use plausibility checks."-Journal of Chemical Education "The discussion of univariate statistical tests is one of the more thorough I have seen in this type of book . . . The treatment of linear regression is also thorough, and a complete set of equations for uncertainty in the results is presented . . . The bibliography is extensive and will serve as a valuable resource for those seeking more information on virtually any topic covered in the book."-Journal of American Chemical Society "This book treats the application of statistics to analytical chemistry in a very practical manner. [It] integrates PC computing power, testing programs, and analytical know-how in the context of good manufacturing practice/good laboratory practice (GMP/GLP) . . .The book is of value in many fields of analytical chemistry and should be available in all relevant libraries."-Chemometrics and Intelligent Laboratory Systems
Author : Donald T. Sawyer,William R. Heineman,Janice M. Beebe
Publisher : John Wiley & Sons
Page : 454 pages
File Size : 49,7 Mb
Release : 1984-09-03
Category : Science
ISBN : UOM:39015016061528
Potentiometric methods; Conductometric methods; Controlled potential methods (voltammetry); Electrolytic methods and controlled-current methods; Analytical ultraviolet-visible absorption spectroscopy; Absorption spectroscopy of electronic transitions; Infrared spectroscopy; Atomic absorption and atomic emission spectroscopy; Fluorescence spectroscopy; Nuclear magnetic resonance spectroscopy; Gas chromatography; High performance liquid chromatography (HPLC); Exclusion chromatography; Ion-exchange chromatography; Liquid-solid chromatography; Thin-layer chromatography (TCL); Electrophoresis.
Author : Benedict Bricker
Publisher : Unknown
Page : 272 pages
File Size : 45,8 Mb
Release : 2012-09
Category : Chemistry, Analytic
ISBN : 1781541795
No further information has been provided for this title.
Author : Peter J. T. Morris,Peter John Turnbull Morris,Royal Society of Chemistry (Great Britain)
Publisher : Royal Society of Chemistry
Page : 386 pages
File Size : 47,5 Mb
Release : 2002
Category : Science
ISBN : 0854044795
Most chemists today have either taken part in, or been affected by, the chemical revolution that has taken place over the course of the last century. Developments in instrumentation have changed not just what chemists do, but also how they think about chemistry. New and exciting areas of previously inaccessible research have been opened up as a direct result of this revolution. This is the first book to examine this instrumental revolution and goes on to assess the impact on chemical practice in areas ranging from organic chemistry and biochemistry to environmental analysis and process control, thus demonstrating how fundamental and extensive are the changes that have occurred. With contributions from internationally recognised specialists, this lavishly illustrated book provides a focal point for any historian of chemistry or chemist with an interest in this fascinating topic. This book is published in association with the Science Museum, London, UK and the Chemical Heritage Foundation, Philadelphia.
Author : Gary D. Christian
Publisher : Unknown
Page : 714 pages
File Size : 43,5 Mb
Release : 1986-01-17
Category : Science
ISBN : UOM:39015053939883
This is a practical approach to quantitative analytical chemistry, covering all areas of modern quantitative analysis taught in a standard first course in quantitative analysis. Includes experiments in each method. This edition includes coverage of electronic balance and propagation of error. Equilibria are introduced in terms of Gibbs free energy; buffers and calculations are presented in terms of photon acceptor/donor. Experiments are now all at the back of the book. SI units are emphasized throughout. Numerous applications to the life sciences.
Author : John Kenkel
Publisher : CRC Press
Page : 584 pages
File Size : 41,7 Mb
Release : 2002-10-29
Category : Science
ISBN : 1566705193
Surpassing its bestselling predecessors, this thoroughly updated third edition is designed to be a powerful training tool for entry-level chemistry technicians. Analytical Chemistry for Technicians, Third Edition explains analytical chemistry and instrumental analysis principles and how to apply them in the real world. A unique feature of this edition is that it brings the workplace of the chemical technician into the classroom. With over 50 workplace scene sidebars, it offers stories and photographs of technicians and chemists working with the equipment or performing the techniques discussed in the text. It includes a supplemental CD that enhances training activities. The author incorporates knowledge gained from a number of American Chemical Society and PITTCON short courses and from personal visits to several laboratories at major chemical plants, where he determined firsthand what is important in the modern analytical laboratory. The book includes more than sixty experiments specifically relevant to the laboratory technician, along with a Questions and Problems section in each chapter. Analytical Chemistry for Technicians, Third Edition continues to offer the nuts and bolts of analytical chemistry while focusing on the practical aspects of training.
Author : Dr Antonije E. Onjia
Publisher : Tehnološko-metalurški falkultet, Beograd, Institut za nuklearne nauke VINČA
Page : 151 pages
File Size : 53,5 Mb
Release : 2017-10-03
Category : Electronic
ISBN : 9788674013380
Author : Robert Bruce Thompson
Publisher : "O'Reilly Media, Inc."
Page : 432 pages
File Size : 46,5 Mb
Release : 2012-02-17
Category : Science
ISBN : 9781449331429
For students, DIY hobbyists, and science buffs, who can no longer get real chemistry sets, this one-of-a-kind guide explains how to set up and use a home chemistry lab, with step-by-step instructions for conducting experiments in basic chemistry -- not just to make pretty colors and stinky smells, but to learn how to do real lab work: Purify alcohol by distillation Produce hydrogen and oxygen gas by electrolysis Smelt metallic copper from copper ore you make yourself Analyze the makeup of seawater, bone, and other common substances Synthesize oil of wintergreen from aspirin and rayon fiber from paper Perform forensics tests for fingerprints, blood, drugs, and poisons and much more From the 1930s through the 1970s, chemistry sets were among the most popular Christmas gifts, selling in the millions. But two decades ago, real chemistry sets began to disappear as manufacturers and retailers became concerned about liability. ,em>The Illustrated Guide to Home Chemistry Experiments steps up to the plate with lessons on how to equip your home chemistry lab, master laboratory skills, and work safely in your lab. The bulk of this book consists of 17 hands-on chapters that include multiple laboratory sessions on the following topics: Separating Mixtures Solubility and Solutions Colligative Properties of Solutions Introduction to Chemical Reactions & Stoichiometry Reduction-Oxidation (Redox) Reactions Acid-Base Chemistry Chemical Kinetics Chemical Equilibrium and Le Chatelier's Principle Gas Chemistry Thermochemistry and Calorimetry Electrochemistry Photochemistry Colloids and Suspensions Qualitative Analysis Quantitative Analysis Synthesis of Useful Compounds Forensic Chemistry With plenty of full-color illustrations and photos, Illustrated Guide to Home Chemistry Experiments offers introductory level sessions suitable for a middle school or first-year high school chemistry laboratory course, and more advanced sessions suitable for students who intend to take the College Board Advanced Placement (AP) Chemistry exam. A student who completes all of the laboratories in this book will have done the equivalent of two full years of high school chemistry lab work or a first-year college general chemistry laboratory course. This hands-on introduction to real chemistry -- using real equipment, real chemicals, and real quantitative experiments -- is ideal for the many thousands of young people and adults who want to experience the magic of chemistry.
Author : Todd M. Schuster,Thomas M. Laue
Publisher : Springer Science & Business Media
Page : 359 pages
File Size : 51,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781468468281
There are numerous examples in the history of science when the parallel develop ments of two or more disciplines, methodologies, technologies or theoretical in sights have converged to produce significant scientific advances. The decades following the 1950s have produced several such significant advances, as a result of a convergence of developments in molecular biology and in solid state-based electronics instrumentation. Since one of these areas of significant advancement, analytical ultracentrifu gation, has been undergoing a renaissance, we thought it would be a useful activity to call upon a group of researchers who have been developing either the experi mental or theoretical aspects of the methodology and gather in one place a group of articles summarizing the current status of the field. The success of recombinant DNA methodologies at producing biologically active macromolecules of commer cial interest has evoked interests in mechanisms of function. Pursuit of the related questions has emphasized the importance of studies of macromolecular binding and interaction. Several contributions to this volume remind us that analytical ultra centrifugation is rigorously based on solid thermodynamic theory and, as such, is fully capable of providing comprehensive quantitative descriptions of molecular interactions in solution. Furthermore, a number of the chapters provide examples, along with innovative methods for carrying out these characterizations. The past decade has seen several developments that reflect the rebirth of interest in analytical ultracentrifugation.