High Pressure Experimental Methods

Author : M. I. Eremets
Publisher : Oxford University Press on Demand
Page : 390 pages
File Size : 50,8 Mb
Release : 1996
Category : Science
ISBN : 0198562691

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High Pressure Experimental Methods by M. I. Eremets Pdf

The properties of materials are altered, sometimes radically, when very high pressures are applied. This book surveys the apparatus available for high pressure studies with a particular emphasis on diamond anvil cells and related equipment. It also examines pressure measurement techniques atextreme values. A large part of the book considers the experimental needs and arrangement for studies involving the interaction of high pressures with high and low temperatures, magnetic fields, and shock waves. Optical properties, Brillouin and Raman scattering, infrared spectroscopy, eletronspin and nuclear magnetic resonance at high pressures are also covered.

Author : W. F. Sherman,A. A. Stadtmuller
Publisher : Unknown
Page : 496 pages
File Size : 51,7 Mb
Release : 1987
Category : Science
ISBN : STANFORD:36105030461128

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Experimental Techniques in High Pressure Research by W. F. Sherman,A. A. Stadtmuller Pdf

This book is divided into two sections - the first dealing with the components that work up the high pressure system and the second with the experiments that may be performed with high pressure equipment of relevance to a wide range of disciplines.

Author : G. C. Ulmer
Publisher : Springer Science & Business Media
Page : 368 pages
File Size : 41,7 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642880971

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Research Techniques for High Pressure and High Temperature by G. C. Ulmer Pdf

Within the last two decades, the experimental technology for the study of high temperature solid-vapor and liquid-vapor equilibria has mushroomed so fast that· both academic and industrial research ers desirous of working in this field -- be they physical chemists, metallurgists, ceramists, petrologists, crystal chemists, or mem bers of any of the several branches of materials science -- find themselves in the situation that in order to learn the art of the latest techniques, a period of apprenticeship or residency needs be spent at an institution or laboratory currently engaged in this type of solid-vapor or liquid-vapor research. The tech niques for control of the vapor phase at total pressures of one atmosphere or greater have not been well defined in the literature. Therefore, the purpose of this volume will be to serve as a labora tory manual for the control, calibration, and measurement of high temperature-high pressure equilibria. The avowed aims of this treatment of experimental techniques are: (1) to give, in terms understandable at the graduate student level, the laboratory procedures necessary to the design and utilization of good experimental technique, (2) to list the limitations, dangers, and technical pitfalls inherent or intrinsic to the described techniques, (3) to give theory and specific data only where they are essential to the experimental design, (4) to give with each chapter references that are extensive enough to serve as a bibliography of the state-of-the-art of technique development within the last decade.

Author : Stefan Klotz
Publisher : CRC Press
Page : 274 pages
File Size : 41,7 Mb
Release : 2012-12-04
Category : Science
ISBN : 9781439835630

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Techniques in High Pressure Neutron Scattering by Stefan Klotz Pdf

Drawing on the author's practical work from the last 20 years, Techniques in High Pressure Neutron Scattering is one of the first books to gather recent methods that allow neutron scattering well beyond 10 GPa. The author shows how neutron scattering has to be adapted to the pressure range and type of measurement.Suitable for both newcomers and exp

Author : Wilfried B. Holzapfel,Neil S. Isaacs
Publisher : Oxford University Press on Demand
Page : 388 pages
File Size : 54,5 Mb
Release : 1997
Category : Science
ISBN : 0198558112

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High Pressure Techniques in Chemistry and Physics by Wilfried B. Holzapfel,Neil S. Isaacs Pdf

This volume provides a practical introduction to the use of high-pressure techniques in chemistry and physics. The authors provide details of the experimental methods and equipment needed to carry out observations and measurements at very high pressures. The pressures involved range from a fewthousand bars for some chemical studies to hundreds of thousands of bars for some physical experimentation.High-pressure techniques may be used to learn more about the structure of matter and mechanisms of chemical reactions. This volume includes detailed descriptions of equipment to measure the following criteria under high pressure conditions: compressibility and equations of state; dielectricconstants and conductance; viscocity; X-ray and neutron diffraction; optical absorption and luminescence; Mossbauer spectra; NMR. IR. and UV spectra; molecular dynamics; kinetics; organic and inorganic synthesis; electro-chemistry and electrophoresis. Applications such as the preservation of foodare also discussed.High-pressure techniques in chemistry and physics: a practical approach is a comprehensive and detailed guide for all those engaged in high-pressure research and a valuable source of information for newcomers to the field. Each chapter contains useful toptics on specific equipment and techniques, aswell as step-by-step protocols, essential background information, and key citations in the literature.

Author : Scott S Bair
Publisher : Elsevier
Page : 260 pages
File Size : 47,5 Mb
Release : 2007-03-06
Category : Technology & Engineering
ISBN : 0080475302

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High Pressure Rheology for Quantitative Elastohydrodynamics by Scott S Bair Pdf

Computational elastohydrodynamics, a part of tribology, has existed happily enough for about fifty years without the use of accurate models for the rheology of the liquids used as lubricants. For low molecular weight liquids, such as low viscosity mineral oils, it has been possible to calculate, with precision, the film thickness in a concentrated contact provided that the pressure and temperature are relatively low, even when the pressure variation of viscosity is not accurately modelled in detail. Other successes have been more qualitative in nature, using effective properties which come from the fitting of parameters used in calculations to experimental measurements of the contact behaviour, friction or film thickness. High Pressure Rheology for Quantitative Elastohydrodynamics is intended to provide a sufficiently accurate framework for the rheology of liquids at elevated pressure that it may be possible for computational elastohydrodynamics to discover the relationships between the behaviour of a lubricated concentrated contact and the measurable properties of the liquid lubricant. The required high-pressure measurement techniques are revealed in detail and data are presented for chemically well-defined liquids that may be used as quantitative reference materials. * Presents the property relations required for a quantitative calculation of the tribological behaviour of lubricated concentrated contacts. * Details of high-pressure experimental techniques. * Complete description of the pressure and temperature dependence of viscosity for high pressures. * Some little-known limitations on EHL modelling.

Author : W. F. Sherman
Publisher : Unknown
Page : 481 pages
File Size : 52,8 Mb
Release : 2024-06-29
Category : Electronic
ISBN : 0608220167

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Experimental Techniques in High-Pressure Research by W. F. Sherman Pdf

Author : Andrzej Katrusiak,Paul McMillan
Publisher : Springer Science & Business Media
Page : 574 pages
File Size : 54,9 Mb
Release : 2004-03-31
Category : Science
ISBN : 9781402021022

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High-Pressure Crystallography by Andrzej Katrusiak,Paul McMillan Pdf

Despite the tremendous advances in the techniques and equipment for carrying out high-pressure crystallography, the application or exploration of the high-pressure variable in detailed structural studies remains rare. The chapters in this book provide a set of lecture notes and supplementary material for a course on high pressure crystallography. The material comprises state-of-the-art reviews of high-pressure experiments using X-ray and neutron diffraction techniques at synchrotron and neutron facilities and in the laboratory, as well as complementary experimental high-pressure techniques and theoretical methods for investigating matter at elevated pressures. The materials studies range from elemental solids and liquids to inorganic compounds, minerals, organic compounds, clathrates and pharmaceutical compounds, to large biological molecules such as proteins and viruses. The book provides a reference for workers in high-pressure science wishing to learn more about crystallography and for established crystallographers potentially interested in high pressure as a variable, as well as an introductory guide to new researchers in the field.

Author : John Loveday
Publisher : CRC Press
Page : 344 pages
File Size : 43,7 Mb
Release : 2012-06-06
Category : Science
ISBN : 9781439814284

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High-Pressure Physics by John Loveday Pdf

High-pressure science has undergone a revolution in the last 15 years. The development of intense new x-ray and neutron sources, improved detectors, new instrumentation, greatly increased computation power, and advanced computational algorithms have enabled researchers to determine the behavior of matter at static pressures in excess of 400 GPa. Shock-wave techniques have allowed access to the experimental pressure-temperature range beyond 1 TPa and 10,000 K. High-Pressure Physics introduces the current state of the art in this field. Based on lectures presented by leading researchers at the 63rd Scottish Universities Summer School in Physics, the book summarizes the latest experimental and theoretical techniques. Highlighting applications in a range of physics disciplines—from novel materials synthesis to planetary interiors—this book cuts across many areas and supplies a solid grounding in high-pressure physics. Chapters cover a wide array of topics and techniques, including: High-pressure devices The design of pressure cells Electrical transport experiments The fabrication process for customizing diamond anvils Equations of state (EOS) for solids in a range of pressures and temperatures Crystallography, optical spectroscopy, and inelastic x-ray scattering (IXS) techniques Magnetism in solids The internal structure of Earth and other planets Measurement and control of temperature in high-pressure experiments Solid state chemistry and materials research at high pressure Liquids and glasses The study of hydrogen at high density A resource for graduate students and young researchers, this accessible reference provides an overview of key research areas and applications in high-pressure physics.

Author : Elena Boldyreva,Przemyslaw Dera
Publisher : Springer Science & Business Media
Page : 603 pages
File Size : 41,6 Mb
Release : 2010-08-20
Category : Science
ISBN : 9789048192571

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High-Pressure Crystallography by Elena Boldyreva,Przemyslaw Dera Pdf

This unique book is devoted to the theme of crystallographic studies at high pressure. It places emphasis on the phenomena characteristic to the compressed state of matter, as well as experimental and theoretical techniques, used to study these phenomena.

Author : G. T. Hefter,R. P. T. Tomkins
Publisher : John Wiley & Sons
Page : 657 pages
File Size : 42,6 Mb
Release : 2003-08-01
Category : Science
ISBN : 9780471497080

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The Experimental Determination of Solubilities by G. T. Hefter,R. P. T. Tomkins Pdf

* Guidelines are provided on the reliability of various methods, as well as information for selecting the appropriate technique. * Unique coverage of the whole range of solubility measurements. * Very useful for investigators interested in embarking upon solubility measurements.

Author : Gregory S. Patience
Publisher : Elsevier
Page : 426 pages
File Size : 40,7 Mb
Release : 2017-09-08
Category : Science
ISBN : 9780444637925

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Experimental Methods and Instrumentation for Chemical Engineers by Gregory S. Patience Pdf

Experimental Methods and Instrumentation for Chemical Engineers, Second Edition, touches many aspects of engineering practice, research, and statistics. The principles of unit operations, transport phenomena, and plant design constitute the focus of chemical engineering in the latter years of the curricula. Experimental methods and instrumentation is the precursor to these subjects. This resource integrates these concepts with statistics and uncertainty analysis to define what is necessary to measure and to control, how precisely and how often.The completely updated second edition is divided into several themes related to data: metrology, notions of statistics, and design of experiments. The book then covers basic principles of sensing devices, with a brand new chapter covering force and mass, followed by pressure, temperature, flow rate, and physico-chemical properties. It continues with chapters that describe how to measure gas and liquid concentrations, how to characterize solids, and finally a new chapter on spectroscopic techniques such as UV/Vis, IR, XRD, XPS, NMR, and XAS. Throughout the book, the author integrates the concepts of uncertainty, along with a historical context and practical examples.A problem solutions manual is available from the author upon request. Includes the basics for 1st and 2nd year chemical engineers, providing a foundation for unit operations and transport phenomena Features many practical examples Offers exercises for students at the end of each chapter Includes up-to-date detailed drawings and photos of equipment

Author : Rudolf Eggers
Publisher : John Wiley & Sons
Page : 408 pages
File Size : 44,9 Mb
Release : 2012-07-11
Category : Technology & Engineering
ISBN : 9783527652679

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Industrial High Pressure Applications by Rudolf Eggers Pdf

Industrial high pressure processes open the door to many reactions that are not possible under 'normal' conditions. These are to be found in such different areas as polymerization, catalytic reactions, separations, oil and gas recovery, food processing, biocatalysis and more. The most famous high pressure process is the so-called Haber-Bosch process used for fertilizers and which was awarded a Nobel prize. Following an introduction on historical development, the current state, and future trends, this timely and comprehensive publication goes on to describe different industrial processes, including methanol and other catalytic syntheses, polymerization and renewable energy processes, before covering safety and equipment issues. With its excellent choice of industrial contributions, this handbook offers high quality information not found elsewhere, making it invaluable reading for a broad and interdisciplinary audience.

Author : Allen F. Donovan
Publisher : Princeton University Press
Page : 1021 pages
File Size : 43,6 Mb
Release : 2015-12-08
Category : Science
ISBN : 9781400875030

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High Speed Problems of Aircraft and Experimental Methods by Allen F. Donovan Pdf

Volume VIII of the High Speed Aerodynamics and Jet Propulsion series. This volume includes: performance calculation at high speed; stability and control of high speed aircraft; aeroelasticity and flutter; model testing; transonic wind tunnels; supersonic tunnels; hypersonic experimental facilities; low density wind tunnels; shock tube; wind tunnel measurements; instrumented models in free flight; piloted aircraft testing; free flight range methods. Originally published in 1961. The Princeton Legacy Library uses the latest print-on-demand technology to again make available previously out-of-print books from the distinguished backlist of Princeton University Press. These editions preserve the original texts of these important books while presenting them in durable paperback and hardcover editions. The goal of the Princeton Legacy Library is to vastly increase access to the rich scholarly heritage found in the thousands of books published by Princeton University Press since its founding in 1905.

Author : Mikhail Adolʹfovich Styrikovich
Publisher : Unknown
Page : 292 pages
File Size : 47,8 Mb
Release : 1961
Category : Heat
ISBN : UVA:X001029899

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Hydrodynamics and Heat Transfer During Boiling in High-pressure Boilers by Mikhail Adolʹfovich Styrikovich Pdf