Multinuclear Magnetic Resonance In Liquids And Solids Chemical Applications

Author : P. Granger,Robin K. Harris
Publisher : Springer Science & Business Media
Page : 473 pages
File Size : 40,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9789400921498

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Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications by P. Granger,Robin K. Harris Pdf

The idea of this NATO school was born during philosophical discussions with Dr Brevard on the present and future of NMR during a night walk under the palm trees in Biskra during a seminar held in this oasis. It was clear for us that the recent progress in the field of NMR, especially inverse spectroscopy and the development of MAS, was opening new perspectives for chemists. We realised also that organometallic and inorganic chemists were not clearly informed about the potentialities of all the new methods. NA TO, with its summer schools, was offering a good opportunity to propose to the chemical community a session where those problems would be largely developped. This School is then the prolongation of the two previous ones: Palermo in 1976 on "the less receptive nuclei" and Stirling in 1982 on "the multinuclear approach to NMR spectroscopy" . It was divided into two sub-sessions: NMR in the liquid state and NMR in the solid state. This is reflected in the book organization. As indicated by the title of this School, we were mainly concerned with the methodological aspects of multinuclear NMR. If many examples are given, they appear only as a support for the understanding of the theory or in explanation of some practical aspects of the different experiments. Each domain is introduced by a lecture which presents selected examples.

Author : P Granger,Robin K Harris
Publisher : Unknown
Page : 492 pages
File Size : 41,9 Mb
Release : 1990-10-31
Category : Electronic
ISBN : 9400921500

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Multinuclear Magnetic Resonance in Liquids and Solids - Chemical Applications by P Granger,Robin K Harris Pdf

Author : Kenneth J.D. MacKenzie,M.E. Smith
Publisher : Elsevier
Page : 748 pages
File Size : 53,8 Mb
Release : 2002-04-26
Category : Science
ISBN : 9780080537108

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Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by Kenneth J.D. MacKenzie,M.E. Smith Pdf

Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Author : G Davidson
Publisher : Royal Society of Chemistry
Page : 474 pages
File Size : 52,9 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847555090

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G Davidson Pdf

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Author : L. M. Jackman,S. Sternhell
Publisher : Elsevier
Page : 474 pages
File Size : 42,8 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483280943

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Applications of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry by L. M. Jackman,S. Sternhell Pdf

Application of Nuclear Magnetic Resonance Spectroscopy in Organic Chemistry, Second Edition covers the theoretical background necessary for the intelligent application of NMR spectroscopy to common problems encountered in organic chemistry. This book is composed of five parts, and begins with introduction to the theory and practice of nuclear magnetic resonance. The succeeding chapter deals with the theory of chemical effects in NMR spectroscopy. These topics are followed by a discussion on the application of chemical shift to organic compound analysis and the principles of the spin-spin coupling .The final chapter considers the applications of time- dependent phenomena in NMR spectroscopy. This book will prove useful to analytical chemists and researchers in the allied fields.

Author : J. Fraissard,Olga Lapina
Publisher : Springer Science & Business Media
Page : 652 pages
File Size : 43,5 Mb
Release : 2012-12-06
Category : Science
ISBN : 9789401005340

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Magnetic Resonance in Colloid and Interface Science by J. Fraissard,Olga Lapina Pdf

Magnetic resonance techniques are especially interesting in the study of colloids and interfaces due to their unique ability to elucidate structure, dynamics and function at the atomic and molecular level. This book illustrates the most up to date applications of innovative NMR and EPR techniques, including magnetic resonance imaging and microscopy, to gas-solid and liquid-solid interfaces, organic and biological surfaces, microemulsions, liquid crystals, membranes, structure and dynamics of polymers and micellar systems, and diffusion in heterogeneous systems. A compendium of advanced NMR and EPR techniques and a state of the art description of the power of advanced new methodologies for the study of molecular dynamics and interfaces.

Author : R. Tycko
Publisher : Springer Science & Business Media
Page : 576 pages
File Size : 41,5 Mb
Release : 2003-07-31
Category : Medical
ISBN : 1402014597

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Nuclear Magnetic Resonance Probes of Molecular Dynamics by R. Tycko Pdf

Nuclear Magnetic Resonance Probes of Molecular Dynamics describes the theoretical basis and experimental techniques that make modern NMR spectroscopy a powerful and flexible tool for probing molecular dynamics in chemical, physical, and biochemical systems. Individual chapters, written by leaders in the development and application of NMR from around the world, treat systems that range from synthetic polymers, liquid crystals, and catalysts to proteins and oligonucleotides and techniques that include deuterium NMR, magic angle spinning, multidimensional spectroscopy, and magnetic resonance imaging. A combination of elementary and advanced material makes the book a useful introduction to the field for students at the graduate level as well as an important reference for practising NMR spectroscopists.

Author : Atta-ur- Rahman
Publisher : Taylor & Francis
Page : 1274 pages
File Size : 50,6 Mb
Release : 2000
Category : Biography & Autobiography
ISBN : 9058230317

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New Advances in Analytical Chemistry by Atta-ur- Rahman Pdf

Presenting recent developments in various spectroscopic techniques such as NMR Spectroscopy, mass spectroscopy etc. in the form of comprehensive reviews written by leading authorities in the field. This monograph should prove exceedingly useful to both research students and postdoctoral workers who wish to keep abreast with frontiers in analytical techniques.

Author : G. Batta,K. Kövér,C. Szántay, Jr.
Publisher : Elsevier
Page : 356 pages
File Size : 55,8 Mb
Release : 1997-12-04
Category : Science
ISBN : 0080536506

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Methods for Structure Elucidation by High-Resolution NMR by G. Batta,K. Kövér,C. Szántay, Jr. Pdf

Nuclear Magnetic Resonance Spectroscopy (NMR) is now widely regarded as having evolved into a subscience. The field has become immensely diverse, ranging from medical use through solid state NMR to liquid state applications, with countless books and scientific journals devoted to these topics. Theoretical as well as experimental advance continues to be rapid, and has in fact accelerated by many novel innovations. This multi-authored book focuses on the latest developments in the rapidly evolving field of high resolution NMR, specifically with a view to applications on the structure elucidation of organic molecules of moderate molecular weight. Conceptually it differs from basic educational texts, hard-core scientific papers and regular review articles in that each chapter may be regarded as the authors' personal account of their special insights and results that crystallised after several years of research into a given topic. The book revolves around several themes and offers a handful of scientific "gems" of various colors, reflecting the great diversity of NMR. It contains 16 loosely connected chapters written by some of today's most accomplished NMR scientists in the world. Each chapter is a unique synthesis of the authors' previous research results in the given field, and thus projects special insights. Much emphasis has been given to the latest developments in NMR, in particular to selective pulses and pulsed field gradients. As a part of the series "Analytical Spectroscopy Library", with subsequent editions coming along this book should provide a platform for future research accounts of similar flavor. The material is presented in a mostly non-mathematical fashion, and is intended mainly for chemists, application NMR scientists and students with already some background in NMR. Some of the chapters slightly overlap in the discussed topics, which is particularly exciting in terms of gaining insight into the same area from different angles.

Author : D. M. P. Mingos
Publisher : Springer Science & Business Media
Page : 202 pages
File Size : 44,7 Mb
Release : 2004-01-28
Category : Science
ISBN : 3540200843

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Supramolecular Assembly Via Hydrogen Bonds I by D. M. P. Mingos Pdf

Author : Melinda J. Duer
Publisher : John Wiley & Sons
Page : 592 pages
File Size : 49,8 Mb
Release : 2008-04-15
Category : Science
ISBN : 9780470999387

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Solid State NMR Spectroscopy by Melinda J. Duer Pdf

This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of the material within each chapter. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. The basic techniques that all chapters rely on are collected into a second chapter to avoid unnecessary repetition later. Remaining chapters in the "Fundamentals" part deal with the major areas of solid-state NMR which all solid-state NMR spectroscopists should know about. Each begins with an overview of the topic that puts the chapter in context. The basic principles upon which the techniques in the chapter rely are explained in a separate section. Each of these chapters exemplifies the principles and techniques with the applications most commonly found in current practice. The "Further Applications" section contains a series of shorter chapters which describe the NMR techniques used in other, more specific areas. The basic principles upon which these techniques rely will be expounded only if not already in the Fundamentals part.

Author : A.T. Peters,J. Szep
Publisher : Springer Science & Business Media
Page : 223 pages
File Size : 51,7 Mb
Release : 2013-03-09
Category : Science
ISBN : 9789401113588

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Analytical Chemistry of Synthetic Colorants by A.T. Peters,J. Szep Pdf

More than one and a half decades have passed since the last book was published describing developments in the analytical chemistry of synthetic colorants. In the intervening period, the scope and technical capabilities of instrumentation for analysing dyes and pigments has significantly expanded. It is now possible to rapidly resolve a number of problems whose solutions were previously either unattainable or very difficult to achieve. For instance, the unambiguous assignment of all the signals in the proton NMR spectrum of a trisazo direct dye, and the confirmation of the molecular weight of involatile, and, in particular, sulphonated dyes, without derivatisation, are now routine analytical techniques in many laboratories today. In addition, it is now possible to record the NMR spectrum of a dye molecule on less than 1 mg of material, and we are no longer limited to solution spectra, since solid samples can now be routinely analysed in NMR experiments. Whilst not attempting to be all encompassing, this volume is intended to bridge the gap between what was covered in the earlier work edited by Professor Venkataraman and the developments which have since ensued in some key areas. It provides important updates in X-ray crystallography, proton NMR, IR spectroscopy and mass spectrometry, and additionally covers topics such as ESR, micro spectrophotometry and emission spectroscopy.

Author : Graham A. Webb
Publisher : Academic Press
Page : 376 pages
File Size : 40,5 Mb
Release : 2014-07-22
Category : Science
ISBN : 9780128003275

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Annual Reports on NMR Spectroscopy by Graham A. Webb Pdf

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. This volume of Annual Reports on NMR Spectroscopy focuses on the analytical tools used by chemists and physicists, taken together with other volumes of this series, an excellent account of progress in NMR and its many applications is provided and anyone using NMR will find interest in this Serial

Author : G A Webb
Publisher : Royal Society of Chemistry
Page : 616 pages
File Size : 48,5 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847553775

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Nuclear Magnetic Resonance by G A Webb Pdf

As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Author : Vladimir I. Bakhmutov
Publisher : CRC Press
Page : 0 pages
File Size : 40,5 Mb
Release : 2015-04-10
Category : Medical
ISBN : 1482262703

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NMR Spectroscopy in Liquids and Solids by Vladimir I. Bakhmutov Pdf

NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics. The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR— including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.