Solid State Nmr Spectroscopy

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Solid State NMR

Klaus Müller,Marco Geppi
Solid State NMR Book PDF

Author : Klaus Müller,Marco Geppi
Publisher : John Wiley & Sons
Page : 562 pages
File Size : 42,9 Mb
Release : 2021-08-23
Category : Science
ISBN : 9783527318162

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Solid State NMR by Klaus Müller,Marco Geppi Pdf

Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.

Solid State NMR Spectroscopy

Melinda J. Duer
Solid State NMR Spectroscopy Book PDF

Author : Melinda J. Duer
Publisher : John Wiley & Sons
Page : 592 pages
File Size : 45,8 Mb
Release : 2008-04-15
Category : Science
ISBN : 9780470999387

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Solid State NMR Spectroscopy by Melinda J. Duer Pdf

This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details. This dual requirement is met through careful construction of the material within each chapter. The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR. The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. The basic techniques that all chapters rely on are collected into a second chapter to avoid unnecessary repetition later. Remaining chapters in the "Fundamentals" part deal with the major areas of solid-state NMR which all solid-state NMR spectroscopists should know about. Each begins with an overview of the topic that puts the chapter in context. The basic principles upon which the techniques in the chapter rely are explained in a separate section. Each of these chapters exemplifies the principles and techniques with the applications most commonly found in current practice. The "Further Applications" section contains a series of shorter chapters which describe the NMR techniques used in other, more specific areas. The basic principles upon which these techniques rely will be expounded only if not already in the Fundamentals part.

Modern Methods in Solid-state NMR

Paul Hodgkinson
Modern Methods in Solid state NMR Book PDF

Author : Paul Hodgkinson
Publisher : Royal Society of Chemistry
Page : 452 pages
File Size : 46,9 Mb
Release : 2018-04-05
Category : Science
ISBN : 9781788014199

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Modern Methods in Solid-state NMR by Paul Hodgkinson Pdf

Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the “practical aspects” of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of “NMR crystallography” – the use of solids NMR as a complement to diffraction crystallography. This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.

Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials

Kenneth J.D. MacKenzie,M.E. Smith
Multinuclear Solid State Nuclear Magnetic Resonance of Inorganic Materials Book PDF

Author : Kenneth J.D. MacKenzie,M.E. Smith
Publisher : Elsevier
Page : 748 pages
File Size : 43,9 Mb
Release : 2002-04-26
Category : Science
ISBN : 9780080537108

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Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by Kenneth J.D. MacKenzie,M.E. Smith Pdf

Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Solid-State NMR in Materials Science

Vladimir I. Bakhmutov
Solid State NMR in Materials Science Book PDF

Author : Vladimir I. Bakhmutov
Publisher : CRC Press
Page : 283 pages
File Size : 49,5 Mb
Release : 2011-12-19
Category : Science
ISBN : 9781439869635

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Solid-State NMR in Materials Science by Vladimir I. Bakhmutov Pdf

Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often responsible for complex systems mechanical properties. Written for non-specialists, Solid-State NMR in Materials Science: Principles and Applications introduces the general physical principles of pulsed NMR, by including elements of the theory and practice in the registration of NMR signals, and by explaining different NMR equipment. After the preliminaries, the book covers: The theory and features of solid-state NMR and nuclear relaxation in solids, including dynamics of materials Different materials, diamagnetic and paramagnetic, from metals and metal clusters to amorphous composites The methodology of collection and interpretations of solid-state NMR data, including strategies and criteria for structural characterizations of different materials Practical examples of multinuclear NMR and relaxation experiments as well as interpretations of data obtained Numerous solid-state NMR experiments performed for various materials to evaluate their structure and dynamics Written in clear and simple language, this book includes clear illustrations, numerous examples, and detailed bibliographies. It an excellent reference not only for young and experienced researchers, but also for students interested in a future in materials science.

Solid State NMR of Polymers

T. Asakura,Isao Ando
Solid State NMR of Polymers Book PDF

Author : T. Asakura,Isao Ando
Publisher : Elsevier
Page : 1017 pages
File Size : 41,6 Mb
Release : 1998-08-03
Category : Science
ISBN : 9780080541464

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Solid State NMR of Polymers by T. Asakura,Isao Ando Pdf

In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described. Features of this book: • Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field • Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists. This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

Solid State NMR Spectroscopy for Biopolymers

Hazime Saitô,Isao Ando,Akira Naito
Solid State NMR Spectroscopy for Biopolymers Book PDF

Author : Hazime Saitô,Isao Ando,Akira Naito
Publisher : Springer Science & Business Media
Page : 455 pages
File Size : 43,6 Mb
Release : 2006-08-05
Category : Science
ISBN : 9781402043031

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Solid State NMR Spectroscopy for Biopolymers by Hazime Saitô,Isao Ando,Akira Naito Pdf

‘‘Biopolymers’’ are polymeric materials of biological origin, including globular, membrane, and fibrous proteins, polypeptides, nucleic acids, po- saccharides, lipids, etc. and their assembly, although preference to respe- ive subjects may be different among readers who are more interested in their biological significance or industrial and/or medical applications. Nevert- less, characterizing or revealing their secondary structure and dynamics may be an equally very important and useful issue for both kinds of readers. Special interest in revealing the 3D structure of globular proteins, nucleic acids, and peptides was aroused in relation to the currently active Structural Biology. X-ray crystallography and multidimensional solution NMR sp- troscopy have proved to be the standard and indispensable means for this purpose. There remain, however, several limitations to this end, if one intends to expand its scope further. This is because these approaches are not always straightforward to characterize fibrous or membrane proteins owing to extreme difficulty in crystallization in the former, and insufficient spectral resolution due to sparing solubility or increased effective molecular mass in the presence of surrounding lipid bilayers in the latter.

Solid-State NMR

David C. Apperley,Robin K. Harris,Paul Hodgkinson
Solid State NMR Book PDF

Author : David C. Apperley,Robin K. Harris,Paul Hodgkinson
Publisher : Momentum Press
Page : 280 pages
File Size : 49,8 Mb
Release : 2012-06-10
Category : Technology & Engineering
ISBN : 9781606503522

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Solid-State NMR by David C. Apperley,Robin K. Harris,Paul Hodgkinson Pdf

The power of nuclear magnetic resonance, NMR, for characterizing molecules dissolved in solution is widely acknowledged and NMR forms an essential component of undergraduate chemistry degrees. However, the application of NMR to the solid state is much less well appreciated. This text sets out the fundamental principles of solid-state NMR, explaining how NMR in solids differs from that in solution, showing how the various interactions of NMR can be manipulated to yield high-resolution spectra and to give information on local structure and dynamics in solids. This book aims to take some of the mystique out of solid-state NMR by providing a comprehensible discussion of the methodology, including the basic concepts and a practical guide to implementation of the experiments. A basic knowledge of solution-state NMR is assumed and is only briefly covered. The text is intended for those in academia and industry expecting to use solid-state NMR in their research and looking for an accessible introduction to the field. It will also be valuable for non-experts interested in learning how NMR can be usefully applied to solid systems. Detailed mathematical treatments are delayed to a chapter at the mid-point of the text and can be skipped. Introductions to experiments and numerical simulations are provided to help link NMR results to experimental practice. The different aspects of solid-state NMR, from basic pulse-and-acquire experiments to sophisticated techniques for the measurement of anisotropy information are presented. Examples illustrate the wide variety of applications of the technique and its complementarity to other solid-state characterization techniques such as X-ray diffraction. Various aspects of NMR crystallography are covered as are topics of motion in solids.

Current Developments in Solid State NMR Spectroscopy

Norbert Müller,Perunthiruthy K. Madhu
Current Developments in Solid State NMR Spectroscopy Book PDF

Author : Norbert Müller,Perunthiruthy K. Madhu
Publisher : Springer Science & Business Media
Page : 143 pages
File Size : 47,5 Mb
Release : 2013-04-17
Category : Science
ISBN : 9783709137154

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Current Developments in Solid State NMR Spectroscopy by Norbert Müller,Perunthiruthy K. Madhu Pdf

Why to apply solid-state NMR? - By now, we should have learned that NMR is mainly used for the study of molecules in solution, while x-ray diffraction is the method of choice for solids. Based on this fact, the two recent 'NMR-Nobelprizes' went indeed into the liquid phase: my own one eleven years ago, and particularly the most recent one to Kurt Wuthrich. His prize is beyond any doubts very well justified. His contribution towards the study of biomolecules in solution, in their native (or almost native) environment is truly monumental. We all will profit from it indirectly when one of our future diseases will be cured with better drugs, based on the insightful knowledge gained through liquid-state NMR. Two fields of NMR are still left out of the Nobel Prize game: magnetic reso nance imaging (MRI) and solid-state NMR. The disrespect for MRI in Stockholm is particularly difficult to understand; but this is not a subject to be discussed at the present place. Solid-state NMR is the third of the three great fields of NMR, powerful already today and very promising for the near future.

Solid-state NMR Spectroscopy of Inorganic Materials

John J. Fitzgerald,American Chemical Society. Meeting
Solid state NMR Spectroscopy of Inorganic Materials Book PDF

Author : John J. Fitzgerald,American Chemical Society. Meeting
Publisher : Unknown
Page : 440 pages
File Size : 48,6 Mb
Release : 1999
Category : Medical
ISBN : UOM:39015043093916

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Solid-state NMR Spectroscopy of Inorganic Materials by John J. Fitzgerald,American Chemical Society. Meeting Pdf

This book strikes a balance between state-of-the-art solid-state NMR techniques and the applications of these techniques to problems in materials science. The applications focus on modern inorganic materials such as metal oxides, catalysts, zeolites, glasses, ceramics, semiconductors, ion conductors, superconductors, and composites. The book features chapters on multiple-quantum MAS NMR, dynamic-angle spinning NMR for quadrupolar nuclides, and two-dimensional NMR methods. It includes an introductory chapter that provides an a thorough and integrated overview of the field, complete with numerous references.

Solid State NMR of Polymers

L.J. Mathias
Solid State NMR of Polymers Book PDF

Author : L.J. Mathias
Publisher : Springer Science & Business Media
Page : 432 pages
File Size : 54,5 Mb
Release : 1991-10-31
Category : Science
ISBN : 0306440156

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Solid State NMR of Polymers by L.J. Mathias Pdf

The chapters in this collection are from papers which were presented at a symposium on solid-state NMR of polymers. A two-part program on available NMR techniques applicable to solid polymer analysis was presented at the 3rd Chemical Congress of North American held in Toronto, Ontario, June 5-10,1988. The program was sponsored by the Division of Polymer Chemistry with support provided by the Division, its Industrial Sponsors, and the Donors of the Petroleum Research Fund administered by the American Chemical Society. Co-organizers included Professor Colin Fyfe of the University of British Columbia (Vancouver, Canada), Professor Hans Spiess of the Max Planck Institut fur Polymerforschung (Mainz, West Germany), and myself. The full-day tutorial, which was free to registered attendees, covered the range of topics. The purpose of the tutorial was to provide a basic introduction to the field so that newcomers to its present and future applications could develop sufficient understanding to learn effectively from the subsequent symposium. The first talk attempted to give listeners a feel for the way a novice spectroscopist can learn to use the various NMR techniques to explore his own areas of interest. Simple experiments can provide unique information about solid polymers that can be useful in interpreting synthetic results and in relating solid-state conformation, morphology and molecular motion to physical properties.

Solid-state NMR

Frances Separovic,Marc-Antoine Sani
Solid state NMR Book PDF

Author : Frances Separovic,Marc-Antoine Sani
Publisher : Unknown
Page : 0 pages
File Size : 46,6 Mb
Release : 2020
Category : Membranes (Biology)
ISBN : 0750325321

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Solid-state NMR by Frances Separovic,Marc-Antoine Sani Pdf

The purpose of this book is to describe the methodology and applications of solid-state NMR spectroscopy to studies of membrane proteins, membrane-active peptides and model biological membranes. As well as structural studies, this book contains coverage of membrane interactions and molecular motions. Advances in biological solid-state NMR are very pertinent with high-field developments seeing applications in biological membranes and whole cells. Experts who are leaders in the development and application of biological solid-state NMR are chapter contributors. Part of Biophysical Society-IOP series.

Multidimensional Solid-State NMR and Polymers

Klaus Schmidt-Rohr,Hans Wolfgang Spiess
Multidimensional Solid State NMR and Polymers Book PDF

Author : Klaus Schmidt-Rohr,Hans Wolfgang Spiess
Publisher : Elsevier
Page : 501 pages
File Size : 55,6 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780080925622

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Multidimensional Solid-State NMR and Polymers by Klaus Schmidt-Rohr,Hans Wolfgang Spiess Pdf

NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation.The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics. Presents original theories and new perspectives on scattering techniques Provides a systematic treatment of the whole subject Gives readers access to previously unpublished material Includes extensive illustrations

NMR and MRI of Electrochemical Energy Storage Materials and Devices

Yong Yang,Riqiang Fu,Hua Huo
NMR and MRI of Electrochemical Energy Storage Materials and Devices Book PDF

Author : Yong Yang,Riqiang Fu,Hua Huo
Publisher : Royal Society of Chemistry
Page : 573 pages
File Size : 49,8 Mb
Release : 2021-06-17
Category : Science
ISBN : 9781839160103

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NMR and MRI of Electrochemical Energy Storage Materials and Devices by Yong Yang,Riqiang Fu,Hua Huo Pdf

Energy storage material is a hot topic in material science and chemistry. During the past decade, nuclear magnetic resonance (NMR) has emerged as a powerful tool to aid understanding of the working and failing mechanisms of energy storage materials and devices. The aim of this book is to introduce the use of NMR methods for investigating electrochemical storage materials and devices. Presenting a comprehensive overview of NMR spectroscopy and magnetic resonance imaging (MRI) on energy storage materials, the book will include the theory of paramagnetic interactions and relevant calculation methods, a number of specific NMR approaches developed in the past decade for battery materials (e.g. in situ, ex situ NMR, MRI, DNP, 2D NMR, NMR dynamics) and case studies on a variety of related materials. Helping both NMR spectroscopists entering the field of batteries and battery specialists seeking diagnostic methods for material and device degradation, it is written by leading authorities from international research groups in this field.

Spectroscopic Analyses

Eram Sharmin,Fahmina Zafar
Spectroscopic Analyses Book PDF

Author : Eram Sharmin,Fahmina Zafar
Publisher : BoD – Books on Demand
Page : 242 pages
File Size : 55,6 Mb
Release : 2017-12-06
Category : Science
ISBN : 9789535136279

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Spectroscopic Analyses by Eram Sharmin,Fahmina Zafar Pdf

The book presents developments and applications of these methods, such as NMR, mass, and others, including their applications in pharmaceutical and biomedical analyses. The book is divided into two sections. The first section covers spectroscopic methods, their applications, and their significance as characterization tools; the second section is dedicated to the applications of spectrophotometric methods in pharmaceutical and biomedical analyses. This book would be useful for students, scholars, and scientists engaged in synthesis, analyses, and applications of materials/polymers.