Nmr Spectroscopy In Inorganic Chemistry

Author : Jonathan A. Iggo,Jonathan A. (Department of Chemistry Iggo, University of Liverpool),Konstantin Luzyanin,Konstantin (Department of Chemistry Luzyanin, University of Liverpool)
Publisher : Unknown
Page : 137 pages
File Size : 48,5 Mb
Release : 2020-04-30
Category : Electronic
ISBN : 9780198794851

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NMR Spectroscopy in Inorganic Chemistry by Jonathan A. Iggo,Jonathan A. (Department of Chemistry Iggo, University of Liverpool),Konstantin Luzyanin,Konstantin (Department of Chemistry Luzyanin, University of Liverpool) Pdf

The renowned Oxford Chemistry Primers series, which provides focused introductions to a range of important topics in chemistry, has been refreshed and updated to suit the needs of today's students, lecturers, and postgraduate researchers. The rigorous, yet accessible, treatment of each subjectarea is ideal for those wanting a primer in a given topic to prepare them for more advanced study or research. Moreover, cutting-edge examples and applications throughout the texts show the relevance of the chemistry being described to current research and industry.This new edition of NMR Spectroscopy in Inorganic Chemistry has been extensively updated to include worked examples, problems, self-test questions, and interactive online questions encouraging active learning and promoting a deeper understanding. With a concise and accessible introduction topredicting NMR spectra and expanded sections on quadrupolar nuclei, this excellent introductory text will help students get to grips with the basics before building on that understanding through diagrammatic content to explain the more challenging concepts.Examples are included from many different areas of inorganic chemistry which are then closely related to the theory described. By giving a simple overview of the relevant theory and avoiding the "pattern recognition" approach frequently used, it demystifies NMR.

Author : D. W. H. Rankin,Norbert Mitzel,Carole Morrison
Publisher : John Wiley & Sons
Page : 606 pages
File Size : 40,8 Mb
Release : 2013-01-02
Category : Science
ISBN : 9781118462881

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Structural Methods in Molecular Inorganic Chemistry by D. W. H. Rankin,Norbert Mitzel,Carole Morrison Pdf

Determining the structure of molecules is a fundamental skill that all chemists must learn. Structural Methods in Molecular Inorganic Chemistry is designed to help readers interpret experimental data, understand the material published in modern journals of inorganic chemistry, and make decisions about what techniques will be the most useful in solving particular structural problems. Following a general introduction to the tools and concepts in structural chemistry, the following topics are covered in detail: • computational chemistry • nuclear magnetic resonance spectroscopy • electron paramagnetic resonance spectroscopy • Mössbauer spectroscopy • rotational spectra and rotational structure • vibrational spectroscopy • electronic characterization techniques • diffraction methods • mass spectrometry The final chapter presents a series of case histories, illustrating how chemists have applied a broad range of structural techniques to interpret and understand chemical systems. Throughout the textbook a strong connection is made between theoretical topics and the real world of practicing chemists. Each chapter concludes with problems and discussion questions, and a supporting website contains additional advanced material. Structural Methods in Molecular Inorganic Chemistry is an extensive update and sequel to the successful textbook Structural Methods in Inorganic Chemistry by Ebsworth, Rankin and Cradock. It is essential reading for all advanced students of chemistry, and a handy reference source for the professional chemist.

Author : Richard Vernon Parish
Publisher : Ellis Horwood
Page : 232 pages
File Size : 46,7 Mb
Release : 1990
Category : Science
ISBN : UOM:39015019867491

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NMR, NQR, EPR, and Mössbauer Spectroscopy in Inorganic Chemistry by Richard Vernon Parish Pdf

Author : J.W. Akitt,B. E. Mann
Publisher : CRC Press
Page : 400 pages
File Size : 45,7 Mb
Release : 2017-12-21
Category : Science
ISBN : 9781482268379

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NMR and Chemistry by J.W. Akitt,B. E. Mann Pdf

Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.

Author : Ivano Bertini,Claudio Luchinat,Giacomo Parigi,Enrico Ravera
Publisher : Elsevier
Page : 508 pages
File Size : 47,7 Mb
Release : 2016-09-15
Category : Science
ISBN : 9780444634481

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NMR of Paramagnetic Molecules by Ivano Bertini,Claudio Luchinat,Giacomo Parigi,Enrico Ravera Pdf

NMR of Paramagnetic Molecules: Applications to Metallobiomolecules and Models, Second Edition is a self-contained, comprehensive reference for chemists, physicists, and life scientists whose research involves analyzing paramagnetic compounds. Since the previous edition of this book was published, there have been many advancements in the field of paramagnetic NMR spectroscopy. This completely updated and expanded edition contains the latest fundamental theory and methods for mastery of this analytical technique. Users will learn how to interpret the NMR spectra of paramagnetic molecules, improve experimental techniques, and strengthen their understanding of the underlying theory and applications. Reflects all advances in the field in a completely updated new edition Presents new material on self-orientation residual dipolar couplings, solid state NMR, dynamic nuclear polarization, and paramagnetic restraints for structure calculations Includes information relevant to paramagnetic molecules, metallobiomolecules, paramagnetic compounds, and paramagnetic NMR spectroscopy Presents specific examples of paramagnetic inorganic species and experimental techniques for structure characterization

Author : P. S. Pregosin
Publisher : Elsevier Publishing Company
Page : 372 pages
File Size : 43,5 Mb
Release : 1991
Category : Science
ISBN : UOM:39015024968011

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Transition Metal Nuclear Magnetic Resonance by P. S. Pregosin Pdf

Transition metal NMR spectroscopy has progressed enormously in recent years. New methods, and specifically solid-state methods and new pulse sequences, have allowed access to data from nuclei with relatively low receptivities with the result that chemists have begun to consider problems previously inaccessible. Moreover, theory, and computational science in particular, now permits the calculation of not just 13 C, 15 N and other light nuclei chemical shifts, but also heavy main-group elements and transition metals. This, combined with increasing access to high field pulsed spectrometers has produced a wealth of new data on NMR of transition metals. understanding and using the nuclear magnetic resonance spectra of the metals of Groups 3-12. The reader is provided with a view on how these nuclei are currently being approached, and what information can be obtained. The authors have liberally reproduced spectra as well as correlations relating metal-NMR data to different physical characteristics of their molecules.

Author : B. Blümich
Publisher : Springer Science & Business Media
Page : 220 pages
File Size : 54,6 Mb
Release : 2013-03-09
Category : Science
ISBN : 9783642500497

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Solid-State NMR II by B. Blümich Pdf

1. G. Engelhardt, H. Koller, Stuttgart, FRG: 29Si NMR of Inorganic Solids 2. H. Pfeifer, Leizpig, FRG: NMR of Solid Surfaces 3. A. Sebald, Bayreuth, FRG: MAS and CP/MAS NMR of Less Common Spin-1/2 Nuclei 4. C. J{ger, Mainz, FRG: Satellite Transition Spectroscopy of Quadrupolar Nuclei 5. D. Brinkmann, M. Mali, Z}rich, CH: NMR-NQR Studies of High-Temperature Superconductors.

Author : G. Davidson
Publisher : Royal Society of Chemistry
Page : 476 pages
File Size : 53,8 Mb
Release : 1994
Category : Inorganic compounds
ISBN : 9780851869810

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G. Davidson Pdf

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 54,5 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235

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Nuclear Magnetic Resonance Spectroscopy by Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge Pdf

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Author : G Davidson
Publisher : Royal Society of Chemistry
Page : 504 pages
File Size : 50,7 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847555106

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G Davidson Pdf

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Author : Kenneth J.D. MacKenzie,M.E. Smith
Publisher : Elsevier
Page : 748 pages
File Size : 44,9 Mb
Release : 2002-04-26
Category : Science
ISBN : 9780080537108

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Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials by Kenneth J.D. MacKenzie,M.E. Smith Pdf

Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Author : John J. Fitzgerald,American Chemical Society. Meeting
Publisher : Unknown
Page : 440 pages
File Size : 46,9 Mb
Release : 1999
Category : Medical
ISBN : UOM:39015043093916

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Solid-state NMR Spectroscopy of Inorganic Materials by John J. Fitzgerald,American Chemical Society. Meeting Pdf

This book strikes a balance between state-of-the-art solid-state NMR techniques and the applications of these techniques to problems in materials science. The applications focus on modern inorganic materials such as metal oxides, catalysts, zeolites, glasses, ceramics, semiconductors, ion conductors, superconductors, and composites. The book features chapters on multiple-quantum MAS NMR, dynamic-angle spinning NMR for quadrupolar nuclides, and two-dimensional NMR methods. It includes an introductory chapter that provides an a thorough and integrated overview of the field, complete with numerous references.

Author : Vladimir I. Bakhmutov
Publisher : CRC Press
Page : 360 pages
File Size : 43,7 Mb
Release : 2015-04-10
Category : Medical
ISBN : 9781482262728

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NMR Spectroscopy in Liquids and Solids by Vladimir I. Bakhmutov Pdf

NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics. The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR— including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.

Author : G Davidson
Publisher : Royal Society of Chemistry
Page : 468 pages
File Size : 55,8 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847555120

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G Davidson Pdf

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Author : Simonpietro Agnello
Publisher : John Wiley & Sons
Page : 500 pages
File Size : 53,8 Mb
Release : 2021-09-08
Category : Technology & Engineering
ISBN : 9781119697329

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Spectroscopy for Materials Characterization by Simonpietro Agnello Pdf

SPECTROSCOPY FOR MATERIALS CHARACTERIZATION Learn foundational and advanced spectroscopy techniques from leading researchers in physics, chemistry, surface science, and nanoscience In Spectroscopy for Materials Characterization, accomplished researcher Simonpietro Agnello delivers a practical and accessible compilation of various spectroscopy techniques taught and used to today. The book offers a wide-ranging approach taught by leading researchers working in physics, chemistry, surface science, and nanoscience. It is ideal for both new students and advanced researchers studying and working with spectroscopy. Topics such as confocal and two photon spectroscopy, as well as infrared absorption and Raman and micro-Raman spectroscopy, are discussed, as are thermally stimulated luminescence and spectroscopic studies of radiation effects on optical materials. Each chapter includes a basic introduction to the theory necessary to understand a specific technique, details about the characteristic instrumental features and apparatuses used, including tips for the appropriate arrangement of a typical experiment, and a reproducible case study that shows the discussed techniques used in a real laboratory. Readers will benefit from the inclusion of: Complete and practical case studies at the conclusion of each chapter to highlight the concepts and techniques discussed in the material Citations of additional resources ideal for further study A thorough introduction to the basic aspects of radiation matter interaction in the visible-ultraviolet range and the fundamentals of absorption and emission A rigorous exploration of time resolved spectroscopy at the nanosecond and femtosecond intervals Perfect for Master and Ph.D. students and researchers in physics, chemistry, engineering, and biology, Spectroscopy for Materials Characterization will also earn a place in the libraries of materials science researchers and students seeking a one-stop reference to basic and advanced spectroscopy techniques.