Scanning Electrochemical Microscopy

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Scanning Electrochemical Microscopy

Author : Allen J. Bard,Michael V. Mirkin
Publisher : CRC Press
Page : 668 pages
File Size : 55,9 Mb
Release : 2001-04-18
Category : Science
ISBN : 020391077X

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Scanning Electrochemical Microscopy by Allen J. Bard,Michael V. Mirkin Pdf

Scanning Electrochemical Microscopy describes the theory and operating principles of scanning electrochemical microscopy (SECM), including instrumentation, tip preparation, imaging techniques and potentiometric probes. The book explores applications relevant to electron transfer reactions, reaction kinetics, chemical events at interfaces, biologica

Scanning Electrochemical Microscopy

Author : Allen J. Bard,Michael V. Mirkin
Publisher : CRC Press
Page : 619 pages
File Size : 55,9 Mb
Release : 2022-07-29
Category : Science
ISBN : 9781000584059

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Scanning Electrochemical Microscopy by Allen J. Bard,Michael V. Mirkin Pdf

Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field over several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Third Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. The vitality and growing popularity of SECM over the past 30+ years have largely been determined by its versatility and capability to remain useful in the changing scientific and technological environments. New applications reported during the last decade reflect significant current activity in biomedical and energy-related research. This thoroughly updated edition provides up-to-date comprehensive reviews of different aspects of SECM. New chapters by renowned professionals in the field cover recent advances in different areas of SECM including nanoSECM, surface reactions and films, batteries, and fuel cells. Expanded coverage of electrocatalysis and surface interrogation as well as photoelectrochemistry and photoelectrocatalysis are also provided. Useful for a broad range of interdisciplinary research—from biological systems to nanopatterning—this book is invaluable to all interested in learning and applying SECM.

Electrochemical Methods for Neuroscience

Author : Adrian C. Michael,Laura Borland
Publisher : CRC Press
Page : 544 pages
File Size : 52,7 Mb
Release : 2006-12-13
Category : Science
ISBN : 9781420005868

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Electrochemical Methods for Neuroscience by Adrian C. Michael,Laura Borland Pdf

Since the first implant of a carbon microelectrode in a rat 35 years ago, there have been substantial advances in the sensitivity, selectivity and temporal resolution of electrochemical techniques. Today, these methods provide neurochemical information that is not accessible by other means. The growing recognition of the versatility of electrochemical techniques indicates a need for a greater understanding of the scientific foundation and use of these powerful tools. Electrochemical Methods for Neuroscience provides an updated summary of the current, albeit evolving, state of the art and lays the scientific foundation for incorporating electrochemical techniques into on-going or newly emerging research programs in the neuroscience disciplines. With contributions from pioneers in the field, the text outlines the applications and benefits of a wide range of electrochemical techniques. It explores the methodology behind the acquisition of neurochemical and neurobiological data through continuous amperometry, fast scan cyclic voltammetry, high-speed chronoamperometry, ion-selective microelectrodes, enzyme based microelectrodes, and in vivo voltammetry with telemetry. The text also introduces emerging concepts in the field such as the correlation of electrochemical recordings with information obtained from patch clamp, electrophysiological, and behavioral techniques. By presenting up-to-date information on the growing collection of electrochemical methods, microsensors, and research techniques, Electrochemical Methods for Neuroscience assists seasoned researchers and newcomers to the field in making sound decisions about adopting the most appropriate of these tools for their future research objectives.

Scanning Electrochemical Microscopy, Second Edition

Author : Allen J. Bard,Michael V. Mirkin
Publisher : CRC Press
Page : 673 pages
File Size : 52,5 Mb
Release : 2012-04-16
Category : Science
ISBN : 9781439831120

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Scanning Electrochemical Microscopy, Second Edition by Allen J. Bard,Michael V. Mirkin Pdf

Because of its simplicity of use and quantitative results, Scanning Electrochemical Microscopy (SECM) has become an indispensable tool for the study of surface reactivity. The fast expansion of the SECM field during the last several years has been fueled by the introduction of new probes, commercially available instrumentation, and new practical applications. Scanning Electrochemical Microscopy, Second Edition offers essential background and in-depth overviews of specific applications in self-contained chapters. Recent methodological advances have greatly increased the capacity of SECM to characterize interfaces at the nanoscale and to obtain molecular-level chemical information. This thoroughly updated edition retains original chapters describing the principles of SECM measurements, instrumentation, preparation of SECM probes, imaging methodologies, and theory and offers: New chapters on studies of single biological cells, corrosion, electrocatalysis, and hybrid techniques Descriptions of recent advances of SECM in several areas of current interest: biotechnological applications, nanofabrication and surface patterning, and molecular transport across films and membranes Discussion of the ongoing shift from micrometer-scale experiments to the nanoscale Useful for a broad range of interdisciplinary research—from biological systems to probing reactions at the liquid–liquid interface—this book is invaluable to all interested in learning and applying SECM.

Handbook of Electrochemistry

Author : Cynthia G. Zoski
Publisher : Elsevier
Page : 935 pages
File Size : 50,8 Mb
Release : 2007-02-07
Category : Science
ISBN : 9780444519580

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Handbook of Electrochemistry by Cynthia G. Zoski Pdf

Electrochemistry plays a key role in a broad range of research and applied areas including the exploration of new inorganic and organic compounds, biochemical and biological systems, corrosion, energy applications involving fuel cells and solar cells, and nanoscale investigations. The Handbook of Electrochemistry serves as a source of electrochemical information, providing details of experimental considerations, representative calculations, and illustrations of the possibilities available in electrochemical experimentation. The book is divided into five parts: Fundamentals, Laboratory Practical, Techniques, Applications, and Data. The first section covers the fundamentals of electrochemistry which are essential for everyone working in the field, presenting an overview of electrochemical conventions, terminology, fundamental equations, and electrochemical cells, experiments, literature, textbooks, and specialized books. Part 2 focuses on the different laboratory aspects of electrochemistry which is followed by a review of the various electrochemical techniques ranging from classical experiments to scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry. Applications of electrochemistry include electrode kinetic determinations, unique aspects of metal deposition, and electrochemistry in small places and at novel interfaces and these are detailed in Part 4. The remaining three chapters provide useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials. * serves as a source of electrochemical information * includes useful electrochemical data and information involving electrode potentials, diffusion coefficients, and methods used in measuring liquid junction potentials * reviews electrochemical techniques (incl. scanning electrochemical microscopy, electrogenerated chemiluminesence and spectroelectrochemistry)

Polymer Electrolyte Membrane and Direct Methanol Fuel Cell Technology

Author : Christoph Hartnig,Christina Roth
Publisher : Elsevier
Page : 516 pages
File Size : 48,7 Mb
Release : 2012-02-20
Category : Technology & Engineering
ISBN : 9780857095480

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Polymer Electrolyte Membrane and Direct Methanol Fuel Cell Technology by Christoph Hartnig,Christina Roth Pdf

Polymer electrolyte membrane fuel cells (PEMFCs) and direct methanol fuel cells (DMFCs) technology are promising forms of low-temperature electrochemical power conversion technologies that operate on hydrogen and methanol respectively. Featuring high electrical efficiency and low operational emissions, they have attracted intense worldwide commercialization research and development efforts. These R&D efforts include a major drive towards improving materials performance, fuel cell operation and durability. In situ characterization is essential to improving performance and extending operational lifetime through providing information necessary to understand how fuel cell materials perform under operational loads. Polymer Electrolyte Membrane and Direct Methanol Fuel Cell Technology, Volume 2 details in situ characterization, including experimental and innovative techniques, used to understand fuel cell operational issues and materials performance. Part I reviews enhanced techniques for characterization of catalyst activities and processes, such as X-ray absorption and scattering, advanced microscopy and electrochemical mass spectrometry. Part II reviews characterization techniques for water and fuel management, including neutron radiography and tomography, magnetic resonance imaging and Raman spectroscopy. Finally, Part III focuses on locally resolved characterization methods, from transient techniques and electrochemical microscopy, to laser-optical methods and synchrotron radiography. With its international team of expert contributors, Polymer electrolyte membrane and direct methanol fuel cell technology will be an invaluable reference for low temperature fuel cell designers and manufacturers, as well as materials science and electrochemistry researchers and academics. Polymer electrolyte membrane and direct methanol fuel cell technology is an invaluable reference for low temperature fuel cell designers and manufacturers, as well as materials science and electrochemistry researchers and academics. Details in situ characterisation of polymer electrolyte membrane fuel cells (PEMFCs) and direct methanol fuel cells (DMFCs), including the experimental and innovative techniques used to understand fuel cell operational issues and materials performance Examines enhanced techniques for characterisation of catalyst activities and processes, such as X-ray absorption and scattering, advanced microscopy and electrochemical mass spectrometry Reviews characterisation techniques for water and fuel management, including neutron radiography and tomography, and comprehensively covers locally resolved characterisation methods, from transient techniques to laser-optical methods

Liquid Cell Electron Microscopy

Author : Frances M. Ross
Publisher : Cambridge University Press
Page : 529 pages
File Size : 41,8 Mb
Release : 2017
Category : Science
ISBN : 9781107116573

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Liquid Cell Electron Microscopy by Frances M. Ross Pdf

2.6.2 Electrodes for Electrochemistry

Nanoelectrochemistry

Author : Michael V. Mirkin,Shigeru Amemiya
Publisher : CRC Press
Page : 852 pages
File Size : 48,5 Mb
Release : 2015-03-27
Category : Science
ISBN : 9781466561229

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Nanoelectrochemistry by Michael V. Mirkin,Shigeru Amemiya Pdf

Nanoscale electrochemistry has revolutionized electrochemical research and technologies and has made broad impacts in other fields, including nanotechnology and nanoscience, biology, and materials chemistry. Nanoelectrochemistry examines well-established concepts and principles and provides an updated overview of the field and its applications.This

Biosensing for the 21st Century

Author : Fred Lisdat
Publisher : Springer
Page : 504 pages
File Size : 45,8 Mb
Release : 2007-11-20
Category : Science
ISBN : 9783540752011

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Biosensing for the 21st Century by Fred Lisdat Pdf

With contributions by numerous experts

The Use of Electrochemical Scanning Tunnelling Microscopy (EC-STM) in Corrosion Analysis

Author : R Lindstrom,V Maurice,L Klein,P. Marcus
Publisher : Woodhead Publishing
Page : 48 pages
File Size : 45,6 Mb
Release : 2006-11-30
Category : Technology & Engineering
ISBN : 9781845692568

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The Use of Electrochemical Scanning Tunnelling Microscopy (EC-STM) in Corrosion Analysis by R Lindstrom,V Maurice,L Klein,P. Marcus Pdf

The European Federation of Corrosion’s Working Party on Surface Science and the Mechanisms of Corrosion and Protection (EFC WP6) has defined, as one of its objectives, the development of a reference material and reference guidelines for the application of electrochemical scanning tunnelling microscopy (EC-STM) in corrosion science. The use of EC-STM to study the relationship between surface structure and surface reactivity in situ on electrodes in contact with an electrolyte is of major importance in corrosion research. This report describes the reference material and procedural guidelines required to use this technique effectively. STM-users are instructed how to obtain high resolution data on a carefully prepared copper single-crystal surface. Describes the reference material and procedural guidelines required to use this technique effectively Discusses an area of major importance in corrosion research

Semiconductor Electrodes

Author : Harry O. Finklea
Publisher : Elsevier Publishing Company
Page : 552 pages
File Size : 50,5 Mb
Release : 1988
Category : Science
ISBN : UOM:39015016059324

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Semiconductor Electrodes by Harry O. Finklea Pdf

Semiconductors have been studied as electrodes in electrochemical systems since the mid-1950's. However, it was not until the 1970's that the search for alternative energy sources, especially solar energy, led to an enormous expansion in semiconductor electrode research. One attractive option for solar energy conversion is the semiconductor liquid-junction solar cell, which can be designed to produce either electrical power or fuel such as hydrogen. Consequently the number of papers published concerning semiconductor electrodes has rapidly increased. Previous books have principally focused on the underlying theory (largely from solid state physics) and principles of operation of all semiconductor electrodes. It therefore seemed both useful and appropriate to review the field with the intention of collating information for each semiconductor or family of semiconductors, with contributions from authors who are all recognized experts in their field. Each chapter is devoted to critically assessing the recent literature on a particular semiconductor or family of semiconductors.

Tools and Trends in Bioanalytical Chemistry

Author : Lauro Tatsuo Kubota,José Alberto Fracassi da Silva,Marcelo Martins Sena,Wendel Andrade Alves
Publisher : Springer Nature
Page : 559 pages
File Size : 50,6 Mb
Release : 2021-11-25
Category : Science
ISBN : 9783030823818

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Tools and Trends in Bioanalytical Chemistry by Lauro Tatsuo Kubota,José Alberto Fracassi da Silva,Marcelo Martins Sena,Wendel Andrade Alves Pdf

This textbook covers the main tools and techniques used in bioanalysis, provides an overview of their principles, and offers several examples of their application and future trends in diagnosis. Chapters from expert contributors explore the role of bioanalysis in different areas such as biochemistry, physiology, forensics, and clinical diagnosis, including topics from sampling/sample preparation, chemometrics in bioanalysis to the latest techniques used in the field. Particular attention is given to the recent advances in the application of mass spectrometry, NMR, electrochemical methods and separation techniques in bioanalysis. Readers will also find more about the application of microchip-based devices and analytical microarrays. This textbook will appeal to graduate/advanced undergraduate students in Chemistry, Biology, Biochemistry, Pharmacy, and Chemical Engineering. It is also a useful resource for researchers and professionals working in the fields of biomedicine and veterinary sciences, with clear explanations and examples of how the different bioanalytical devices are applied for clinical diagnosis.

Scanning Probe Microscopy

Author : Sergei V. Kalinin,Alexei Gruverman
Publisher : Springer Science & Business Media
Page : 1002 pages
File Size : 46,8 Mb
Release : 2007-04-03
Category : Technology & Engineering
ISBN : 9780387286686

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Scanning Probe Microscopy by Sergei V. Kalinin,Alexei Gruverman Pdf

This volume will be devoted to the technical aspects of electrical and electromechanical SPM probes and SPM imaging on the limits of resolution, thus providing technical introduction into the field. This volume will also address the fundamental physical phenomena underpinning the imaging mechanism of SPMs.

Electrochemical Impedance Spectroscopy

Author : Mark E. Orazem,Bernard Tribollet
Publisher : John Wiley & Sons
Page : 510 pages
File Size : 49,7 Mb
Release : 2011-10-13
Category : Science
ISBN : 9781118209943

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Electrochemical Impedance Spectroscopy by Mark E. Orazem,Bernard Tribollet Pdf

Using electrochemical impedance spectroscopy in a broad range of applications This book provides the background and training suitable for application of impedance spectroscopy to varied applications, such as corrosion, biomedical devices, semiconductors and solid-state devices, sensors, batteries, fuel cells, electrochemical capacitors, dielectric measurements, coatings, electrochromic materials, analytical chemistry, and imaging. The emphasis is on generally applicable fundamentals rather than on detailed treatment of applications. With numerous illustrative examples showing how these principles are applied to common impedance problems, Electrochemical Impedance Spectroscopy is ideal either for course study or for independent self-study, covering: Essential background, including complex variables, differential equations, statistics, electrical circuits, electrochemistry, and instrumentation Experimental techniques, including methods used to measure impedance and other transfer functions Process models, demonstrating how deterministic models of impedance response can be developed from physical and kinetic descriptions Interpretation strategies, describing methods of interpretating of impedance data, ranging from graphical methods to complex nonlinear regression Error structure, providing a conceptual understanding of stochastic, bias, and fitting errors in frequency-domain measurements An overview that provides a philosophy for electrochemical impedance spectroscopy that integrates experimental observation, model development, and error analysis This is an excellent textbook for graduate students in electrochemistry, materials science, and chemical engineering. It's also a great self-study guide and reference for scientists and engineers who work with electrochemistry, corrosion, and electrochemical technology, including those in the biomedical field, and for users and vendors of impedance-measuring instrumentation.

Modern Electrochemical Methods in Nano, Surface and Corrosion Science

Author : Mahmood Aliofkhazraei
Publisher : BoD – Books on Demand
Page : 354 pages
File Size : 45,7 Mb
Release : 2014-06-11
Category : Science
ISBN : 9789535115861

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Modern Electrochemical Methods in Nano, Surface and Corrosion Science by Mahmood Aliofkhazraei Pdf

The basics and principles of new electrochemical methods and also their usage for fabrication and analysis of different nanostructures were discussed in this book. These methods consist of electrochemical methods in nanoscale (e.g. electrochemical atomic force microscopy and electrochemical scanning tunneling microscopy) and also electrochemical methods for fabrication of nanomaterials.