Scanning Force Microscopy Of Polymers

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Scanning Force Microscopy of Polymers

Author : G. Julius Vancso,Holger Schönherr
Publisher : Springer Science & Business Media
Page : 258 pages
File Size : 44,8 Mb
Release : 2010-08-02
Category : Technology & Engineering
ISBN : 9783642012310

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Scanning Force Microscopy of Polymers by G. Julius Vancso,Holger Schönherr Pdf

Scope of the Book Synthetic and natural polymers exhibit a complex structural and morphological hierarchy on multiple length scales [1], which determines their performance. Thus, research aiming at visualizing structure and morphology using a multitude of microscopy techniques has received considerable attention since the early days of polymer science and technology. Various well-developed techniques such as optical microscopy and different forms of electron microscopy (Scanning Electron Micr- copy, SEM; Transmission Electron Microscopy, TEM; Environmental Scanning Electron Microscopy, ESEM) allow one to view polymeric structure at different levels of magni?cation. These classical techniques, and their applications to po- mers, are well documented in the literature [2, 3]. The invention of Scanning Tunneling Microscopy (STM) inspired the devel- ment of Atomic Force Microscopy (AFM) and other forms of scanning proximity microscopes in the late 1980s [4, 5]. AFM, unlike STM, can be used to image n- conducting specimens such as polymers. In addition, AFM imaging is feasible in liquids, which has several advantages. Using liquid imaging cells the forces between specimen and AFM probe are drastically reduced, thus sample damage is prevented. In addition, the use of water as imaging medium opened up new applications aiming at imaging, characterizing, and analyzing biologically important systems.

Electron Microscopy of Polymers

Author : Goerg H. Michler
Publisher : Springer Science & Business Media
Page : 472 pages
File Size : 52,9 Mb
Release : 2008-07-05
Category : Technology & Engineering
ISBN : 9783540363521

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Electron Microscopy of Polymers by Goerg H. Michler Pdf

The study of polymers by electron microscopy (EM) needs special techniques, precautions and preparation methods, including ultramicrotomy. General characteristics of the different techniques of EM, including scanning force microscopy, are given in this hands-on book. The application of these techniques to the study of morphology and properties, particularly micromechanical properties, is described in detail. Examples from all classes of polymers are presented.

Polymer Microscopy

Author : Linda Sawyer,David T. Grubb,Gregory F. Meyers
Publisher : Springer Science & Business Media
Page : 568 pages
File Size : 50,5 Mb
Release : 2008-12-24
Category : Science
ISBN : 9780387726281

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Polymer Microscopy by Linda Sawyer,David T. Grubb,Gregory F. Meyers Pdf

This extensively updated and revised Third Edition is a comprehensive and practical guide to the study of the microstructure of polymers. It is the result of the authors' many years of academic and industrial experience. Introductory chapters deal with the basic concepts of both polymer morphology and processing and microscopy and imaging theory. The core of the book is more applied, with many examples of specimen preparation and image interpretation leading to materials characterization. Emerging techniques such as compositional mapping in which microscopy is combined with spectroscopy are considered. The book closes with a problem solving guide.

Scanning Probe Microscopy of Polymers

Author : Buddy D. Ratner,American Chemical Society. Meeting
Publisher : Unknown
Page : 392 pages
File Size : 46,9 Mb
Release : 1998
Category : Science
ISBN : UOM:39015041915540

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Scanning Probe Microscopy of Polymers by Buddy D. Ratner,American Chemical Society. Meeting Pdf

The highlights of this book include an examination of the use of scanning probe microscopy to characterize a variety of polymeric materials, from polymer single crystals and molecular films to composites and biopolymers. The volume provides a synthesis of critical overviews and important new developments, including applications in atomic resolution, chemical force microscopy, and recognition/nanolithography. It includes a review of basic principles and operational modes, terminology, trends, and a discussion of key industrial applications, such as polymer fibers, polymer composites, and filled polymers. It also includes chapters on biopolymers and living cells and on methods for probing micromechanical properties.

Atomic Force Microscopy of Polymers

Author : Sergei N. Magonov,Natalya Yerina,Sergey Belikov
Publisher : Wiley-Interscience
Page : 320 pages
File Size : 41,8 Mb
Release : 2009-10-02
Category : Science
ISBN : 0470105240

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Atomic Force Microscopy of Polymers by Sergei N. Magonov,Natalya Yerina,Sergey Belikov Pdf

Atomic Force Microscopy of Polymers: From High-Resolution Imaging to Probing Local Mechanical Properties gives background information on how the atomic force microscope (AFM) was developed, how it is used for characterization techniques, and how it complements such techniques. The book details how to properly use this instrument, including preparing samples and developing theoretical models with the information from AFM-generated images.

Scanning Force Microscopy of Polymer Systems

Author : Johann Rasmusson,Universitetet i Linköping. Institutionen för fysik och mätteknik
Publisher : Unknown
Page : 38 pages
File Size : 49,9 Mb
Release : 1995
Category : Electronic
ISBN : 9178716241

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Scanning Force Microscopy of Polymer Systems by Johann Rasmusson,Universitetet i Linköping. Institutionen för fysik och mätteknik Pdf

Synthetic Polymeric Membranes

Author : K. C. Khulbe,C. Y. Feng,Takeshi Matsuura
Publisher : Springer Science & Business Media
Page : 198 pages
File Size : 50,9 Mb
Release : 2007-12-03
Category : Technology & Engineering
ISBN : 9783540739944

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Synthetic Polymeric Membranes by K. C. Khulbe,C. Y. Feng,Takeshi Matsuura Pdf

Researchers in polymeric membranes as well as R&D professionals will find this work an essential addition to the literature. It concentrates on the method recently developed to study the surfaces of synthetic polymeric membranes using an Atomic Force Microscope (AFM), which is fast becoming a very important tool. Each chapter includes information on basic principles, commercial applications, an overview of current research and guidelines for future research.

Applied Scanning Probe Methods III

Author : Bharat Bhushan,Harald Fuchs
Publisher : Springer Science & Business Media
Page : 414 pages
File Size : 50,7 Mb
Release : 2006-04-28
Category : Technology & Engineering
ISBN : 9783540269106

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Applied Scanning Probe Methods III by Bharat Bhushan,Harald Fuchs Pdf

The Nobel Prize of 1986 on Sc- ning Tunneling Microscopy sig- led a new era in imaging. The sc- ning probes emerged as a new i- trument for imaging with a pre- sion suf?cient to delineate single atoms. At ?rst there were two – the Scanning Tunneling Microscope, or STM, and the Atomic Force Mic- scope, or AFM. The STM relies on electrons tunneling between tip and sample whereas the AFM depends on the force acting on the tip when it was placed near the sample. These were quickly followed by the - gneticForceMicroscope,MFM,and the Electrostatic Force Microscope, EFM. The MFM will image a single magnetic bit with features as small as 10nm. With the EFM one can monitor the charge of a single electron. Prof. Paul Hansma at Santa Barbara opened the door even wider when he was able to image biological objects in aqueous environments. At this point the sluice gates were opened and a multitude of different instruments appeared. There are signi?cant differences between the Scanning Probe Microscopes or SPM, and others such as the Scanning Electron Microscope or SEM. The probe microscopes do not require preparation of the sample and they operate in ambient atmosphere, whereas, the SEM must operate in a vacuum environment and the sample must be cross-sectioned to expose the proper surface. However, the SEM can record 3D image and movies, features that are not available with the scanning probes.

Applied Scanning Probe Methods II

Author : Bharat Bhushan,Harald Fuchs
Publisher : Springer Science & Business Media
Page : 456 pages
File Size : 50,8 Mb
Release : 2006-06-22
Category : Technology & Engineering
ISBN : 9783540274537

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Applied Scanning Probe Methods II by Bharat Bhushan,Harald Fuchs Pdf

The Nobel Prize of 1986 on Sc- ningTunnelingMicroscopysignaled a new era in imaging. The sc- ning probes emerged as a new - strument for imaging with a p- cision suf?cient to delineate single atoms. At ?rst there were two – the Scanning Tunneling Microscope, or STM, and the Atomic Force Mic- scope, or AFM. The STM relies on electrons tunneling between tip and sample whereas the AFM depends on the force acting on the tip when it was placed near the sample. These were quickly followed by the M- netic Force Microscope, MFM, and the Electrostatic Force Microscope, EFM. The MFM will image a single magnetic bit with features as small as 10nm. With the EFM one can monitor the charge of a single electron. Prof. Paul Hansma at Santa Barbara opened the door even wider when he was able to image biological objects in aqueous environments. At this point the sluice gates were opened and a multitude of different instruments appeared. There are signi?cant differences between the Scanning Probe Microscopes or SPM, and others such as the Scanning Electron Microscope or SEM. The probe microscopes do not require preparation of the sample and they operate in ambient atmosphere, whereas, the SEM must operate in a vacuum environment and the sample must be cross-sectioned to expose the proper surface. However, the SEM can record 3D image and movies, features that are not available with the scanning probes.

Polymer Microscopy

Author : Linda Sawyer,David T. Grubb
Publisher : Springer Science & Business Media
Page : 417 pages
File Size : 41,5 Mb
Release : 2013-03-09
Category : Technology & Engineering
ISBN : 9789401585958

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Polymer Microscopy by Linda Sawyer,David T. Grubb Pdf

A practical guide to the study and understanding of the structure of synthetic polymer materials using the complete range of microscopic techniques. The major part of the book is devoted to specimen preparation and applications. New applications and additional references provide a critical update.

Atomic Force Microscopy/Scanning Tunneling Microscopy

Author : Samuel H. Cohen,M.T. Bray,Marcia L. Lightbody
Publisher : Springer Science & Business Media
Page : 468 pages
File Size : 43,9 Mb
Release : 1994
Category : Science
ISBN : 9780306448904

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Atomic Force Microscopy/Scanning Tunneling Microscopy by Samuel H. Cohen,M.T. Bray,Marcia L. Lightbody Pdf

Papers presented at the first US Army Natick Research, Development and Engineering Center Symposium on [title], held in Natick, Mass., June 1993. The various symposium topics included application of AFM/STM in material sciences, polymers, physics, biology and biotechnology, along with recent developments including new probe microscopies. The procee.

Applications of Scanned Probe Microscopy to Polymers

Author : James Daryl Batteas,Chris A. Michaels,Gilbert C. Walker
Publisher : Unknown
Page : 292 pages
File Size : 43,7 Mb
Release : 2005
Category : Language Arts & Disciplines
ISBN : UOM:39015060574491

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Applications of Scanned Probe Microscopy to Polymers by James Daryl Batteas,Chris A. Michaels,Gilbert C. Walker Pdf

Applications of Scanned Probe Microscopy to Polymers stresses the analysis of polymer and biopolymer surfaces using the ever-expanding methodologies of scanned probe microscopies. This book includes studies of optical properties by near-field methodologies, local mechanical properties of polymer films by AFM, the dynamics and mechanics of single molecules probed by AFM, and methodologies for enhanced imaging modes. A primary focus of this book is the quantitative measurement of surface properties by scanned probe techniques, which illustrates how the field has evolved and what new challenges lie ahead. Applications of Scanned Probe Microscopy to Polymers will be valuable to students and professionals looking for studies that illustrate what types of polymer material properties may be probed by scanned probe microscopies.

New Developments in Polymer Analytics II

Author : Manfred Schmidt
Publisher : Springer
Page : 190 pages
File Size : 45,8 Mb
Release : 2003-07-01
Category : Science
ISBN : 9783540487630

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New Developments in Polymer Analytics II by Manfred Schmidt Pdf

The two companion volumes of "Advances in Polymer Science" - Volumes 150 and 151 - deal with recent progress in the characterization of polymers, mostly in solution but also at surfaces. The contributions comprise multidimensional chromatography for elucidation, the composition and the chain length distribution of copolymers, capillary electrophoresis of synthetic water-soluble polymers including polyelectrolytes, field flow fractionation techniques for quick and reliable separation and characterization of broad polymer samples and a novel application of thermal grating experiments for probing Brownian and thermal diffusion. Finally the rapid development of atomic forces techniques is reviewed with particular emphasis on the visualization of macromolecules and the patterning of surfaces.

Applied Scanning Probe Methods XII

Author : Bharat Bhushan,Harald Fuchs
Publisher : Springer Science & Business Media
Page : 224 pages
File Size : 50,5 Mb
Release : 2008-10-24
Category : Technology & Engineering
ISBN : 9783540850397

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Applied Scanning Probe Methods XII by Bharat Bhushan,Harald Fuchs Pdf

Crack initiation and growth are key issues when it comes to the mechanical reliab- ity of microelectronic devices and microelectromechanical systems (MEMS). Es- cially in organic electronics where exible substrates will play a major role these issues will become of utmost importance. It is therefore necessary to develop me- ods which in situ allow the experimental investigation of surface deformation and fracture processes in thin layers at a micro and nanometer scale. While scanning electron microscopy (SEM) might be used it is also associated with some major experimental drawbacks. First of all if polymers are investigated they usually have to be coated with a metal layer due to their commonly non-conductive nature. Additi- ally they might be damaged by the electron beam of the microscope or the vacuum might cause outgasing of solvents or evaporation of water and thus change material properties. Furthermore, for all kinds of materials a considerable amount of expe- mental effort is necessary to build a tensile testing machine that ts into the chamber. Therefore, a very promising alternative to SEM is based on the use of an atomic force microscope (AFM) to observe in situ surface deformation processes during straining of a specimen. First steps towards this goal were shown in the 1990s in [1–4] but none of these approaches truly was a microtensile test with sample thicknesses in the range of micrometers. To the authors’ knowledge, this was shown for the rst time by Hild et al. in [5]. 16.