Thermal Analysis In Practice

Author : Matthias Wagner
Publisher : Unknown
Page : 352 pages
File Size : 40,7 Mb
Release : 2017-12
Category : Materials
ISBN : 1569906432

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Thermal Analysis in Practice by Matthias Wagner Pdf

Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

Author : Anonim
Publisher : Unknown
Page : 327 pages
File Size : 53,9 Mb
Release : 2009
Category : Electronic
ISBN : OCLC:845717694

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Thermal Analysis in Practice by Anonim Pdf

Author : Michael E. Brown
Publisher : Elsevier
Page : 725 pages
File Size : 48,9 Mb
Release : 1998-09-07
Category : Science
ISBN : 9780080539591

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Handbook of Thermal Analysis and Calorimetry by Michael E. Brown Pdf

Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.

Author : Paul Gabbott
Publisher : John Wiley & Sons
Page : 480 pages
File Size : 55,7 Mb
Release : 2008-04-30
Category : Science
ISBN : 9780470698129

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Principles and Applications of Thermal Analysis by Paul Gabbott Pdf

Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Author : M.E. Brown
Publisher : Springer Science & Business Media
Page : 220 pages
File Size : 47,7 Mb
Release : 2012-12-06
Category : Technology & Engineering
ISBN : 9789400912199

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Introduction to Thermal Analysis by M.E. Brown Pdf

The aim of this book is, as its title suggests, to help sOilleone with little or no knowledge of what thermal analysis can do, to find out briefly what the subject is all about, to decide whether it will be of use to him or her, and to help in getting started on the more common techniques. Some of the less-common techniques are mentioned, but more specialized texts should be consulted before venturing into these areas. This book arose out of a set of notes prepared for courses on thermal analysis given at instrument workshops organized by'the S.A. Chemical Institute. It has also been useful for similar short courses given at various universities and technikons. I have made extensive use ofthe manufacturers' literature, and I am grateful to them for this information. A wide variety of applications has been drawn from the literature to use as examples and these are acknowledged in the text. A fuller list of the books, reviews and other literature ofthermal analysis is given towards the back of this book. The ICTA booklet 'For Better Thermal Analysis' is also a valuable source of information. I am particularly grateful to my wife, Cindy, for typing the manuscript, to Mrs Heather Wilson for the line drawings, and to Professor David Dollimore of the University of Toledo, Ohio, for many helpful suggestions.

Author : Wesley William Wendlandt
Publisher : Wiley-Interscience
Page : 840 pages
File Size : 52,6 Mb
Release : 1986-03-10
Category : Science
ISBN : UOM:39015016085063

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Thermal Analysis by Wesley William Wendlandt Pdf

Provides a comprehensive introduction to thermal analysis and its usefulness in every area of science from archeology to zoology. Covers many new applications of techniques in TG, DTA, DSC, EGD/EGA, and others. Describes instruments available for each technique, including microcomputers. Includes rewritten chapters on EGD/EGA, miscellaneous techniques, and the determination of purity by DSC.

Author : Joseph D. Menczel,R. Bruce Prime
Publisher : John Wiley & Sons
Page : 607 pages
File Size : 54,8 Mb
Release : 2014-07-09
Category : Science
ISBN : 9781118995990

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Thermal Analysis of Polymers by Joseph D. Menczel,R. Bruce Prime Pdf

Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Author : Paul Gabbott
Publisher : Wiley-Blackwell
Page : 496 pages
File Size : 55,9 Mb
Release : 2008
Category : Science
ISBN : UOM:39015074241996

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Principles and Applications of Thermal Analysis by Paul Gabbott Pdf

Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Author : Gottfried W. Ehrenstein,Gabriela Riedel,Pia Trawiel
Publisher : Carl Hanser Verlag GmbH Co KG
Page : 402 pages
File Size : 47,5 Mb
Release : 2012-11-12
Category : Technology & Engineering
ISBN : 9783446434141

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Thermal Analysis of Plastics by Gottfried W. Ehrenstein,Gabriela Riedel,Pia Trawiel Pdf

Thermal analysis has proven to be one of the most important and meaningful test methods in the plastics industry and in testing laboratories. Although thermal analysis is used for fundamental studies related to materials science of polymers, its power lies in understanding this behavior during manufacturing processes. This understanding aids in process optimization, reduction of manufacturing cycle times, failure analysis as well as overall improvement of the material properties of the finished product, to name a few. In this book, the different test methods and their variations are described in detail, emphasizing the principles and their application in practice. Using practical examples, different approaches to problem solving are presented with a focus on the interpretation of the experimental results. Thermal analysis provides information on important properties of plastic materials, such as nucleation, crystallization, degree of crystallinity, recrystallization, melting and solidification, glass transition, curing and postcuring, thermal stability, thermal expansion, relaxation of orientation and internal stresses, pvT-data, and others. This book is a must for everybody involved in material and product development, testing, processing, quality assurance, or failure analysis in industry and laboratories. Contents: - Differential Scanning Calorimetry (DSC) - Oxidative Induction Time/Temperature (OIT) - Thermogravimetry (TG) - Thermo-Mechanical Analysis (TMA) - pvT-Measurements - Dynamic-Mechanical Analysis (DMA) - Micro-Thermal Analysis - Brief Characterization of Key Polymers

Author : Mike Reading,Douglas J. Hourston
Publisher : Springer Science & Business Media
Page : 340 pages
File Size : 47,5 Mb
Release : 2006-10-12
Category : Technology & Engineering
ISBN : 9781402037504

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Modulated Temperature Differential Scanning Calorimetry by Mike Reading,Douglas J. Hourston Pdf

MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Author : El-Zeiny Ebeid,Mohamed Barakat Zakaria
Publisher : Elsevier
Page : 324 pages
File Size : 46,7 Mb
Release : 2021-06-23
Category : Science
ISBN : 9780323901925

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Thermal Analysis by El-Zeiny Ebeid,Mohamed Barakat Zakaria Pdf

Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures

Author : Jaroslav Šesták,Pavel Hubík,Jiří J. Mareš
Publisher : Springer
Page : 567 pages
File Size : 51,5 Mb
Release : 2017-03-24
Category : Science
ISBN : 9783319458991

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Thermal Physics and Thermal Analysis by Jaroslav Šesták,Pavel Hubík,Jiří J. Mareš Pdf

Features twenty-five chapter contributions from an international array of distinguished academics based in Asia, Eastern and Western Europe, Russia, and the USA. This multi-author contributed volume provides an up-to-date and authoritative overview of cutting-edge themes involving the thermal analysis, applied solid-state physics, micro- and nano-crystallinity of selected solids and their macro- and microscopic thermal properties. Distinctive chapters featured in the book include, among others, calorimetry time scales from days to microseconds, glass transition phenomena, kinetics of non-isothermal processes, thermal inertia and temperature gradients, thermodynamics of nanomaterials, self-organization, significance of temperature and entropy. Advanced undergraduates, postgraduates and researchers working in the field of thermal analysis, thermophysical measurements and calorimetry will find this contributed volume invaluable. This is the third volume of the triptych volumes on thermal behaviour of materials; the previous two receiving thousand of downloads guaranteeing their worldwide impact.

Author : Peter J. Haines
Publisher : Royal Society of Chemistry
Page : 244 pages
File Size : 48,8 Mb
Release : 2002
Category : Education
ISBN : 0854046100

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Principles of Thermal Analysis and Calorimetry by Peter J. Haines Pdf

The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.

Author : Anonim
Publisher : Unknown
Page : 368 pages
File Size : 55,5 Mb
Release : 2004
Category : Plastics
ISBN : 1628701935

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Thermal Analysis of Plastics by Anonim Pdf

Author : V.S. Ramachandran,Ralph M. Paroli,James J. Beaudoin,Ana H. Delgado
Publisher : William Andrew
Page : 702 pages
File Size : 41,8 Mb
Release : 2002-10-28
Category : Technology & Engineering
ISBN : 9780815517757

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Handbook of Thermal Analysis of Construction Materials by V.S. Ramachandran,Ralph M. Paroli,James J. Beaudoin,Ana H. Delgado Pdf

This comprehensive book containing essential information on the applicability of thermal analysis techniques to evaluate inorganic and organic materials in construction technology should serve as a useful reference for the scientist, engineer, construction technologist, architect, manufacturer, and user of construction materials, standard-writing bodies, and analytical chemists. The material scientists at the National Research Council of Canada have established one of the best thermal analysis laboratories in the world. Various types of thermal analysis techniques have been applied successfully to the investigation of inorganic and organic construction materials. These studies have provided important information on the characterization of raw as well as finished materials, quality control, quantitative estimation, interrelationships between physical, chemical, mechanical, and durability characteristics. Information on the application of thermal analysis to construction materials is dispersed in literature and hence the IRC scientists embarked on producing a handbook, the first of its kind, incorporating the latest knowledge available in this field of activity. Almost all important construction materials have been included.