Thermal Analysis

Author : Matthias Wagner
Publisher : Unknown
Page : 352 pages
File Size : 49,7 Mb
Release : 2017-12
Category : Materials
ISBN : 1569906432

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Thermal Analysis in Practice by Matthias Wagner Pdf

Thermal analysis comprises a group of techniques used to determine the physical or chemical properties of a substance as it is heated, cooled, or held at constant temperature. It is particularly important for polymer characterization, but also has major application in analysis of pharmaceuticals and foodstuffs. This comprehensive handbook presents practical and theoretical aspects of the key techniques of DSC, TGA, TMA, DMA, and related methods. It also includes separate chapters on the glass transition, polymers, polymorphism, purity determination, and method development. The large number of practical examples included should inspire readers toward new ideas for applications in their own fields of work. The chapters are independent of one another and can be read individually in any desired order. Based on years of experience in thermal analysis of users, application specialists, consultants, and course instructors, this book provides practical help to newcomers, inexperienced users, and anyone else interested in the practical aspects of thermal analysis.

Author : M.E. Brown
Publisher : Springer Science & Business Media
Page : 264 pages
File Size : 51,5 Mb
Release : 2006-04-11
Category : Technology & Engineering
ISBN : 9780306484049

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Introduction to Thermal Analysis by M.E. Brown Pdf

to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

Author : Anonim
Publisher : Elsevier
Page : 860 pages
File Size : 51,6 Mb
Release : 2018-03-12
Category : Science
ISBN : 9780444640635

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Handbook of Thermal Analysis and Calorimetry by Anonim Pdf

Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications

Author : Bernhard Wunderlich
Publisher : Springer Science & Business Media
Page : 918 pages
File Size : 53,8 Mb
Release : 2005-04-04
Category : Science
ISBN : 3540236295

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Thermal Analysis of Polymeric Materials by Bernhard Wunderlich Pdf

Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.

Author : Paul Gabbott
Publisher : John Wiley & Sons
Page : 480 pages
File Size : 51,8 Mb
Release : 2008-04-30
Category : Science
ISBN : 9780470698129

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Principles and Applications of Thermal Analysis by Paul Gabbott Pdf

Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Author : Joseph D. Menczel,R. Bruce Prime
Publisher : John Wiley & Sons
Page : 607 pages
File Size : 44,5 Mb
Release : 2014-07-09
Category : Science
ISBN : 9781118995990

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Thermal Analysis of Polymers by Joseph D. Menczel,R. Bruce Prime Pdf

Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Author : W. Smykatz-Kloss
Publisher : Springer Science & Business Media
Page : 188 pages
File Size : 41,6 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642659515

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Differential Thermal Analysis by W. Smykatz-Kloss Pdf

At first glance it may seem presumptuous to want to add yet another to the numerous books on Differential Thermal Analysis (DT A). Thermoanalytical methods have been in use for some time, as shown by the more than five thousand publications containing DT A or TG curves listed by SMOTHERS and CHIANG in the bibliography to their handbook and abstracted in the several volumes of Thermal Analysis Abstracts (TAA), edited by J. P. REDFERN for the International Con federation for Thermal Analysis (ICT A). Every three years the proceed ings of ICT A meetings are published, bringing the latest results of thermoanalytic research. There is also the Scifax DT A Data Index, edited by R. C. MACKENZIE (1962) and modeled on the ASTM pattern card index (used for X-ray investigations), a compilation of the DT A data for several hundred minerals, and inorganic and organic materials. The theoretical foundations of thermogravimetry and DT A have been described in detail by LEHMANN, DAS and PAETSCH (1953), R. C. MACKENZIE (1957, 1970), DUVAL (1963), WENDLANDT (1964), GARN (1965), F. PAULIK et al. (1966), SMOTHERS and CHIANG (1966), and KEATTCH (1969). Thermoanalytical results are strongly influenced by various factors relative to preparation and equipment (see 1-2. 4 of this study). This is the reason why we frequently find, in these books as well as in the Scifax-Card catalog, contradictory data on the same substance.

Author : Robert Speyer
Publisher : CRC Press
Page : 304 pages
File Size : 51,5 Mb
Release : 1993-09-16
Category : Science
ISBN : 0824789636

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Thermal Analysis of Materials by Robert Speyer Pdf

Discussing the design and optimum use of thermal analysis instrumentation for materials' property measurement, this work details how the instruments work, what they measure, potential pitfalls and the fitting of experimental results to theoretical models. It presents a tutorial on writing computer programs for data manipulation, advanced thermoanalytical methods and case studies.

Author : Oscar Menis,Harry L. Rook,Paul D. Garn
Publisher : Unknown
Page : 276 pages
File Size : 46,5 Mb
Release : 1980
Category : Thermal analysis
ISBN : UCR:31210025450162

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The State-of-the-art of Thermal Analysis by Oscar Menis,Harry L. Rook,Paul D. Garn Pdf

Author : M.E. Brown
Publisher : Springer Science & Business Media
Page : 220 pages
File Size : 50,5 Mb
Release : 2012-12-06
Category : Technology & Engineering
ISBN : 9789400912199

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Introduction to Thermal Analysis by M.E. Brown Pdf

The aim of this book is, as its title suggests, to help sOilleone with little or no knowledge of what thermal analysis can do, to find out briefly what the subject is all about, to decide whether it will be of use to him or her, and to help in getting started on the more common techniques. Some of the less-common techniques are mentioned, but more specialized texts should be consulted before venturing into these areas. This book arose out of a set of notes prepared for courses on thermal analysis given at instrument workshops organized by'the S.A. Chemical Institute. It has also been useful for similar short courses given at various universities and technikons. I have made extensive use ofthe manufacturers' literature, and I am grateful to them for this information. A wide variety of applications has been drawn from the literature to use as examples and these are acknowledged in the text. A fuller list of the books, reviews and other literature ofthermal analysis is given towards the back of this book. The ICTA booklet 'For Better Thermal Analysis' is also a valuable source of information. I am particularly grateful to my wife, Cindy, for typing the manuscript, to Mrs Heather Wilson for the line drawings, and to Professor David Dollimore of the University of Toledo, Ohio, for many helpful suggestions.

Author : Imre Miklós Szilágyi,György Liptay
Publisher : Springer
Page : 372 pages
File Size : 40,7 Mb
Release : 2014-11-18
Category : Science
ISBN : 9783319094861

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Who is Who in Thermal Analysis and Calorimetry by Imre Miklós Szilágyi,György Liptay Pdf

This is an expanded and revised second edition, presenting accurate and comprehensive information about our leading thermal scientists to current and future generations. In our globalized world, most researchers in thermal analysis do not know each other in person and are not familiar with each other’s achievements. This volume provides the reader with an up-to-date list of the prominent members in this community. The publication contains only living scientists. The selection is based partly on several decades of the editors' personal professional experience and also partly on the opinion of the Regional Editors of the Journal of Thermal Analysis and Calorimetry.

Author : Sidney Speil
Publisher : Unknown
Page : 84 pages
File Size : 43,7 Mb
Release : 1944
Category : Clay
ISBN : UOM:39015078496745

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Applications of Thermal Analysis to Clays and Aluminous Minerals by Sidney Speil Pdf

Author : Paul Kurowski
Publisher : SDC Publications
Page : 302 pages
File Size : 53,8 Mb
Release : 2018-04
Category : Computers
ISBN : 9781630571658

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Thermal Analysis with SOLIDWORKS Simulation 2018 and Flow Simulation 2018 by Paul Kurowski Pdf

Thermal Analysis with SOLIDWORKS Simulation 2018 goes beyond the standard software manual. It concurrently introduces the reader to thermal analysis and its implementation in SOLIDWORKS Simulation using hands-on exercises. A number of projects are presented to illustrate thermal analysis and related topics. Each chapter is designed to build on the skills and understanding gained from previous exercises. Thermal Analysis with SOLIDWORKS Simulation 2018 is designed for users who are already familiar with the basics of Finite Element Analysis (FEA) using SOLIDWORKS Simulation or who have completed the book Engineering Analysis with SOLIDWORKS Simulation 2018. Thermal Analysis with SOLIDWORKS Simulation 2018 builds on these topics in the area of thermal analysis. Some understanding of FEA and SOLIDWORKS Simulation is assumed.

Author : Donald J. Evans,Karl Strnat
Publisher : Unknown
Page : 34 pages
File Size : 51,5 Mb
Release : 1963
Category : Nonferrous metals
ISBN : UOM:39015095317403

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An Apparatus for Direct and Differential Thermal Analysis at Temperatures Up to 1500°C by Donald J. Evans,Karl Strnat Pdf

A recording apparatus suitable for thermal and differential thermal analysis was developed. It can be used to obtain data for phase diagram investigations on small samples of rare metals and their alloys at temperatures up to 1500 C. The thermal analysis apparatus consists of a platinum wound resistance furnace with protective atmos phere provisions and a Pt/Pt 13% Rh thermo couple as sensor which feeds a one mV strip chart recorder. A bucking potentiometer used in series with the thermocouple permits a temperature reso lution of better than 0.5 C. For differential thermal analysis, an additional 100 microvolt strip chart recorder is used. The heating or cooling rate can be varied between 0.5 C/min and approximately 15 C/minute. The thermal analysis apparatus was calibrated at several fixed points and has an overall accuracy of =1.5 C. (Author).

Author : Joseph Adam Pask,Ben Davies
Publisher : Unknown
Page : 36 pages
File Size : 44,9 Mb
Release : 1943
Category : Aluminum oxide
ISBN : UOM:39015078493767

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Thermal Analysis of Clay Minerals and Acid Extraction of Alumina from Clays by Joseph Adam Pask,Ben Davies Pdf