Differential Thermal Analysis

Author : W. Smykatz-Kloss
Publisher : Springer Science & Business Media
Page : 259 pages
File Size : 51,9 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642659515

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Differential Thermal Analysis by W. Smykatz-Kloss Pdf

At first glance it may seem presumptuous to want to add yet another to the numerous books on Differential Thermal Analysis (DT A). Thermoanalytical methods have been in use for some time, as shown by the more than five thousand publications containing DT A or TG curves listed by SMOTHERS and CHIANG in the bibliography to their handbook and abstracted in the several volumes of Thermal Analysis Abstracts (TAA), edited by J. P. REDFERN for the International Con federation for Thermal Analysis (ICT A). Every three years the proceed ings of ICT A meetings are published, bringing the latest results of thermoanalytic research. There is also the Scifax DT A Data Index, edited by R. C. MACKENZIE (1962) and modeled on the ASTM pattern card index (used for X-ray investigations), a compilation of the DT A data for several hundred minerals, and inorganic and organic materials. The theoretical foundations of thermogravimetry and DT A have been described in detail by LEHMANN, DAS and PAETSCH (1953), R. C. MACKENZIE (1957, 1970), DUVAL (1963), WENDLANDT (1964), GARN (1965), F. PAULIK et al. (1966), SMOTHERS and CHIANG (1966), and KEATTCH (1969). Thermoanalytical results are strongly influenced by various factors relative to preparation and equipment (see 1-2. 4 of this study). This is the reason why we frequently find, in these books as well as in the Scifax-Card catalog, contradictory data on the same substance.

Author : Wesley William Wendlandt
Publisher : Wiley-Interscience
Page : 840 pages
File Size : 47,6 Mb
Release : 1986-03-10
Category : Science
ISBN : UOM:39015016085063

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Thermal Analysis by Wesley William Wendlandt Pdf

Provides a comprehensive introduction to thermal analysis and its usefulness in every area of science from archeology to zoology. Covers many new applications of techniques in TG, DTA, DSC, EGD/EGA, and others. Describes instruments available for each technique, including microcomputers. Includes rewritten chapters on EGD/EGA, miscellaneous techniques, and the determination of purity by DSC.

Author : Michael Ian Pope,M. D. Judd
Publisher : Unknown
Page : 206 pages
File Size : 43,5 Mb
Release : 1977
Category : Science
ISBN : MINN:31951P00089895P

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Differential Thermal Analysis by Michael Ian Pope,M. D. Judd Pdf

Author : M.E. Brown
Publisher : Springer Science & Business Media
Page : 268 pages
File Size : 53,7 Mb
Release : 2006-01-10
Category : Technology & Engineering
ISBN : 9780306484049

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Introduction to Thermal Analysis by M.E. Brown Pdf

to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.

Author : Paul Gabbott
Publisher : John Wiley & Sons
Page : 480 pages
File Size : 51,6 Mb
Release : 2008-04-30
Category : Science
ISBN : 9780470698129

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Principles and Applications of Thermal Analysis by Paul Gabbott Pdf

Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Author : El-Zeiny Ebeid,Mohamed Barakat Zakaria
Publisher : Elsevier
Page : 324 pages
File Size : 55,6 Mb
Release : 2021-06-23
Category : Science
ISBN : 9780323901925

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Thermal Analysis by El-Zeiny Ebeid,Mohamed Barakat Zakaria Pdf

Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures

Author : Michael I. Pope,M. D. Judd
Publisher : Unknown
Page : 196 pages
File Size : 42,7 Mb
Release : 1980
Category : Electronic
ISBN : OCLC:634254722

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Differential thermal analysis by Michael I. Pope,M. D. Judd Pdf

Author : William Joseph Smothers,Yao Chiang
Publisher : Unknown
Page : 656 pages
File Size : 46,9 Mb
Release : 1966
Category : Science
ISBN : STANFORD:36105030121805

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Handbook of Differential Thermal Analysis by William Joseph Smothers,Yao Chiang Pdf

Contents - 1. ORIGINS OF DTA: AN INTRODUCTION - 2. EQUIPMENT - 3. FACTORS IN QUALITATIVE DTA - 4. SELECTED APPLICATIONS OF QUALITATIVE DATA - 5. THEORETICAL BACKGROUND IN QUANTITATIVE DTA- 6. QUANTITATIVE DTA - 7. USE AND CORRELATION OF DTA RESULTS - 8. COMMERCIAL EQUIPMENT - United States - Germany - Great Britain - Hungary - Japan - APPENDIX - 1. PUBLICATIONS ON DTA - 2. AUTHOR INDEX FOR PUBLICATIONS - 3. ALPHABETICAL LIST OF MATERIALS STUDIED BY DTA - INDEX -

Author : James W. Dodd,Kenneth H. Tonge
Publisher : Unknown
Page : 370 pages
File Size : 40,9 Mb
Release : 1987
Category : Science
ISBN : UOM:39015018165368

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Thermal Methods by James W. Dodd,Kenneth H. Tonge Pdf

In the light of the versatility of thermal methods of analysis, and the increasing sophistication of the instrumentation available, this book discusses the basic principles of these methods, the manner in which they are affected by experimental conditions and the results which can be expected. Having read this book the reader should appreciate how and when to apply these techniques, and should understand the basic principles sufficiently to approach new instrumentation with confidence.

Author : Anonim
Publisher : Unknown
Page : 0 pages
File Size : 55,7 Mb
Release : 1972
Category : Electronic
ISBN : OCLC:1345567955

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Differential Thermal Analysis by Anonim Pdf

Author : Bernhard Wunderlich
Publisher : Elsevier
Page : 465 pages
File Size : 43,5 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780323139670

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Thermal Analysis by Bernhard Wunderlich Pdf

Thermal Analysis deals with the theories of thermal analysis (thermodynamics, irreversible thermodynamics, and kinetics) as well as instrumentation and techniques (thermometry, differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry). Applications of thermal analysis are also described. This book consists of seven chapters and begins with a brief outline of the history and meaning of heat and temperature before listing the techniques of thermal analysis. The reader is then introduced to the basis of thermal analysis, paying particular attention to the macroscopic theories of matter, namely, equilibrium thermodynamics, irreversible thermodynamics, and kinetics. The next chapter discusses thermometry, focusing on the international temperature scale and the techniques of measuring temperature. Examples of heating and cooling curves are linked to the discussion of transitions. The groundwork for a detailed understanding of transition temperature is given. The chapters that follow explore the principles of differential thermal analysis, calorimetry, thermomechanical analysis and dilatometry, and thermogravimetry. This book is intended for the senior undergraduate or beginning graduate student, as well as for the researcher and teacher interested in thermal analysis.

Author : Louis H. Berkelhamer
Publisher : Unknown
Page : 38 pages
File Size : 51,8 Mb
Release : 1944
Category : Thermal analysis
ISBN : UOM:39015078497040

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An Apparatus for Differential Thermal Analysis by Louis H. Berkelhamer Pdf

Author : Antonín Blažek
Publisher : Unknown
Page : 298 pages
File Size : 41,7 Mb
Release : 1973
Category : Science
ISBN : UCAL:B4982819

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Thermal Analysis by Antonín Blažek Pdf

Author : Michael E. Brown
Publisher : Springer
Page : 230 pages
File Size : 47,9 Mb
Release : 1988-06-30
Category : Science
ISBN : UCSD:31822002496602

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Introduction to Thermal Analysis by Michael E. Brown Pdf

Basic principles and practical requirements of the main techniques are discussed. The author also introduces less common techniques and gives examples of applications. Special attention is given to the use of computers in thermal analysis. Annotation copyright Book News, Inc. Portland, Or.

Author : P.J. Haines
Publisher : Springer Science & Business Media
Page : 297 pages
File Size : 54,7 Mb
Release : 2012-12-06
Category : Science
ISBN : 9789401113243

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Thermal Methods of Analysis by P.J. Haines Pdf

The wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu tors by colleagues and instrument manufacturers is most gratefully ack nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC).