Electron Probe Quantitation

Author : K.F.J. Heinrich,D. Newbury
Publisher : Springer Science & Business Media
Page : 397 pages
File Size : 42,5 Mb
Release : 2013-06-29
Category : Science
ISBN : 9781489926173

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Electron Probe Quantitation by K.F.J. Heinrich,D. Newbury Pdf

In 1968, the National Bureau of Standards (NBS) published Special Publication 298 "Quantitative Electron Probe Microanalysis," which contained proceedings of a seminar held on the subject at NBS in the summer of 1967. This publication received wide interest that continued through the years far beyond expectations. The present volume, also the result of a gathering of international experts, in 1988, at NBS (now the National Institute of Standards and Technology, NIST), is intended to fulfill the same purpose. After years of substantial agreement on the procedures of analysis and data evaluation, several sharply differentiated approaches have developed. These are described in this publi cation with all the details required for practical application. Neither the editors nor NIST wish to endorse any single approach. Rather, we hope that their exposition will stimulate the dialogue which is a prerequisite for technical progress. Additionally, it is expected that those active in research in electron probe microanalysis will appreciate more clearly the areas in which further investigations are warranted.

Author : Victor D. Scott,Glyn Love
Publisher : Unknown
Page : 356 pages
File Size : 54,8 Mb
Release : 1983
Category : Analytical chemistry
ISBN : UCAL:B4477134

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Quantitative Electron-probe Microanalysis by Victor D. Scott,Glyn Love Pdf

Author : A. J. Tousimis,L. Marton
Publisher : Elsevier
Page : 463 pages
File Size : 46,5 Mb
Release : 2013-11-06
Category : Science
ISBN : 9781483284637

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Electron Probe Microanalysis by A. J. Tousimis,L. Marton Pdf

Electron Probe Microanalysis presents a collection of reviews on various aspects of electron probe microanalysis. This book discusses the model for quantitative electron probe analysis. Organized into 14 chapters, this book begins with an overview of the various kinds of microanalysis followed by a discussion of the advantages that can be derived from using the electron probe method. This text then examines the various applications of backscattered electron and specimen current methods for quantitative analysis. Other chapters consider the fundamental concepts for quantitative electron probe microanalysis utilizing pure elements as standards. This book discusses as well the absolute method of quantitative chemical analysis by emission X-ray spectroscopy. The final chapter deals with the main advantage of the Kossel technique in the study of the thermodynamic and mechanical characteristics of crystals. This book is a valuable resource for scientists and research workers. Non-specialists who need information on this excellent analytical tool will also find this book useful.

Author : Roger Theisen
Publisher : Springer
Page : 186 pages
File Size : 52,5 Mb
Release : 1965
Category : Science
ISBN : STANFORD:36105032129921

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Quantitative Electron Microprobe Analysis by Roger Theisen Pdf

The Electron "licroprobe X-!{ay Analyscr conceivcd b ' R C.\S'L\I: \G and A. Cl'!: '\ lEI( in 1949 has been developcd as an extremelv po\\'crful tool in spcctrochcmical analysis for a wide range of applications, ranging from qualitative elcmcntary distribution studies, to highly localiscd quantitatin analysis on a one micron scale. \\'ith the increasing number oi' versatile instruments, commcrcially available, the domain of applications - in metallurgy, solid state physics, mineralogy and geology, biology and medicine, arts and archeology - is rapidly expanding, particularly because reliable quantitative analyses can be achieved. It is well established that in multicomponent specimens, the relative x-ray intensity generated by the electron bombardment - i.e. the intensity ratio of the characteristic x-ray radiation emitted under identical experimental conditions by the specimen and a calibration standard - is not directly correlated to the elementary mass concentration. The use of a wide scale of carefully prepared homogeneous calibration standards is generally very tedious and restricted to binar)' systems. For more complex specimens, the conversion of recorded x-ra)' intensity ratios to elementary mass concentration requires, besides carefule selection of experimental conditions, an adequate correction calculation to take account oi' the various physical phenomenas occurring in the tarp;et - electron retardation, electron backseattering, x-ray excitation efficieney, fluorescence enhaneement by eharaeteristic and continuous radiation and x-ray mass absorption.

Author : Kurt F. J. Heinrich
Publisher : Unknown
Page : 24 pages
File Size : 45,7 Mb
Release : 1970
Category : Analytical chemistry
ISBN : UIUC:30112106654418

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Present State of the Classical Theory of Quantitative Electron Probe Microanalysis by Kurt F. J. Heinrich Pdf

Although the foundations for a procedure of data reduction in quantitative electron probe analysis have not been changed for several years, there has been progress in the choice of expressions, parameters, and constants. A brief account of recommended expressions and procedures is given. Reference is made to the Standard Reference Materials of Au-Ag and Au-Cu alloys issued for electron probe microanalysis.These are especially useful for investigating the application of correction procedures.

Author : Kurt F. J. Heinrich
Publisher : Unknown
Page : 308 pages
File Size : 46,5 Mb
Release : 1968
Category : Analytical chemistry
ISBN : UOM:39015086431619

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Quantitative Electron Probe Microanalysis by Kurt F. J. Heinrich Pdf

Author : Harvey Yakowitz,Robert L. Myklebust,Kurt F. J. Heinrich
Publisher : Unknown
Page : 56 pages
File Size : 48,5 Mb
Release : 1973
Category : Electron probe microanalysis
ISBN : UIUC:30112106612184

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FRAME by Harvey Yakowitz,Robert L. Myklebust,Kurt F. J. Heinrich Pdf

Author : S. J. B. Reed
Publisher : Cambridge University Press
Page : 232 pages
File Size : 54,6 Mb
Release : 2005-08-25
Category : Science
ISBN : 9781139446389

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Electron Microprobe Analysis and Scanning Electron Microscopy in Geology by S. J. B. Reed Pdf

Originally published in 2005, this book covers the closely related techniques of electron microprobe analysis (EMPA) and scanning electron microscopy (SEM) specifically from a geological viewpoint. Topics discussed include: principles of electron-target interactions, electron beam instrumentation, X-ray spectrometry, general principles of SEM image formation, production of X-ray 'maps' showing elemental distributions, procedures for qualitative and quantitative X-ray analysis (both energy-dispersive and wavelength-dispersive), the use of both 'true' electron microprobes and SEMs fitted with X-ray spectrometers, and practical matters such as sample preparation and treatment of results. Throughout, there is an emphasis on geological aspects not mentioned in similar books aimed at a more general readership. The book avoids unnecessary technical detail in order to be easily accessible, and forms a comprehensive text on EMPA and SEM for geological postgraduate and postdoctoral researchers, as well as those working in industrial laboratories.

Author : R. L. Myklebust,C. E. Fiori,Kurt F. J. Heinrich
Publisher : Unknown
Page : 98 pages
File Size : 48,8 Mb
Release : 1979
Category : Electron probe microanalysis
ISBN : UOM:39015086568733

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Frame C by R. L. Myklebust,C. E. Fiori,Kurt F. J. Heinrich Pdf

Author : Kurt F. J. Heinrich
Publisher : Unknown
Page : 60 pages
File Size : 50,6 Mb
Release : 1972
Category : Electron probe microanalysis
ISBN : UIUC:30112106560730

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A Simple Correction Procedure for Quantitative Electron Probe Microanalysis by Kurt F. J. Heinrich Pdf

Author : Jean Hénoc,Kurt F. J. Heinrich,Robert L. Myklebust
Publisher : Unknown
Page : 136 pages
File Size : 41,9 Mb
Release : 1973
Category : Electron probe microanalysis
ISBN : UOM:39015077288259

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A Rigorous Correction Procedure for Quantitative Electron Probe Microanalysis (COR 2) by Jean Hénoc,Kurt F. J. Heinrich,Robert L. Myklebust Pdf

Author : Philip J. Potts,J.F. Bowles,Stephen.J. Reed,R. Cave
Publisher : Springer Science & Business Media
Page : 430 pages
File Size : 42,6 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781461520535

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Microprobe Techniques in the Earth Sciences by Philip J. Potts,J.F. Bowles,Stephen.J. Reed,R. Cave Pdf

30% discount for members of The Mineralogical Society of Britain and Ireland This text covers the range of microanalytical techniques available for the analysis of geological samples, principally in research applications. Each chapter is written in a clear, informative style and has a tutorial element, designed to introduce each technique for the beginning and experienced researcher alike.

Author : Abraham Boekestein,Miodrag K. Pavicevic
Publisher : Springer Science & Business Media
Page : 271 pages
File Size : 53,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783709166796

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Electron Microbeam Analysis by Abraham Boekestein,Miodrag K. Pavicevic Pdf

This supplement of Mikrochimica Acta contains selected papers from the Second Workshop of the European Microbeam Analysis Society (EMAS) "Modern Developments and Applications in Microbeam Analysis", on which took place in May 1991 in Dubrovnik (Yugoslavia). EMAS was founded in 1987 by members from almost all European countries, in order to stimulate research, applications and development of all forms of microbeam methods. One of the most important activities EMAS is the organisation of biannual workshops for demonstrating the current status and developing trends of microbeam methods. For this meeting, EMAS chose to highlight the following topics: electron-beam microanalysis (EPMA) of thin films and quantitative analysis of ultra-light elements, Auger electron spectroscopy (AES), electron energy loss spec trometry (EELS), high-resolution transmission electron microscopy (HRTEM), quantitative analysis of biological samples and standard-less electron-beam microanalysis. Seven introductory lectures and almost seventy poster presentations were given by speakers from twelve European and two non-European (U.S.A. and Argentina) countries were made. One cannot assume that all fields of research in Europe were duly represented, but a definite trend is discernible. EPMA with wavelength-dispersive spectrometry (WDS) or energy-dispersive spectrometry (EDS) is the method with by far the widest range of applications, followed by TEM with EELS and then AES. There are also interesting suggestions for the further development of new appa ratus with new fields of application. Applications are heavily biased towards materials science (thin films in microelectronics and semicon ductors), ceramics and metallurgy, followed by analysis of biological and mineral samples.

Author : G. F. Bastin,H. J. M. Heijligers
Publisher : Unknown
Page : 138 pages
File Size : 51,8 Mb
Release : 1988
Category : Electronic
ISBN : 9068190105

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Quantitative Electron Probe Microanalysis of Nitrogen by G. F. Bastin,H. J. M. Heijligers Pdf

Author : William John Malcolm Salter
Publisher : Unknown
Page : 176 pages
File Size : 43,5 Mb
Release : 1970
Category : Analytical chemistry
ISBN : WISC:89038669065

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A Manual of Quantitative Electron Probe Microanalysis by William John Malcolm Salter Pdf