Experimental Approaches Of Nmr Spectroscopy

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Experimental Approaches of NMR Spectroscopy

The Nuclear Magnetic Resonance Society of Japan
Experimental Approaches of NMR Spectroscopy Book PDF

Author : The Nuclear Magnetic Resonance Society of Japan
Publisher : Springer
Page : 636 pages
File Size : 48,9 Mb
Release : 2017-11-23
Category : Science
ISBN : 9789811059667

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Experimental Approaches of NMR Spectroscopy by The Nuclear Magnetic Resonance Society of Japan Pdf

This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

Nuclear Magnetic Resonance Spectroscopy

Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Nuclear Magnetic Resonance Spectroscopy Book PDF

Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 43,6 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235

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Nuclear Magnetic Resonance Spectroscopy by Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge Pdf

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

NMR — From Spectra to Structures

Terence N. Mitchell,Burkhard Costisella
NMR From Spectra to Structures Book PDF

Author : Terence N. Mitchell,Burkhard Costisella
Publisher : Springer Science & Business Media
Page : 144 pages
File Size : 42,7 Mb
Release : 2013-04-17
Category : Science
ISBN : 9783662054345

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NMR — From Spectra to Structures by Terence N. Mitchell,Burkhard Costisella Pdf

NMR spectroscopy is one of the most important analytical methods available today. This practice-oriented textbook shows how NMR spectra is used in the education of organic structures. The emphasis is on practical rather than on theoretical aspects, which are treated only briefly. NMR- From Spectra to Strucures is a textbook providing an ideal practical guide to today ́s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only the 1D NMR spectra (proton, carbon, DEPT/APT) but, for the first time in a textbook, also the most important 2D spectra (H,H and C,H correlation).

Modern NMR Approaches to the Structure Elucidation of Natural Products

Antony J. Williams,Gary E. Martin,David Rovnyak
Modern NMR Approaches to the Structure Elucidation of Natural Products Book PDF

Author : Antony J. Williams,Gary E. Martin,David Rovnyak
Publisher : Royal Society of Chemistry
Page : 344 pages
File Size : 44,8 Mb
Release : 2016
Category : Science
ISBN : 9781849733830

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Modern NMR Approaches to the Structure Elucidation of Natural Products by Antony J. Williams,Gary E. Martin,David Rovnyak Pdf

Modern NMR Approaches for the Structure Elucidation of Natural Products is part of a two-volume set focusing on the structure elucidation of natural products. Volume 1 discusses contemporary NMR approaches including optimized hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. It also discusses data processing and algorithmic-based analysis of the data to establish molecular structures. This meshing of details regarding data acquisition, software and hardware approaches to the elucidation of natural products will bring together contributions from leading experts in the field. Volume 2 reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, anti-cancer agents, alkaloids, terpenes, steroids, antibiotics, carbohydrates, peptides and venoms. There are no books on the market that are focused on the unique combination of experimental approaches and modern hardware and software approaches to the structure elucidation of natural products. These books will, spread over 2 volumes, bring together acknowledged experts in the field of structure elucidation and be attractive to those with a specific interest in the characterisation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterisation of impurities and degradation products of pharmaceuticals that can be scarce as natural product samples.

In Vivo NMR Spectroscopy

Robin A. de Graaf
In Vivo NMR Spectroscopy Book PDF

Author : Robin A. de Graaf
Publisher : John Wiley & Sons
Page : 584 pages
File Size : 52,6 Mb
Release : 2019-03-11
Category : Science
ISBN : 9781119382546

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In Vivo NMR Spectroscopy by Robin A. de Graaf Pdf

Presents basic concepts, experimental methodology and data acquisition, and processing standards of in vivo NMR spectroscopy This book covers, in detail, the technical and biophysical aspects of in vivo NMR techniques and includes novel developments in the field such as hyperpolarized NMR, dynamic 13C NMR, automated shimming, and parallel acquisitions. Most of the techniques are described from an educational point of view, yet it still retains the practical aspects appreciated by experimental NMR spectroscopists. In addition, each chapter concludes with a number of exercises designed to review, and often extend, the presented NMR principles and techniques. The third edition of In Vivo NMR Spectroscopy: Principles and Techniques has been updated to include experimental detail on the developing area of hyperpolarization; a description of the semi-LASER sequence, which is now a method of choice; updated chemical shift data, including the addition of 31P data; a troubleshooting section on common problems related to shimming, water suppression, and quantification; recent developments in data acquisition and processing standards; and MatLab scripts on the accompanying website for helping readers calculate radiofrequency pulses. Provide an educational explanation and overview of in vivo NMR, while maintaining the practical aspects appreciated by experimental NMR spectroscopists Features more experimental methodology than the previous edition End-of-chapter exercises that help drive home the principles and techniques and offer a more in-depth exploration of quantitative MR equations Designed to be used in conjunction with a teaching course on the subject In Vivo NMR Spectroscopy: Principles and Techniques, 3rd Edition is aimed at all those involved in fundamental and/or diagnostic in vivo NMR, ranging from people working in dedicated in vivo NMR institutes, to radiologists in hospitals, researchers in high-resolution NMR and MRI, and in areas such as neurology, physiology, chemistry, and medical biology.

High-resolution NMR Techniques in Organic Chemistry

T. Claridge
High resolution NMR Techniques in Organic Chemistry Book PDF

Author : T. Claridge
Publisher : Elsevier
Page : 408 pages
File Size : 47,5 Mb
Release : 1999-12-24
Category : Science
ISBN : 0080427995

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High-resolution NMR Techniques in Organic Chemistry by T. Claridge Pdf

From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

Multidimensional NMR in Liquids

Frank J. M. van de Ven
Multidimensional NMR in Liquids Book PDF

Author : Frank J. M. van de Ven
Publisher : Wiley-VCH
Page : 432 pages
File Size : 43,7 Mb
Release : 1995
Category : Science
ISBN : UOM:39015038412501

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Multidimensional NMR in Liquids by Frank J. M. van de Ven Pdf

Multidimensional NMR in Liquids offers a lucid treatment of basic NMR phenomena, building up to today's most sophisticated NMR experiments from first principles. Using easy-to-grasp product-operator formalism, diagrams, and practical examples, one-, two-, and N-dimensional NMR experiments are explained with minimal recourse to quantum mechanics.

Experimental Pulse NMR

Eiichi Fukushima
Experimental Pulse NMR Book PDF

Author : Eiichi Fukushima
Publisher : CRC Press
Page : 556 pages
File Size : 46,5 Mb
Release : 2018-03-08
Category : Science
ISBN : 9780429962417

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Experimental Pulse NMR by Eiichi Fukushima Pdf

This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.

Modern NMR Approaches to the Structure Elucidation of Natural Products

Antony Williams,Gary Martin,David Rovnyak
Modern NMR Approaches to the Structure Elucidation of Natural Products Book PDF

Author : Antony Williams,Gary Martin,David Rovnyak
Publisher : Royal Society of Chemistry
Page : 532 pages
File Size : 48,9 Mb
Release : 2016-12-14
Category : Science
ISBN : 9781849733939

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Modern NMR Approaches to the Structure Elucidation of Natural Products by Antony Williams,Gary Martin,David Rovnyak Pdf

The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1,n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 µg sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products. Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples.

Modern Methods in Solid-state NMR

Paul Hodgkinson
Modern Methods in Solid state NMR Book PDF

Author : Paul Hodgkinson
Publisher : Royal Society of Chemistry
Page : 452 pages
File Size : 47,6 Mb
Release : 2018-04-09
Category : Science
ISBN : 9781782628545

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Modern Methods in Solid-state NMR by Paul Hodgkinson Pdf

Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques. In this unique volume, a range of experts in different areas of modern solid-state NMR explain about their area of expertise, emphasising the “practical aspects” of implementing different techniques, and illustrating what questions can and cannot be addressed. Later chapters address complex materials, showing how different NMR techniques discussed in earlier chapters can be brought together to characterise important materials types. The volume as a whole focusses on topics relevant to the developing field of “NMR crystallography” – the use of solids NMR as a complement to diffraction crystallography. This book is an ideal complement to existing introductory texts and reviews on solid-state NMR. New researchers wanting to understand new areas of solid-state NMR will find each chapter to be the equivalent to spending time in the laboratory of an internationally leading expert, learning the hints and tips that make the difference between knowing about a technique and being ready to put it into action. With no equivalent on the market, it will be of interest to every solid-state NMR researcher (academic and postgraduate) working in the chemical sciences.

Modern NMR Techniques for Chemistry Research

A.E. Derome
Modern NMR Techniques for Chemistry Research Book PDF

Author : A.E. Derome
Publisher : Elsevier
Page : 299 pages
File Size : 41,7 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483286426

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Modern NMR Techniques for Chemistry Research by A.E. Derome Pdf

Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.

Solid State NMR

Klaus Müller,Marco Geppi
Solid State NMR Book PDF

Author : Klaus Müller,Marco Geppi
Publisher : John Wiley & Sons
Page : 562 pages
File Size : 50,9 Mb
Release : 2021-08-23
Category : Science
ISBN : 9783527318162

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Solid State NMR by Klaus Müller,Marco Geppi Pdf

Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.

Nuclear Magnetic Resonance in Biochemistry

Thomas James
Nuclear Magnetic Resonance in Biochemistry Book PDF

Author : Thomas James
Publisher : Academic Press
Page : 440 pages
File Size : 46,5 Mb
Release : 1975-06-28
Category : Science
ISBN : UOM:39015000285281

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Nuclear Magnetic Resonance in Biochemistry by Thomas James Pdf

Nuclear Magnetic Resonance in Biochemistry: Principles and Applications focuses on the principles and applications of nuclear magnetic resonance (NMR) in biochemistry. Topics covered include experimental methods in NMR; the mechanisms of NMR relaxation; chemical and paramagnetic shifts; spin-spin splitting; the use of NMR in investigations of biopolymers and biomolecular interactions; and molecular dynamics in biological and biochemical systems. This text is comprised of eight chapters; the first of which gives an overview of NMR spectroscopy and its use in studies of biological systems. The next two chapters discuss the theoretical basis for NMR applications in biochemistry, with emphasis on Bloch equations, quantum mechanics, correlation function and correlation time, double resonance, and chemical exchange. The reader is then introduced to the basis for chemical shifts and spin-spin splitting, along with several examples of the use of these NMR parameters in studies of small molecule interactions and structure. The experimental apparatus and procedures employed in NMR studies, Fourier transform NMR, and NMR spectral parameters of small molecules interacting with macromolecules are also considered. The book highlights the information obtainable from the spectra of biopolymers, and then concludes with a chapter on NMR investigations of the state of motion of lipids in membranes and model membranes; water in macromolecular and cellular systems; and sodium ion in biological tissue. This book is intended primarily for chemists, biochemists, biophysicists, and molecular biologists, as well as graduate students.

Protein NMR Spectroscopy

John Cavanagh,Nicholas J. Skelton,Wayne J. Fairbrother,Mark Rance,Arthur G. Palmer III
Protein NMR Spectroscopy Book PDF

Author : John Cavanagh,Nicholas J. Skelton,Wayne J. Fairbrother,Mark Rance,Arthur G. Palmer III
Publisher : Elsevier
Page : 915 pages
File Size : 52,5 Mb
Release : 2010-07-21
Category : Science
ISBN : 9780080471037

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Protein NMR Spectroscopy by John Cavanagh,Nicholas J. Skelton,Wayne J. Fairbrother,Mark Rance,Arthur G. Palmer III Pdf

Protein NMR Spectroscopy, Second Edition combines a comprehensive theoretical treatment of NMR spectroscopy with an extensive exposition of the experimental techniques applicable to proteins and other biological macromolecules in solution. Beginning with simple theoretical models and experimental techniques, the book develops the complete repertoire of theoretical principles and experimental techniques necessary for understanding and implementing the most sophisticated NMR experiments. Important new techniques and applications of NMR spectroscopy have emerged since the first edition of this extremely successful book was published in 1996. This updated version includes new sections describing measurement and use of residual dipolar coupling constants for structure determination, TROSY and deuterium labeling for application to large macromolecules, and experimental techniques for characterizing conformational dynamics. In addition, the treatments of instrumentation and signal acquisition, field gradients, multidimensional spectroscopy, and structure calculation are updated and enhanced. The book is written as a graduate-level textbook and will be of interest to biochemists, chemists, biophysicists, and structural biologists who utilize NMR spectroscopy or wish to understand the latest developments in this field. Provides an understanding of the theoretical principles important for biological NMR spectroscopy Demonstrates how to implement, optimize and troubleshoot modern multi-dimensional NMR experiments Allows for the capability of designing effective experimental protocols for investigations of protein structures and dynamics Includes a comprehensive set of example NMR spectra of ubiquitin provides a reference for validation of experimental methods

NMR Spectroscopy and its Application to Biomedical Research

S.K. Sarkar
NMR Spectroscopy and its Application to Biomedical Research Book PDF

Author : S.K. Sarkar
Publisher : Elsevier
Page : 387 pages
File Size : 46,6 Mb
Release : 1996-12-04
Category : Science
ISBN : 0080537596

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NMR Spectroscopy and its Application to Biomedical Research by S.K. Sarkar Pdf

NMR has become the most diverse spectroscopic tool available to date in biomedical research. It is now routinely used to study biomolecular structure and dynamics particularly as a result of recent developments of a cascade of highly sophisticated multidimensional NMR pulse sequences, and of advances in genetic engineering to produce biomolecules, uniformly or selectively enriched with 13C, 15N and 2H. Features of this book: • Provides an up-to-date treatment of NMR techniques and their application to problems of biomedical interest • Most refined multidimensional pulse sequences including the basic aspects are covered by leading NMR spectroscopists. The book will be useful to NMR spectroscopists, biochemists, and to molecular biologists interested in the use of NMR techniques for solving biological problems.