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Author : David Rovnyak
Publisher : Unknown
Page : 420 pages
File Size : 41,6 Mb
Release : 2007
Category : Medical
ISBN : UOM:39015073595434
This book is intended to be a comprehensive resource for educators seeking to enhance NMR-enabled instruction in chemistry. This book describes a host of new, modern laboratories and experiments.
Author : Jeremy K. M. Sanders
Publisher : OUP Oxford
Page : 150 pages
File Size : 51,8 Mb
Release : 1993
Category : Science
ISBN : STANFORD:36105017054201
Nuclear magnetic resonance techniques have advanced dramatically in recent years, and are now more powerful and more versatile than ever before. To exploit these techniques efficiently, the chemist must have both an understanding of their theoretical basis and the ability to interpret the spectra accurately. The new edition of this established workbook develops the latter skill to an advanced level by a combination of worked examples and set problems that cover one- and two-dimensional NMR techniques applied to organic and inorganic systems. Most of the problems are genuine research examples, and this new edition contains eight pages of problems drawn from very recent research work. This second edition is fully compatible with the second edition of Modern NMR Spectroscopy: a guide for chemists, and the two books are thoroughly cross referenced throughout.
Author : J.W. Akitt,B. E. Mann
Publisher : CRC Press
Page : 400 pages
File Size : 50,9 Mb
Release : 2017-12-21
Category : Science
ISBN : 9781482268379
Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.
Author : Roger S. Macomber
Publisher : John Wiley & Sons
Page : 406 pages
File Size : 46,8 Mb
Release : 1997-12-23
Category : Science
ISBN : 9780471157366
Clear, accessible coverage of modern NMR spectroscopy-for students and professionals in many fields of science Nuclear magnetic resonance (NMR) spectroscopy has made quantum leaps in the last decade, becoming a staple tool in such divergent fields as chemistry, physics, materials science, biology, and medicine. That is why it is essential that scientists working in these areas be fully conversant with current NMR theory and practice. This down-to-basics text offers a comprehensive, up-to-date treatment of the fundamentals of NMR spectroscopy. Using a straightforward approach that develops all concepts from a rudimentary level without using heavy mathematics, it gives readers the knowledge they need to solve any molecular structure problem from a complete set of NMR data. Topics are illustrated throughout with hundreds of figures and actual spectra. Chapter-end summaries and review problems with answers are included to help reinforce and test understanding of key material. From NMR studies of biologically important molecules to magnetic resonance imaging, this book serves as an excellent all-around primer on NMR spectroscopic analysis.
Author : A.E. Derome
Publisher : Elsevier
Page : 299 pages
File Size : 51,7 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483286426
Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.
Author : Jeremy K. M. Sanders,Brian K. Hunter
Publisher : Oxford University Press, USA
Page : 314 pages
File Size : 51,8 Mb
Release : 1993-01
Category : Science
ISBN : 0198555660
This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic, and biological chemistry. It also contains much practical advice about the acquisition and use of spectra. Starting from the simple 'one pulse' sequence, the text employs a 'building block' approach to lead naturally to multiple pulse and two-dimensional NMR. Spectra of readily available compounds illustrate each technique. One- and two-dimensional methods are integrated in three chapters which show how to solve problems by making connections between spins through bonds, through space, or through exchange. There are also chapters on spectrum editing and solids. The final chapter contains a case history which attempts to weave the many strands of the text into a coherent strategy. This second edition reflects the progress made by NMR in the past few years: there is greater emphasis on inorganic nuclei; some two-color spectra are used; the treatment of heteronuclear experiments has moved from direct to 'inverse' detection; many new examples and spectra have been included; and the literature to early 1992 has been covered. Like the first edition, this work will be highly useful for all NMR spectroscopists: chemists, academic and industrial researchers, and advanced undergraduate and graduate students needing a clear guide to this valuable technology.
Author : J. W. Akitt
Publisher : Unknown
Page : 400 pages
File Size : 44,9 Mb
Release : 2000
Category : Nuclear magnetic resonance spectroscopy
ISBN : OCLC:1256519970
Author : Millicent Popov
Publisher : CRC Press
Page : 684 pages
File Size : 42,8 Mb
Release : 1990-09-28
Category : Science
ISBN : 0824783328
Details theory, methods, and successful application of NMR technology for chemists, chemical engineers, and biochemists those with specialized knowledge of NMR spectroscopy and those who want to catch up with the spectacular evolution of the field during the last decade. Reviews one-dimensional NMR,
Author : Jeremy K. M. Sanders,Brian K. Hunter
Publisher : Oxford University Press, USA
Page : 328 pages
File Size : 50,9 Mb
Release : 1987
Category : Nuclear magnetic resonance spectroscopy
ISBN : UCAL:B4227255
This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic and biological chemistry. It also contains much practical advice about the acquisition and use of spectra.
Author : Julie Fisher
Publisher : CRC Press
Page : 364 pages
File Size : 47,8 Mb
Release : 2014-10-13
Category : Science
ISBN : 9781466592247
A blend of theory and practical advice, Modern NMR Techniques for Synthetic Chemistry illustrates how NMR spectroscopy can be used to determine the abundance, size, shape, and function of organic molecules. It provides you with a description the NMR technique used (more pictorial than mathematical), indicating the most common pulse sequences, some practical information as appropriate, followed by illustrative examples. This format is followed for each chapter so you can skip the more theoretical details if the practical aspects are what interest you. Following a discussion of basic parameters, the book describes the utility of NMR in detecting and quantifying dynamic processes, with particular emphasis on the usefulness of saturation-transfer (STD) techniques. It details pulsed–field gradient approaches to diffusion measurement, diffusion models, and approaches to ‘inorganic’ nuclei detection, important as many synthetic pathways to new organics involve heavier elements. The text concludes with coverage of applications of NMR to the analysis of complex mixtures, natural products, carbohydrates, and nucleic acids—all areas of activity for researchers working at the chemistry-life sciences interface. The book’s unique format provides some theoretical insight into the NMR technique used, indicating the most common pulse sequences. The book draws upon several NMR methods that are resurging or currently hot in the field and indicates the specific pulse sequence used by various spectrometer manufacturers for each technique. It examines the analysis of complex mixtures, a feature not found in most books on this topic.
Author : Jeremy K. M. Sanders,Edwin C. Constable,Brian K. Hunter
Publisher : Oxford University Press, USA
Page : 140 pages
File Size : 48,9 Mb
Release : 1989
Category : Science
ISBN : STANFORD:36105021379354
This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic and biological chemistry. It also contains much practical advice about the acquisition and use of spectra.
Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 44,6 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Author : James Wells Akitt
Publisher : Unknown
Page : 224 pages
File Size : 48,6 Mb
Release : 1992-01-01
Category : Electronic
ISBN : 0412372703
Author : G. A. Webb
Publisher : Royal Society of Chemistry
Page : 511 pages
File Size : 42,7 Mb
Release : 2009
Category : Medical
ISBN : 9781847559227
For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume in this series comprises a combination of reports offering comprehensive coverage of the literature on this topic. For those wanting to become rapidly acquainted with specific areas of NMR this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an invaluable source of current methods and applications. Reviews include literature published from June 2007 to May 2008.
Author : Jeremy K.M. Sanders,Brian K. Hunter,Edwin C. Constable
Publisher : Unknown
Page : 308 pages
File Size : 47,5 Mb
Release : 1992
Category : Nuclear magnetic resonance spectroscopy
ISBN : OCLC:393089007