A Complete Introduction To Modern Nmr Spectroscopy

Author : Roger S. Macomber
Publisher : John Wiley & Sons
Page : 406 pages
File Size : 48,8 Mb
Release : 1997-12-23
Category : Science
ISBN : 9780471157366

Get Book

A Complete Introduction to Modern NMR Spectroscopy by Roger S. Macomber Pdf

Clear, accessible coverage of modern NMR spectroscopy-for students and professionals in many fields of science Nuclear magnetic resonance (NMR) spectroscopy has made quantum leaps in the last decade, becoming a staple tool in such divergent fields as chemistry, physics, materials science, biology, and medicine. That is why it is essential that scientists working in these areas be fully conversant with current NMR theory and practice. This down-to-basics text offers a comprehensive, up-to-date treatment of the fundamentals of NMR spectroscopy. Using a straightforward approach that develops all concepts from a rudimentary level without using heavy mathematics, it gives readers the knowledge they need to solve any molecular structure problem from a complete set of NMR data. Topics are illustrated throughout with hundreds of figures and actual spectra. Chapter-end summaries and review problems with answers are included to help reinforce and test understanding of key material. From NMR studies of biologically important molecules to magnetic resonance imaging, this book serves as an excellent all-around primer on NMR spectroscopic analysis.

Author : J.W. Akitt,B. E. Mann
Publisher : CRC Press
Page : 400 pages
File Size : 46,5 Mb
Release : 2017-12-21
Category : Science
ISBN : 9781482268379

Get Book

NMR and Chemistry by J.W. Akitt,B. E. Mann Pdf

Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.

Author : J. W. Akitt
Publisher : Unknown
Page : 400 pages
File Size : 41,7 Mb
Release : 2000
Category : Nuclear magnetic resonance spectroscopy
ISBN : OCLC:1256519970

Get Book

NMR and Chemistry by J. W. Akitt Pdf

Author : James Wells Akitt
Publisher : Unknown
Page : 224 pages
File Size : 51,5 Mb
Release : 1992-01-01
Category : Electronic
ISBN : 0412372703

Get Book

Nmr and Chemistry by James Wells Akitt Pdf

Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 53,5 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235

Get Book

Nuclear Magnetic Resonance Spectroscopy by Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge Pdf

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Author : Jeremy K. M. Sanders,Brian K. Hunter
Publisher : Oxford University Press, USA
Page : 328 pages
File Size : 53,6 Mb
Release : 1987
Category : Nuclear magnetic resonance spectroscopy
ISBN : UCAL:B4227255

Get Book

Modern NMR Spectroscopy by Jeremy K. M. Sanders,Brian K. Hunter Pdf

This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic and biological chemistry. It also contains much practical advice about the acquisition and use of spectra.

Author : A.E. Derome
Publisher : Elsevier
Page : 299 pages
File Size : 55,8 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483286426

Get Book

Modern NMR Techniques for Chemistry Research by A.E. Derome Pdf

Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.

Author : Jeremy K. M. Sanders,Edwin C. Constable,Brian K. Hunter
Publisher : Oxford University Press, USA
Page : 140 pages
File Size : 45,9 Mb
Release : 1989
Category : Science
ISBN : STANFORD:36105021379354

Get Book

Modern NMR Spectroscopy by Jeremy K. M. Sanders,Edwin C. Constable,Brian K. Hunter Pdf

This book provides a non-mathematical, descriptive approach to modern NMR spectroscopy, taking examples from organic, inorganic and biological chemistry. It also contains much practical advice about the acquisition and use of spectra.

Author : Jeremy K. M. Sanders
Publisher : OUP Oxford
Page : 150 pages
File Size : 49,6 Mb
Release : 1993
Category : Science
ISBN : STANFORD:36105017054201

Get Book

Modern NMR Spectroscopy by Jeremy K. M. Sanders Pdf

Nuclear magnetic resonance techniques have advanced dramatically in recent years, and are now more powerful and more versatile than ever before. To exploit these techniques efficiently, the chemist must have both an understanding of their theoretical basis and the ability to interpret the spectra accurately. The new edition of this established workbook develops the latter skill to an advanced level by a combination of worked examples and set problems that cover one- and two-dimensional NMR techniques applied to organic and inorganic systems. Most of the problems are genuine research examples, and this new edition contains eight pages of problems drawn from very recent research work. This second edition is fully compatible with the second edition of Modern NMR Spectroscopy: a guide for chemists, and the two books are thoroughly cross referenced throughout.

Author : Anonim
Publisher : CUP Archive
Page : 196 pages
File Size : 48,9 Mb
Release : 2024-06-30
Category : Electronic
ISBN : 8210379456XXX

Get Book

n.m.r. and chemistry by Anonim Pdf

Author : Henrike Heise,Stephen Matthews
Publisher : Springer
Page : 210 pages
File Size : 46,9 Mb
Release : 2014-07-08
Category : Science
ISBN : 9783642379918

Get Book

Modern NMR Methodology by Henrike Heise,Stephen Matthews Pdf

NMR Spectroscopy for Chemical Analysis at Low Magnetic Fields, by Stefan Glöggler, Bernhard Blümich, Stephan Appelt Dynamic Nuclear Hyperpolarization in Liquids, by Ulrich L. Günther NMR with Multiple Receivers, by Eriks Kupce TROSY NMR Spectroscopy of Large Soluble Proteins, by Yingqi Xu, Stephen Matthews Solid-State NMR Spectroscopy of Proteins, by Henrik Müller, Manuel Etzkorn, Henrike Heise Paramagnetic Solid-State Magic-Angle Spinning NMR Spectroscopy, by Guido Pintacuda, Gwendal Kervern

Author : Helmut Duddeck,Wolfgang Dietrich,Gabor Toth
Publisher : Springer Science & Business Media
Page : 214 pages
File Size : 43,7 Mb
Release : 2013-04-18
Category : Science
ISBN : 9783642883101

Get Book

Structure Elucidation by Modern NMR by Helmut Duddeck,Wolfgang Dietrich,Gabor Toth Pdf

During the last few years, routine applications of NMR (Nuclear Magnetic Resonance) techniques have developed at a tremendous pace. The latest generation of spectrometers have enabled chemists to perform new types of experiments, such as spinlock and inverse-detected methods. This third, revised and expanded edition introduces the latest methodologies and incorporates them into new exercises.

Author : Julie Fisher
Publisher : CRC Press
Page : 364 pages
File Size : 42,5 Mb
Release : 2014-10-13
Category : Science
ISBN : 9781466592247

Get Book

Modern NMR Techniques for Synthetic Chemistry by Julie Fisher Pdf

A blend of theory and practical advice, Modern NMR Techniques for Synthetic Chemistry illustrates how NMR spectroscopy can be used to determine the abundance, size, shape, and function of organic molecules. It provides you with a description the NMR technique used (more pictorial than mathematical), indicating the most common pulse sequences, some practical information as appropriate, followed by illustrative examples. This format is followed for each chapter so you can skip the more theoretical details if the practical aspects are what interest you. Following a discussion of basic parameters, the book describes the utility of NMR in detecting and quantifying dynamic processes, with particular emphasis on the usefulness of saturation-transfer (STD) techniques. It details pulsed–field gradient approaches to diffusion measurement, diffusion models, and approaches to ‘inorganic’ nuclei detection, important as many synthetic pathways to new organics involve heavier elements. The text concludes with coverage of applications of NMR to the analysis of complex mixtures, natural products, carbohydrates, and nucleic acids—all areas of activity for researchers working at the chemistry-life sciences interface. The book’s unique format provides some theoretical insight into the NMR technique used, indicating the most common pulse sequences. The book draws upon several NMR methods that are resurging or currently hot in the field and indicates the specific pulse sequence used by various spectrometer manufacturers for each technique. It examines the analysis of complex mixtures, a feature not found in most books on this topic.

Author : Malcolm H. Levitt
Publisher : John Wiley & Sons
Page : 824 pages
File Size : 54,6 Mb
Release : 2013-05-20
Category : Science
ISBN : 9781118681848

Get Book

Spin Dynamics by Malcolm H. Levitt Pdf

Spin Dynamics: Basics of Nuclear Magnetic Resonance, Second Edition is a comprehensive and modern introduction which focuses on those essential principles and concepts needed for a thorough understanding of the subject, rather than the practical aspects. The quantum theory of nuclear magnets is presented within a strong physical framework, supported by figures. The book assumes only a basic knowledge of complex numbers and matrices, and provides the reader with numerous worked examples and exercises to encourage understanding. With the explicit aim of carefully developing the subject from the beginning, the text starts with coverage of quarks and nucleons and progresses through to a detailed explanation of several important NMR experiments, including NMR imaging, COSY, NOESY and TROSY. Completely revised and updated, the Second Edition features new material on the properties and distributions of isotopes, chemical shift anisotropy and quadrupolar interactions, Pake patterns, spin echoes, slice selection in NMR imaging, and a complete new chapter on the NMR spectroscopy of quadrupolar nuclei. New appendices have been included on Euler angles, and coherence selection by field gradients. As in the first edition, all material is heavily supported by graphics, much of which is new to this edition. Written for undergraduates and postgraduate students taking a first course in NMR spectroscopy and for those needing an up-to-date account of the subject, this multi-disciplinary book will appeal to chemical, physical, material, life, medical, earth and environmental scientists. The detailed physical insights will also make the book of interest for experienced spectroscopists and NMR researchers. • An accessible and carefully written introduction, designed to help students to fully understand this complex and dynamic subject • Takes a multi-disciplinary approach, focusing on basic principles and concepts rather than the more practical aspects • Presents a strong pedagogical approach throughout, with emphasis placed on individual spins to aid understanding • Includes numerous worked examples, problems, further reading and additional notes Praise from the reviews of the First Edition: "This is an excellent book... that many teachers of NMR spectroscopy will cherish... It deserves to be a ‘classic’ among NMR spectroscopy texts." NMR IN BIOMEDICINE "I strongly recommend this book to everyone...it is probably the best modern comprehensive description of the subject." ANGEWANDTE CHEMIE, INTERNATIONAL EDITION

Author : Horst Friebolin
Publisher : Wiley-VCH
Page : 436 pages
File Size : 40,7 Mb
Release : 2005-03-14
Category : Science
ISBN : UVA:X030011435

Get Book

Basic One- and Two-Dimensional NMR Spectroscopy by Horst Friebolin Pdf

A classic among NMR textbooks, this thoroughly enlarged and updated fourth edition contains a new treatment applications of Magnetic Reconance Tomography and Magnetic Resonance Spectroscopy, describes polymer solid state NMR and analysis of biopolymers.