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Author : Peter Luger
Publisher : Walter de Gruyter
Page : 329 pages
File Size : 40,6 Mb
Release : 2011-09-08
Category : Science
ISBN : 9783110836899
Author : Peter Luger
Publisher : Walter de Gruyter
Page : 348 pages
File Size : 44,8 Mb
Release : 2014-04-01
Category : Science
ISBN : 9783110308280
An excellent book for professional crystallographers! In 2012 the crystallographic community celebrated 100 years of X-ray diffraction in honour of the pioneering experiment in 1912 by Max von Laue, Friedrich and Knipping. Experimental developments e.g. brilliant X-ray sources, area detection, and developments in computer hardware and software have led to increasing applications in X-ray analysis. This completely revised edition is a guide for practical work in X-ray analysis. An introduction to basic crystallography moves quickly to a practical and experimental treatment of structure analysis. Emphasis is placed on understanding results and avoiding pitfalls. Essential reading for researchers from the student to the professional level interested in understanding the structure of molecules.
Author : Mark Ladd,Rex Palmer
Publisher : Springer Science & Business Media
Page : 784 pages
File Size : 47,8 Mb
Release : 2014-07-08
Category : Science
ISBN : 9781461439547
The advances in and applications of x-ray and neutron crystallography form the essence of this new edition of this classic textbook, while maintaining the overall plan of the book that has been well received in the academic community since the first edition in 1977. X-ray crystallography is a universal tool for studying molecular structure, and the complementary nature of neutron diffraction crystallography permits the location of atomic species in crystals which are not easily revealed by X-ray techniques alone, such as hydrogen atoms or other light atoms in the presence of heavier atoms. Thus, a chapter discussing the practice of neutron diffraction techniques, with examples, broadens the scope of the text in a highly desirable way. As with previous editions, the book contains problems to illustrate the work of each chapter, and detailed solutions are provided. Mathematical procedures related to the material of the main body of the book are not discussed in detail, but are quoted where needed with references to standard mathematical texts. To address the computational aspect of crystallography, the suite of computer programs from the fourth edition has been revised and expanded. The programs enable the reader to participate fully in many of the aspects of x-ray crystallography discussed in the book. In particular, the program system XRAY* is interactive, and enables the reader to follow through, at the monitor screen, the computational techniques involved in single-crystal structure determination, albeit in two dimensions, with the data sets provided. Exercises for students can be found in the book, and solutions are available to instructors.
Author : Dennis W. Bennett
Publisher : John Wiley & Sons
Page : 826 pages
File Size : 48,7 Mb
Release : 2010-03-08
Category : Science
ISBN : 9783527326778
The first textbook for teaching this method to users with little mathematical background logically presents the theory and fundamentals in an easily comprehensible, self-contained way. The result is a must-have for advanced undergraduate students, as well as masters and graduate students and other users of single-crystal X-ray crystallography from many various disciplines.
Author : Paul Peter Ewald
Publisher : Unknown
Page : 764 pages
File Size : 52,8 Mb
Release : 1962
Category : Crystallography
ISBN : UOM:39015069827379
Author : Jenny Pickworth Glusker,Kenneth N. Trueblood
Publisher : OUP Oxford
Page : 304 pages
File Size : 46,5 Mb
Release : 2010-05-27
Category : Science
ISBN : 9780191604249
This book aims to explain how and why the detailed three-dimensional architecture of molecules can be determined by an analysis of the diffraction patterns obtained when X rays or neutrons are scattered by the atoms in single crystals. Part 1 deals with the nature of the crystalline state, diffraction generally, and diffraction by crystals in particular, and, briefly, the experimental procedures that are used. Part II examines the problem of converting the experimentally obtained data into a model of the atomic arrangement that scattered these beams. Part III is concerned with the techniques for refining the approximate structure to the degree warranted by the experimental data. It also describes the many types of information that can be learned by modern crystal structure analysis. There is a glossary of terms used and several appendixes to which most of the mathematical details have been relegated.
Author : Dong ZhiLi
Publisher : CRC Press
Page : 287 pages
File Size : 48,8 Mb
Release : 2022-05-23
Category : Science
ISBN : 9781000569889
The structure–property relationship is a key topic in materials science and engineering. To understand why a material displays certain behaviors, the first step is to resolve its crystal structure and reveal its structure characteristics. Fundamentals of Crystallography, Powder X-ray Diffraction, and Transmission Electron Microscopy for Materials Scientists equips readers with an in-depth understanding of using powder x-ray diffraction and transmission electron microscopy for the analysis of crystal structures. Introduces fundamentals of crystallography Covers XRD of materials, including geometry and intensity of diffracted x-ray beams and experimental methods Describes TEM of materials and includes atomic scattering factors, electron diffraction, and diffraction and phase contrasts Discusses applications of HRTEM in materials research Explains concepts used in XRD and TEM lab training Based on the author’s course lecture notes, this text guides materials science and engineering students with minimal reliance on advanced mathematics. It will also appeal to a broad spectrum of readers, including researchers and professionals working in the disciplines of materials science and engineering, applied physics, and chemical engineering.
Author : Lesley E. Smart,Elaine A. Moore
Publisher : CRC Press
Page : 412 pages
File Size : 44,7 Mb
Release : 1995-06-27
Category : Science
ISBN : 0748740686
Intended for first- and second-year undergraduates, this introduction to solid-state chemistry includes practical examples of applications and modern developments to offer students the opportunity to apply their knowledge in real-life situations. It aims to provide students with a thorough understanding of the traditional knowledge of crystal structures: lattices, unit cells, close packing, and octahedral and tetrahedral holes and their occupation by various ions in the well-known crystal structures. This descriptive work is augmented by free-electron and band theory. Links to other branches of chemistry and practical examples are emphasized, as are the links back to band theory and crystal structures. For this second edition, the book has been updated throughout and has two new chapters, one on X-ray diffraction techniques and another on solid-state preparative methods, as well as new sections on symmetry and ferroelectrics.
Author : Andrei Benediktovich,Ilya Feranchuk,Alexander Ulyanenkov
Publisher : Springer Science & Business Media
Page : 325 pages
File Size : 49,9 Mb
Release : 2013-09-07
Category : Technology & Engineering
ISBN : 9783642381775
This book provides a concise survey of modern theoretical concepts of X-ray materials analysis. The principle features of the book are: basics of X-ray scattering, interaction between X-rays and matter and new theoretical concepts of X-ray scattering. The various X-ray techniques are considered in detail: high-resolution X-ray diffraction, X-ray reflectivity, grazing-incidence small-angle X-ray scattering and X-ray residual stress analysis. All the theoretical methods presented use the unified physical approach. This makes the book especially useful for readers learning and performing data analysis with different techniques. The theory is applicable to studies of bulk materials of all kinds, including single crystals and polycrystals as well as to surface studies under grazing incidence. The book appeals to researchers and graduate students alike.
Author : E. W. Nuffield
Publisher : Unknown
Page : 432 pages
File Size : 55,7 Mb
Release : 1966
Category : Science
ISBN : STANFORD:36105031281384
1. Introduction 1; 2. The nature and generation of X-rays 29; 3. The diffraction of X-rays 46; 4. Systematically absent X-ray reflections and the determination of space group 87; 5. Polycrystal or powder methods 105; 6. Orientation and projection of morphological crystals 208; 7. The Laue method 226; 8. The reciprocal lattice 239; 9. The Buerger precession method 253; 10. The rotation and oscillation methods 283; 11. The equi-inclination Weissenberg method 302; 12. Single-crystal X-ray diffractometry 343; 13. A general method for orienting a crystal 351; Appendix : 1. The 230 space groups 365; 2. The six permutation of the orthorhombic space groups 370; 3. Space-group determinative tables 372; 4. Table of 1/2 (cos2 phi/sin phi + cos2 phi/phi) 385; 5. Data for constructing stereographic scales 388; 6. Mathematical relations between reciprocal- and direct-lattice constants 391; Index 405.
Author : Olga Chetina
Publisher : Unknown
Page : 27 pages
File Size : 49,7 Mb
Release : 2012
Category : Crystal growth
ISBN : 0957407009
Author : Artur Braun
Publisher : Walter de Gruyter GmbH & Co KG
Page : 572 pages
File Size : 53,6 Mb
Release : 2017-04-10
Category : Science
ISBN : 9783110427967
This book is your graduate level entrance into battery, fuel cell and solar cell research at synchrotron x-ray sources. Materials scientists find numerous examples for the combination of electrochemical experiments with simple and with highly complex x-ray scattering and spectroscopy methods. Physicists and chemists can link applied electrochemistry with fundamental concepts of condensed matter physics, physical chemistry and surface science. Contents: Introduction Molecular Structure and Electronic Structure Crystal Structure and Microstructure Real Space Imaging and Tomography Resonant Methods and Chemical Contrast Variation Surface Sensitive and Volume Sensitive Methods Organic and Bio-Organic Samples Complex Case Studies / Electrochemical In Situ Studies Correlation of Electronic Structure And Conductivity Radiation Damages Background Subtraction X-Ray Physics Nobel Prizes Synchrotron Centers World Electromagnetic Spectrum Kα,Β X-Ray Energies Periodic Table of Elements
Author : Ralf Steudel
Publisher : Walter de Gruyter GmbH & Co KG
Page : 741 pages
File Size : 52,5 Mb
Release : 2020-02-24
Category : Science
ISBN : 9783110578065
The current textbook is an excellent inroduction to the chemistry of the non-metallic elements. The book begins by reviewing the key theoretical concepts of chemical bonding and the properties of different bonding types. Subsequent chapters are focused on reactions, structures and applications of the non-metallic compounds. Combining careful pedagogy and clear writing style, the textbook is a must-have for students studying inorganic chemistry.
Author : Jenny P. Glusker,Mitchell Lewis,Miriam Rossi
Publisher : John Wiley & Sons
Page : 876 pages
File Size : 48,9 Mb
Release : 1996-12-17
Category : Science
ISBN : 0471185434
Anhand verschiedener Beispiele zeigen die Autoren die Bedeutung der Kristallographie für Chemie und Biochemie auf und bieten somit eine gute Zusammenfassung der allgemeinen Prinzipien der Kristallstrukturanalyse. Zum einen sollen Interessierte, die diese Methode nicht selbst durchführen, in die Lage versetzt werden, deren Ergebnisse zu interpretieren. Zum anderen wird dem Leser deutlich gemacht, welche Bedeutung die ungeheure Datenmenge, die sich aus dieser Methode ergibt, einerseits für die Chemie sowie andererseits für die Biochemie hat. Das Buch ist verständlich geschrieben und mit zahlreichen Abbildungen versehen. Durch die Darstellung der Kristallstrukturanalyse im Vergleich zu anderen Methoden ist das Werk auch besonders für fortgeschrittene Studenten geeignet, die sich mit der Kristallographie vertraut machen wollen.
Author : Theo Woike,Dominik Schaniel
Publisher : Walter de Gruyter GmbH & Co KG
Page : 282 pages
File Size : 45,6 Mb
Release : 2018-03-05
Category : Science
ISBN : 9783110433920
This book presents theory and methods to study the structure of condensed matter on different time scales. The authors cover the structure analysis by X-ray diffraction methods from crystalline to amorphous materials, from static-relaxed averaged structures to short-lived electronically excited structures, including detailed descriptions of the time-resolved experimental methods. Complementary, an overview of the theoretical description of condensed matter by static and time-dependent density functional theory is given, starting from the fundamental quantities that can be obtained by these methods through to the recent challenges in the description of time dependent phenomena such as optical excitations. Contents Static structural analysis of condensed matter: from single-crystal to amorphous DFT calculations of solids in the ground state TDDFT, excitations, and spectroscopy Time-resolved structural analysis: probing condensed matter in motion Ultrafast science
