Nmr In Organometallic Chemistry

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NMR in Organometallic Chemistry

Paul S. Pregosin
NMR in Organometallic Chemistry Book PDF

Author : Paul S. Pregosin
Publisher : John Wiley & Sons
Page : 406 pages
File Size : 41,6 Mb
Release : 2013-07-26
Category : Science
ISBN : 9783527680290

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NMR in Organometallic Chemistry by Paul S. Pregosin Pdf

The first and ultimate guide for anyone working in transition organometallic chemistry and related fields, providing the background and practical guidance on how to efficiently work with routine research problems in NMR. The book adopts a problem-solving approach with many examples taken from recent literature to show readers how to interpret the data. Perfect for PhD students, postdocs and other newcomers in organometallic and inorganic chemistry, as well as for organic chemists involved in transition metal catalysis.

Advanced Applications of NMR to Organometallic Chemistry

Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Advanced Applications of NMR to Organometallic Chemistry Book PDF

Author : Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Publisher : John Wiley & Sons
Page : 408 pages
File Size : 44,7 Mb
Release : 1996-12-23
Category : Science
ISBN : UCAL:B4378645

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Advanced Applications of NMR to Organometallic Chemistry by Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer Pdf

This new series offers leading contributions by well known chemists reviewing the state-of-the-art of this wide research area. Physical Organometallic Chemistry aims to develop new insights and to promote novel interest and investigations applicable to organometallic chemistry. NMR spectroscopy has had a considerable impact on many fields of chemistry, although it has served organometallic chemistry mainly on a routine level. In a collection of reviews, leading chemists provide an insight into the scope of applications and uncover the potential of this technique for organometallic chemists. Advanced Applications of NMR to Organometallic Chemistry; Illustrates how recent 1D and 2D and specialized multinuclear applications can solve specific problems encountered by organometallic chemists Surveys modern NMR techniques in organometallic chemistry Includes metal NMR related techniques Focuses on the advent of solid state NMR in organometallic chemistry This book will prove invaluable to the NMR spectroscopist and organometallic chemists and will also be of interest to all organic, inorganic and physical chemists Contents: Selective Excitation and Selective Detection in 29Si NMR; Two-dimensional 13C, Metal Nuclei Correlation; Two-dimensional 1H-119Sn Proton Detected Correlation Spectroscopy in Coordination Chemistry of Hypervalent Organotin Compounds; Indirect Nuclear 119Sn-X Spin-Spin Coupling; Solid State NMR Applications in Organotin and Organolead Chemistry; Solid State NMR Investigations of Metal Carbonyl Complexes; High Pressure NMR in Organometallic Chemistry; Multinuclear NMR Spectroscopy in Supercritical Fluids; High Resolution 6,7Li NMR of Organolithium Compounds; Metal NMR of Organovanadium, -Niobium and -Tantalum Compounds; NMR of Metallic Nuclei in Clusters; 171Yb NMR Spectroscopy.

Phosphorus-31 NMR Spectroscopy

Olaf Kühl
Phosphorus 31 NMR Spectroscopy Book PDF

Author : Olaf Kühl
Publisher : Springer Science & Business Media
Page : 138 pages
File Size : 52,6 Mb
Release : 2008-08-22
Category : Science
ISBN : 9783540791188

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Phosphorus-31 NMR Spectroscopy by Olaf Kühl Pdf

Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known and applied by virtually every synthetically working Organic Chemist. Con- quently, the factors governing the differences in chemical shift values, based on chemical environment, bonding, temperature, solvent, pH, etc. , are well understood, and specialty methods developed for almost every conceivable structural challenge. Proton and carbon NMR spectroscopy is part of most bachelors degree courses, with advanced methods integrated into masters degree and other graduate courses. In view of this universal knowledge about proton and carbon NMR spectr- copy within the chemical community, it is remarkable that heteronuclear NMR is still looked upon as something of a curiosity. Admittedly, most organic compounds contain only nitrogen, oxygen, and sulfur atoms, as well as the obligatory hydrogen and carbon atoms, elements that have an unfavourable isotope distribution when it comes to NMR spectroscopy. Each of these three elements has a dominant isotope: 14 16 32 16 32 N (99. 63% natural abundance), O (99. 76%), and S (95. 02%), with O, S, and 34 14 S (4. 21%) NMR silent. N has a nuclear moment I = 1 and a sizeable quadrupolar moment that makes the NMR signals usually very broad and dif cult to analyse.

NMR in Organometallic Chemistry

Paul S. Pregosin
NMR in Organometallic Chemistry Book PDF

Author : Paul S. Pregosin
Publisher : John Wiley & Sons
Page : 416 pages
File Size : 50,5 Mb
Release : 2013-07-26
Category : Science
ISBN : 9783527680313

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NMR in Organometallic Chemistry by Paul S. Pregosin Pdf

The first and ultimate guide for anyone working in transition organometallic chemistry and related fields, providing the background and practical guidance on how to efficiently work with routine research problems in NMR. The book adopts a problem-solving approach with many examples taken from recent literature to show readers how to interpret the data. Perfect for PhD students, postdocs and other newcomers in organometallic and inorganic chemistry, as well as for organic chemists involved in transition metal catalysis.

Fluxional Organometallic and Coordination Compounds

Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Fluxional Organometallic and Coordination Compounds Book PDF

Author : Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Publisher : John Wiley & Sons
Page : 340 pages
File Size : 45,5 Mb
Release : 2005-01-28
Category : Science
ISBN : 9780470858448

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Fluxional Organometallic and Coordination Compounds by Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer Pdf

This series offers leading contributions by well-known chemists reviewing the state of the art of this wide research area. Physical organometallic chemistry aims to develop new insights and to promote novel interest and investigations applicable to organometallic chemistry. This volume focuses on several important topics on fluxionality in organometallic and coordination chemistry, reviewed by experts in each of the respective fields. It is intended to provide both authoritative concepts and stimulating ideas in order to tackle dynamics from different angles, aiming at an interdisciplinary approach. The fascinating fluxionality of metal-ligand interactions has been in the centre of interest ever since modern coordination and organometallic chemistry started, and has expanded towards bioinorganic chemistry, catalysis and materials sciences. Provides information on some of the most relevant physical methods for studying dynamic processes Presents numerous examples of dynamic behavior, demonstrating the efficiency of the respective method and stimulating further applications Connects main group, transition metal and solid state chemistry in the question for dynamics

Unusual Structures and Physical Properties in Organometallic Chemistry

Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Unusual Structures and Physical Properties in Organometallic Chemistry Book PDF

Author : Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer
Publisher : John Wiley & Sons
Page : 446 pages
File Size : 54,8 Mb
Release : 2003-08-01
Category : Science
ISBN : 9780470855614

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Unusual Structures and Physical Properties in Organometallic Chemistry by Marcel Gielen,Rudolph Willem,Bernd Wrackmeyer Pdf

The principal idea of this volume is to offer a Capita Selecta of unconventional and thought-provoking topics in organometallic chemistry, presented by experts in each field. As intended, this approach leads either to reviews covering a specific uncommon class of organometallic compounds or to overviews which relate uncommon physical properties with various classes of organometallic compounds. The contributions are streamlined thus onto two main axes - unusual properties reflecting structures and bonding situations, on the one hand, and uncommon structural features or structure-reactivity relationships, on the other. Extensive cross-referencing of useful information is provided, making this volume accessible for people working in rather different areas of organometallic chemistry. The synthesis of molecules with 'extreme' properties is a challenge for all those working in organometallic chemistry, irrelevant of theoretical/computational, synthetic or application interests. This book presents case studies at the interface of these overlapping interests. Unusual Structures and Physical Properties in Organometallic Chemistry: * Provides test cases for computational and theoretical models * Presents a challenge for synthetic chemists * Provides ideal show cases for analytical techniques This volume will be an invaluable reference for researchers in organometallic chemistry, computational and theoretical chemistry, NMR and other spectroscopic methods.

Advances in Organometallic Chemistry

Anonim
Advances in Organometallic Chemistry Book PDF

Author : Anonim
Publisher : Academic Press
Page : 470 pages
File Size : 52,6 Mb
Release : 1988-02-01
Category : Science
ISBN : 0080580297

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Advances in Organometallic Chemistry by Anonim Pdf

Advances in Organometallic Chemistry

NMR Spectroscopy

Harald Günther
NMR Spectroscopy Book PDF

Author : Harald Günther
Publisher : John Wiley & Sons
Page : 842 pages
File Size : 54,7 Mb
Release : 2013-12-13
Category : Science
ISBN : 9783527674770

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NMR Spectroscopy by Harald Günther Pdf

Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.

NMR Spectroscopy in Organic Chemistry

B. I. Ionin
NMR Spectroscopy in Organic Chemistry Book PDF

Author : B. I. Ionin
Publisher : Springer Science & Business Media
Page : 396 pages
File Size : 40,8 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781468417852

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NMR Spectroscopy in Organic Chemistry by B. I. Ionin Pdf

In recent years high-resolution nuclear magnetic resonance spec troscopy has found very wide application in organie chemistry in structural and physicochemical investigations and. also in the study of the characteristics of organic compounds which are re lated to the distribution of the electron cloud in the molecules. The vigorous development of this method, which may really be re garded as an independent branch of science, is the result of ex tensive progress in NMR technology, the refinement of its theory, and the accumulation of large amounts of experimental material, which has been correlated by empiricallaws and principles. The literature directly concerned with the NMR method and its applica tion has now grown to such an extent that a complete review of it is practically impossible. Therefore the authors have limited themselves to an examination of only the most important, funda mental, and general investigations. The book consists of six chapters. In the first chapter we have attempted to present the fundamentals of the NMR method in such a way that the reader with little knowledge of the subject will be able to use the method in practical work for investigating simple compounds and solving simple problems. The three subsequent chapters give a deeper analysis of the method, while the last two chapters and the appendix illustrate the various applications of NMR spectroscopy in organic chemistry.

Guide to Fluorine NMR for Organic Chemists

William R. Dolbier, Jr.
Guide to Fluorine NMR for Organic Chemists Book PDF

Author : William R. Dolbier, Jr.
Publisher : John Wiley & Sons
Page : 472 pages
File Size : 47,9 Mb
Release : 2016-08-24
Category : Science
ISBN : 9781118831090

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Guide to Fluorine NMR for Organic Chemists by William R. Dolbier, Jr. Pdf

Following its well-received predecessor, this book offers an essential guide to chemists for understanding fluorine in spectroscopy. With over 1000 compounds and 100 spectra, the second edition adds new data – featuring fluorine effects on nitrogen NMR, chemical shifts, and coupling constants. • Explains how to successfully incorporate fluorine into target molecules and utilize fluorine substituents to structurally characterize organic compounds • Includes new data on nitrogen NMR, focusing on N-15, to portray the influence of fluorine upon nitrogen NMR chemical shifts and coupling constants • Expands on each chapter from the first edition with additional data and updated discussion from recent findings • "The flawless ordering of material covered in this stand-alone volume is such that information can be found very easily." – Angewandte Chemie review of the first edition, 2010

Spectroscopic Properties of Inorganic and Organometallic Compounds

G Davidson
Spectroscopic Properties of Inorganic and Organometallic Compounds Book PDF

Author : G Davidson
Publisher : Royal Society of Chemistry
Page : 468 pages
File Size : 49,8 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847555120

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G Davidson Pdf

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Organic Structures from 2D NMR Spectra

L. D. Field,H. L. Li,A. M. Magill
Organic Structures from 2D NMR Spectra Book PDF

Author : L. D. Field,H. L. Li,A. M. Magill
Publisher : John Wiley & Sons
Page : 328 pages
File Size : 43,8 Mb
Release : 2015-06-15
Category : Science
ISBN : 9781118868942

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Organic Structures from 2D NMR Spectra by L. D. Field,H. L. Li,A. M. Magill Pdf

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. Over recent years, a number of powerful two-dimensional NMR techniques (e.g. HSQC, HMBC, TOCSY, COSY and NOESY) have been developed and these have vastly expanded the amount of structural information that can be obtained by NMR spectroscopy. Improvements in NMR instrumentation now mean that 2D NMR spectra are routinely (and sometimes automatically) acquired during the identification and characterisation of organic compounds. Organic Structures from 2D NMR Spectra is a carefully chosen set of more than 60 structural problems employing 2D-NMR spectroscopy. The problems are graded to develop and consolidate a student’s understanding of 2D NMR spectroscopy. There are many easy problems at the beginning of the collection, to build confidence and demonstrate the basic principles from which structural information can be extracted using 2D NMR. The accompanying text is very descriptive and focussed on explaining the underlying theory at the most appropriate level to sufficiently tackle the problems. Organic Structures from 2D NMR Spectra Is a graded series of about 60 problems in 2D NMR spectroscopy that assumes a basic knowledge of organic chemistry and a basic knowledge of one-dimensional NMR spectroscopy Incorporates the basic theory behind 2D NMR and those common 2D NMR experiments that have proved most useful in solving structural problems in organic chemistry Focuses on the most common 2D NMR techniques – including COSY, NOESY, HMBC, TOCSY, CH-Correlation and multiplicity-edited C-H Correlation. Incorporates several examples containing the heteronuclei 31P, 15N and 19F Organic Structures from 2D NMR Spectra is a logical follow-on from the highly successful “Organic Structures from Spectra” which is now in its fifth edition. The book will be invaluable for students of Chemistry, Pharmacy, Biochemistry and those taking courses in Organic Chemistry. Also available: Instructors Guide and Solutions Manual to Organic Structures from 2D NMR Spectra

Spectroscopic Properties of Inorganic and Organometallic Compounds

G. Davidson
Spectroscopic Properties of Inorganic and Organometallic Compounds Book PDF

Author : G. Davidson
Publisher : Royal Society of Chemistry
Page : 473 pages
File Size : 48,6 Mb
Release : 1992
Category : Molecular rotation
ISBN : 9780851862439

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Spectroscopic Properties of Inorganic and Organometallic Compounds by G. Davidson Pdf

Reflecting the growing volume of published work in this field, researchers will find this book an invaluable source of information on current methods and applications.

Organometallic Chemistry

M Green
Organometallic Chemistry Book PDF

Author : M Green
Publisher : Royal Society of Chemistry
Page : 430 pages
File Size : 47,9 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847554192

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Organometallic Chemistry by M Green Pdf

Organometallic chemistry is an interdisciplinary science which continues to grow at a rapid pace. Although there is continued interest in synthetic and structural studies the last decade has seen a growing interest in the potential of organometallic chemistry to provide answers to problems in catalysis synthetic organic chemistry and also in the development of new materials. This Specialist Periodical Report aims to reflect these current interests reviewing progress in theoretical organometallic chemistry, main group chemistry, the lanthanides and all aspects of transition metal chemistry. Specialist Periodical Reports provide systematic and detailed review coverage of progress in the major areas of chemical research. Written by experts in their specialist fields the series creates a unique service for the active research chemist, supplying regular critical in-depth accounts of progress in particular areas of chemistry. For over 80 years the Royal Society of Chemistry and its predecessor, the Chemical Society, have been publishing reports charting developments in chemistry, which originally took the form of Annual Reports. However, by 1967 the whole spectrum of chemistry could no longer be contained within one volume and the series Specialist Periodical Reports was born. The Annual Reports themselves still existed but were divided into two, and subsequently three, volumes covering Inorganic, Organic and Physical Chemistry. For more general coverage of the highlights in chemistry they remain a 'must'. Since that time the SPR series has altered according to the fluctuating degree of activity in various fields of chemistry. Some titles have remained unchanged, while others have altered their emphasis along with their titles; some have been combined under a new name whereas others have had to be discontinued. The current list of Specialist Periodical Reports can be seen on the inside flap of this volume.

Modern NMR Techniques for Chemistry Research

A.E. Derome
Modern NMR Techniques for Chemistry Research Book PDF

Author : A.E. Derome
Publisher : Elsevier
Page : 299 pages
File Size : 55,5 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483286426

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Modern NMR Techniques for Chemistry Research by A.E. Derome Pdf

Presents an introduction to modern NMR methods at a level suited to organic and inorganic chemists engaged in the solution of structural and mechanistic problems. The book assumes familiarity only with the simple use of proton and carbon spectra as sources of structural information and describes the advantages of pulse and Fourier transform spectroscopy which form the basis of all modern NMR experiments. Discussion of key experiments is illustrated by numerous examples of the solutions to real problems. The emphasis throughout is on the practical side of NMR and the book will be of great use to chemists engaged in both academic and industrial research who wish to realise the full possibilities of the new wave NMR.