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Oxidation of Alcohols to Aldehydes and Ketones by Gabriel Tojo,Marcos I. Fernandez Pdf
The aim of this book is to help people performing routine operations in Organic Synthesis in a laboratory. This book, the first one in a series, focuses on the oxidation of alcohols to aldehydes and ketones. Probably, this is the most important routine operation in Organic Synthesis.
Oxidation of Primary Alcohols to Carboxylic Acids by Gabriel Tojo,Marcos I. Fernandez Pdf
As the second volume in a comprehensive encyclopedia of organic reactions, this work provides an elaborated description of the experimental methods used for the oxidation of alcohols to acids. It supplies important data on possible interferences from protecting groups and functional groups, as well as on potential side-reactions. This book is a must for anyone involved in the preparation of organic compounds.
Author : Michael B. Smith,Jerry March Publisher : John Wiley & Sons Page : 2379 pages File Size : 50,8 Mb Release : 2007-01-29 Category : Science ISBN : 9780470084946
March's Advanced Organic Chemistry by Michael B. Smith,Jerry March Pdf
The Sixth Edition of a classic in organic chemistry continues its tradition of excellence Now in its sixth edition, March's Advanced Organic Chemistry remains the gold standard in organic chemistry. Throughout its six editions, students and chemists from around the world have relied on it as an essential resource for planning and executing synthetic reactions. The Sixth Edition brings the text completely current with the most recent organic reactions. In addition, the references have been updated to enable readers to find the latest primary and review literature with ease. New features include: More than 25,000 references to the literature to facilitate further research Revised mechanisms, where required, that explain concepts in clear modern terms Revisions and updates to each chapter to bring them all fully up to date with the latest reactions and discoveries A revised Appendix B to facilitate correlating chapter sections with synthetic transformations
Author : Bernard B. Brodie,James R. Gillette Publisher : Springer Science & Business Media Page : 797 pages File Size : 48,9 Mb Release : 2013-11-27 Category : Medical ISBN : 9783642651779
Concepts in Biochemical Pharmacology by Bernard B. Brodie,James R. Gillette Pdf
This volume of the Handbook of Experimental Pharmacology (Concepts in Biochemical Pharmacology) will show that pharma cology has finally arrived as a true discipline in its own right, and is no longer the handmaiden of organic chemistry and physiology. Instead it is an amalgam of all the biological sciences including biochemistry, biophysical chemistry, physiology, pathology and clinical medicine. In the volumes that make up Concepts in Bio chemical Pharmacology we hope to convince Medical Schools what should now be obvious, that pharmacology is no longer that dull topic bridging the basic sciences with medicine, but is probably the most important subject in the medical curriculum. We are grateful for the advice of Dr. Byron Clark, Director of the Pharmacology-Toxicology Program at the National Institutes of Health whose support made possible much of the work described in this volume. Contents Section Four: Methods 01 Stooging the MetoholiBm 01 Drugs Subsection A. Assay 01 Drugs and Their M etoholites Chapter 22 : Basic Principles in Development of Methods for Drug Assay. B. B. BRODIE. With 2 Figures 1 1 A. Introduction . . . . . . . . . . B. Principles of Developing a Method. . . . . . 1 I. Section of Method of Assay . . . . . . 1 II. Choice of Solvent for Extraction of Drug 2 III. Adsorption of Drugs by Glass Surfaces . . . . . . . . . . . . . . 3 IV. Recoveries of Known Amounts of Compound from Biological Material. 4 V. Assessment of Sensitivity 5 VI. Assessment of Specificity 5 References. . . . . . . . . . .
Methods for Oxidation of Organic Compounds V1 by Alan Haines Pdf
Methods for the Oxidation of Organic Compounds: Alkanes, Alkenes, Alkynes, and Arenes is an account of the different methods used for the controlled oxidation of alkanes, alkenes, alkynes, and arenes. Most of the oxidative techniques considered are illustrated with detailed experimental procedures taken from the literature. This book is comprised of five chapters and begins with a discussion on alkanes, alkyl groups, and hydrocarbon residues. The formation of alkenes, alcohols, hydroperoxides, dialkyl peroxides, cyclic peroxides, ethers, and esters as well as aldehydes, ketones, and carboxylic acids is described, together with the aromatization of cyclic systems. The following chapters are devoted to alkenes, alkynes, and arenes and focus on the formation of compounds ranging from 1,2-diols and oxiranes (1,2-epoxides) to 1,2-dicarbonyl compounds, phenols and their derivatives, and quinones. The formation of dialkynes by oxidative coupling of 1-alkynes is described, along with the oxidative cleavage of arenes and oxidative coupling of phenols. This monograph should be of interest to organic chemists and research students.
Transition Metal Catalysis in Aerobic Alcohol Oxidation by Francesca Cardona,Camilla Parmeggiani Pdf
This book deals with the search for environmentally benign procedures for the oxidation of alcohols and gives an overview of their transition-metal-catalyzed aerobic oxidation.
Chromium Oxidations in Organic Chemistry by G. Cainelli,G. Cardillo Pdf
Chromium oxidation, well known and widely explored in organic chemistry since the very beginning of this science, is a topic of current interest for the organic chemist as evidenced by the continuous development of new techni ques and procedures reported in the literature. Chromium oxidation is a simple process which can be easily performed in the laboratory and scaled up in industry as well. Although almost every oxidizable organic functional group may undergo chromium oxidation, the most important fields of appli cation are the oxidation of alcohols, allylic and benzylic oxidation, oxidative degradation and oxidation of some organometallic compounds. A high degree of selectivity is often possible by choosing the most suitable reagent among those several ones now available. This book takes account of the various functional groups that undergo oxidation and the entire literature up to 1982. It has been written in the hope to help the synthetic organic chemist in his experimental work. For this purpose a number of tables comprising yields and references have been included; detailed descriptions of typical procedures are meant to show the experimental conditions and the scope of the reactions. We wish to thank Dr. Mario Orena for his valuable scientific and technical assistence and Prof. Bruno Camerino, who read the entire manuscript and corrected many of the errors. Bologna, February 1984 Gianfranco Cainelli Giuliana Cardillo Table of Contents I. Introduction . . . . . . . . . . .
Methods for Oxidation of Organic Compounds V2 by Alan Haines Pdf
Methods for the Oxidation of Organic Compounds: Alcohols, Alcohol Derivatives, Alkyl Halides, Nitroalkanes, Alkyl Azides, Carbonyl Compounds, Hydroxyarenes and Aminoarenes describes the different methods used for the controlled oxidation of alcohols, alcohol derivatives, alkyl halides, nitroalkanes, alkyl azides, carbonyl compounds, hydroxyarenes, and aminoarenes. Most of the oxidative techniques considered are illustrated with detailed experimental procedures taken from the literature. This book is comprised of eight chapters and begins with a discussion on the oxidation of alcohols, with particular emphasis on the formation of carbonyl compounds and carboxylic acids. The following chapters focus on the oxidation of esters and alkyl halides; ethers, acetals, and metal derivatives of alcohols; amines, nitro compounds, and azides; carbonyl compounds; 1,2-diols and related compounds; and hydroxyarenes, aminoarenes, dihydroxyarenes, diaminoarenes, and aminohydroxyarenes. Methods such as catalytic oxidation, catalytic dehydrogenation, and electrochemical and biochemical oxidation are mentioned. This monograph should be of interest to organic chemists and research students.
Dihydric Alcohols, Their Oxidation Products and Derivatives by S. Coffey Pdf
Rodd’s Chemistry of Carbon Compounds, Second Edition, Volume I, Part D: Dihydric Alcohols: Their Oxidation Products and Derivatives describes acyclic compounds containing two functional groups on different carbon atoms. This volume is composed of six chapters, and begins with a description of dihydric alcohols and their derivatives. The next chapters are devoted to the classification and nomenclature of other dihydric alcohol derivatives, including hydroxyaldehydes, hydroxyketones, dicarbonyl compounds monohydroxy-monocarboxylic acids, and related compounds. The remaining chapters deal with nitrogen analogues, nitro and amino-monocarboxylic acids, aldehydic and ketonic monocarboxyhc acids, and acyclic dicarboxylic acids. This book is of value to organic chemists and researchers.
Carlos A. M. Afonso,Nuno R. Candeias,Dulce Pereira Simão,Alexandre F. Trindade,Jaime A. S. Coelho,Bin Tan,Robert Franzén
Author : Carlos A. M. Afonso,Nuno R. Candeias,Dulce Pereira Simão,Alexandre F. Trindade,Jaime A. S. Coelho,Bin Tan,Robert Franzén Publisher : Royal Society of Chemistry Page : 976 pages File Size : 55,9 Mb Release : 2016-12-16 Category : Science ISBN : 9781849739634
Comprehensive Organic Chemistry Experiments for the Laboratory Classroom by Carlos A. M. Afonso,Nuno R. Candeias,Dulce Pereira Simão,Alexandre F. Trindade,Jaime A. S. Coelho,Bin Tan,Robert Franzén Pdf
This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.
Science and Technology in Catalysis by Masakazu Anpo,M. Onaka,H. Yamashita Pdf
(Selected) -- Plenary Lecures: New Catalysts for Controlled/Living Atom Transfer Radical Polymerization (ATRP; Catalysis and Applications of Gold Nanoparticles -- Oral Presentations: Ionic Liquids as New Solvents and Catalysis for Petrochemical and Refining Processes; High Throughput Experiment on the Investigation of Oxidation Catalysts with Gas Sensor System -- Poster Presentations: Development of a Low-Temperature Dioxin Decomposition Catalyst; Studies on Unique Properties of Polyolefins Prepared with Metallocene Catalyst Systems -- Index.
Catalysis in Ionic Liquids by Chris Hardacre,Vasile Parvulescu Pdf
Although ionic liquids have only been studied in depth during the last decades, the field is now maturing to such a degree that the focus is on larger scale applications for use in real processes such as catalysis. Current information is scattered across the literature and Catalysis in Ionic Liquids provides a critical analysis of the research published to date on ionic solvents in all areas of the catalytic science. The book covers both catalyst synthesis using ionic liquids as solvents and green syntheses using both ionic liquids as well as mixtures of ionic liquids and carbon dioxide (as a subcritical and supercritical liquid), including enzymatic, homogeneous, and heterogeneous catalysis, electrocatalysis and organocatalysis. As well as the catalysis community, the book will also be of interest to postgraduates, postdoctoral workers and researchers in academia and industry working in organic synthesis, new materials synthesis, renewable sources of energy and electrochemistry. Written by leading experts in the field, this is the reference source to find about catalysis in ionic liquids.
Chemistry, Life, the Universe and Everything by Melanie Cooper,Michael Klymkowsky Pdf
As you can see, this "molecular formula is not very informative, it tells us little or nothing about their structure, and suggests that all proteins are similar, which is confusing since they carry out so many different roles.
