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Author : Aleksandr I. Kitajgorodskij
Publisher : Unknown
Page : 275 pages
File Size : 41,5 Mb
Release : 1966
Category : Crystallography, Mathematical
ISBN : OCLC:256272072
Author : A. Kitaigorodskii
Publisher : Springer
Page : 275 pages
File Size : 51,6 Mb
Release : 2012-05-04
Category : Science
ISBN : 1475703422
Structure analysis is based on the phenomena of the diffraction of radia tion by materials. In the first ten to twenty years after Laue's discovery, a very complete theory was developed for the diffraction of x-rays and, later, of electrons. This theory led to equations by means of which it was possible to compute the intensity pattern for a given structure. The theory of structure analysis came to mean that of the diffraction of radiation. In 1935, Patterson pointed out a way leading to the solution of the inverse problem: the finding of the structure from a given intensity distribution pattern. At first the conservatism of researchers, and then the war, hampered the de velopment and broad application of the ideas set forth in this work. It was only during the last ten years that all the rich possibilities of the Patterson method - the method of the analysis of the convolution of the electron density - were brought to light and applied in practice.
Author : A. Kitaigorodskii
Publisher : Springer Science & Business Media
Page : 285 pages
File Size : 53,7 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781475703405
Structure analysis is based on the phenomena of the diffraction of radia tion by materials. In the first ten to twenty years after Laue's discovery, a very complete theory was developed for the diffraction of x-rays and, later, of electrons. This theory led to equations by means of which it was possible to compute the intensity pattern for a given structure. The theory of structure analysis came to mean that of the diffraction of radiation. In 1935, Patterson pointed out a way leading to the solution of the inverse problem: the finding of the structure from a given intensity distribution pattern. At first the conservatism of researchers, and then the war, hampered the de velopment and broad application of the ideas set forth in this work. It was only during the last ten years that all the rich possibilities of the Patterson method - the method of the analysis of the convolution of the electron density - were brought to light and applied in practice.
Author : Aleksandr Isaakovich Kitaĭgorodskiĭ
Publisher : Unknown
Page : 0 pages
File Size : 52,5 Mb
Release : 1961-03
Category : Electronic
ISBN : 1475703414
Author : Jenny Pickworth Glusker,Kenneth N. Trueblood
Publisher : Oxford University Press
Page : 299 pages
File Size : 50,8 Mb
Release : 2010-05-27
Category : Science
ISBN : 9780199576340
The purpose of this book is to explain why molecular structure can be determined by single-crystal diffraction of X rays. It is not an account of the practical procedural details, but rather an account of the underlying physical principles, and the kinds of experiments and methods of handling the experimental data that are used.
Author : Alexander J Blake,Jacqueline M Cole,John S O Evans,Peter Main,Simon Parsons,David J Watkin
Publisher : Oxford University Press
Page : 406 pages
File Size : 45,5 Mb
Release : 2009-06-18
Category : Science
ISBN : 9780199219469
By choosing an approach that avoids undue emphasis on the mathematics involved, this book gives practical advice on topics such as growing crystals, solving and refining structures, and understanding and using the results.
Author : Александр Исаакович Китайгородский
Publisher : Springer
Page : 296 pages
File Size : 47,6 Mb
Release : 1961-03
Category : Science
ISBN : UCAL:B4148077
Structure analysis is based on the phenomena of the diffraction of radia tion by materials. In the first ten to twenty years after Laue's discovery, a very complete theory was developed for the diffraction of x-rays and, later, of electrons. This theory led to equations by means of which it was possible to compute the intensity pattern for a given structure. The theory of structure analysis came to mean that of the diffraction of radiation. In 1935, Patterson pointed out a way leading to the solution of the inverse problem: the finding of the structure from a given intensity distribution pattern. At first the conservatism of researchers, and then the war, hampered the de velopment and broad application of the ideas set forth in this work. It was only during the last ten years that all the rich possibilities of the Patterson method - the method of the analysis of the convolution of the electron density - were brought to light and applied in practice.
Author : Mark Ladd,Rex Palmer
Publisher : Springer Science & Business Media
Page : 784 pages
File Size : 47,8 Mb
Release : 2014-07-08
Category : Science
ISBN : 9781461439547
The advances in and applications of x-ray and neutron crystallography form the essence of this new edition of this classic textbook, while maintaining the overall plan of the book that has been well received in the academic community since the first edition in 1977. X-ray crystallography is a universal tool for studying molecular structure, and the complementary nature of neutron diffraction crystallography permits the location of atomic species in crystals which are not easily revealed by X-ray techniques alone, such as hydrogen atoms or other light atoms in the presence of heavier atoms. Thus, a chapter discussing the practice of neutron diffraction techniques, with examples, broadens the scope of the text in a highly desirable way. As with previous editions, the book contains problems to illustrate the work of each chapter, and detailed solutions are provided. Mathematical procedures related to the material of the main body of the book are not discussed in detail, but are quoted where needed with references to standard mathematical texts. To address the computational aspect of crystallography, the suite of computer programs from the fourth edition has been revised and expanded. The programs enable the reader to participate fully in many of the aspects of x-ray crystallography discussed in the book. In particular, the program system XRAY* is interactive, and enables the reader to follow through, at the monitor screen, the computational techniques involved in single-crystal structure determination, albeit in two dimensions, with the data sets provided. Exercises for students can be found in the book, and solutions are available to instructors.
Author : B. K. Vainshtein
Publisher : Elsevier
Page : 431 pages
File Size : 43,7 Mb
Release : 2013-10-22
Category : Science
ISBN : 9781483164755
Structure Analysis by Electron Diffraction focuses on the theory and practice of studying the atomic structure of crystalline substances through electron diffraction. The publication first offers information on diffraction methods in structure analysis and the geometrical theory of electron diffraction patterns. Discussions focus on the fundamental concepts of the theory of scattering and structure analysis of crystals, structure analysis by electron diffraction, formation of spot electron diffraction patterns, electron diffraction texture patterns, and polycrystalline electron diffraction patterns. The text then ponders on intensities of reflections, including atomic scattering, temperature factor, structure amplitude, experimental measurements of intensity, and review of equations for intensities of reflections in electron diffraction patterns. The manuscript examines the Fourier methods in electron diffraction and experimental electron diffraction structure investigations. Topics include the determination of the structure of the hydrated chlorides of transition metals; structures of carbides and nitrides of certain metals and semi-conducting alloys; electron diffraction investigation of clay minerals; and possibilities inherent in structure analysis by electron diffraction. The book is a helpful source of data for readers interested in structure analysis by electron diffraction.
Author : Jenny P. Glusker,Mitchell Lewis,Miriam Rossi
Publisher : John Wiley & Sons
Page : 876 pages
File Size : 55,9 Mb
Release : 1996-12-17
Category : Science
ISBN : 0471185434
Anhand verschiedener Beispiele zeigen die Autoren die Bedeutung der Kristallographie für Chemie und Biochemie auf und bieten somit eine gute Zusammenfassung der allgemeinen Prinzipien der Kristallstrukturanalyse. Zum einen sollen Interessierte, die diese Methode nicht selbst durchführen, in die Lage versetzt werden, deren Ergebnisse zu interpretieren. Zum anderen wird dem Leser deutlich gemacht, welche Bedeutung die ungeheure Datenmenge, die sich aus dieser Methode ergibt, einerseits für die Chemie sowie andererseits für die Biochemie hat. Das Buch ist verständlich geschrieben und mit zahlreichen Abbildungen versehen. Durch die Darstellung der Kristallstrukturanalyse im Vergleich zu anderen Methoden ist das Werk auch besonders für fortgeschrittene Studenten geeignet, die sich mit der Kristallographie vertraut machen wollen.
Author : Yoshio Waseda,Eiichiro Matsubara,Kozo Shinoda
Publisher : Springer Science & Business Media
Page : 320 pages
File Size : 49,9 Mb
Release : 2011-03-18
Category : Technology & Engineering
ISBN : 9783642166358
X-ray diffraction crystallography for powder samples is a well-established and widely used method. It is applied to materials characterization to reveal the atomic scale structure of various substances in a variety of states. The book deals with fundamental properties of X-rays, geometry analysis of crystals, X-ray scattering and diffraction in polycrystalline samples and its application to the determination of the crystal structure. The reciprocal lattice and integrated diffraction intensity from crystals and symmetry analysis of crystals are explained. To learn the method of X-ray diffraction crystallography well and to be able to cope with the given subject, a certain number of exercises is presented in the book to calculate specific values for typical examples. This is particularly important for beginners in X-ray diffraction crystallography. One aim of this book is to offer guidance to solving the problems of 90 typical substances. For further convenience, 100 supplementary exercises are also provided with solutions. Some essential points with basic equations are summarized in each chapter, together with some relevant physical constants and the atomic scattering factors of the elements.
Author : M. Ladd
Publisher : Springer Science & Business Media
Page : 586 pages
File Size : 50,9 Mb
Release : 2013-03-07
Category : Science
ISBN : 9781461517931
X-ray crystallography provides us with the most accurate picture we can get of atomic and molecular structures in crystals. It provides a hard bedrock of structural results in chemistry and in mineralogy. In biology, where the structures are not fully crystalline, it can still provide valuable results and, indeed, the impact here has been revolutionary. It is still an immense field for young workers, and no doubt will provide yet more striking developments of a major character. It does, however, require a wide range of intellectual application, and a considerable ability in many fields. This book will provide much help. It is a very straightforward and thorough guide to every aspect of the subject. The authors are ex perienced both as research workers and as teachers of standing, and this is shown in their clarity of exposition. There are plenty of illustrations and worked examples to aid the student to obtain a real grasp of the subject. The practical side is encouraged by the very clarity of the theory.
Author : Andrew Bond
Publisher : Royal Society of Chemistry
Page : 304 pages
File Size : 40,9 Mb
Release : 2019-07-24
Category : Medical
ISBN : 9781782629665
Taking an intuitive and informal approach to solid-state structure and crystallographic concepts, this book is written for anyone who needs a clear understanding of modern crystallography
Author : Uri Shmueli,Professor of Chemistry Uri Shmueli
Publisher : Oxford University Press
Page : 283 pages
File Size : 43,7 Mb
Release : 2007-06-07
Category : Language Arts & Disciplines
ISBN : 019921350X
The book is a detailed but concise exposition of crystal structure determination at a graduate level. Discussions range from geometrical principles of crystallography, through relevant experimental methods, to techniques of reliable and accurate determination of crystal structures.
Author : M. J. Buerger
Publisher : John Wiley & Sons
Page : 696 pages
File Size : 55,9 Mb
Release : 1960-01-15
Category : Science
ISBN : UOM:39015039846541
