Thermal Analysis Of Polymeric Materials

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Thermal Analysis of Polymeric Materials

Author : Bernhard Wunderlich
Publisher : Springer Science & Business Media
Page : 918 pages
File Size : 47,8 Mb
Release : 2005-04-04
Category : Science
ISBN : 3540236295

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Thermal Analysis of Polymeric Materials by Bernhard Wunderlich Pdf

Table of Contents Table of Contents 1 Atoms, small, and large molecules 2 Basics of thermal analysis 3 Dynamics of chemical and phase changes 4 Thermal analysis tools 5 Structure and properties of materials 6 Single component materials 7 Multiple component materials App. A.1 Table of thermal properties of linear macromolecules and related small molecules - the ATHAS data bank App. A.2 Radiation scattering App. A.3 Derivation of the Rayleigh ratio App. A.4 Neural network predictions App. A.5 Legendre transformations, Maxwell relations, linking of entropy and probability, and derivation of (dS/dT) App. A.6 Boltzmann distribution, harmonic vibration, complex numbers, and normal modes App. A.7 Summary of the basic kinetics of chemical reactions App. A.8 The ITS 1990 and the Krypton-86 length standard App. A.9 Development of classical DTA to DSC App. A.10 Examples of DTA and DSC under extreme conditions App. A.11 Description of an online correction of the heat-flow rate App. A.12 Derivation of the heat-flow equations App. A.13 Description of sawtooth-modulation response App. A.14 An introduction to group theory, definitions of configurations and conformations, and a summary of rational and irrational numbers App. A.15 Summary of birefringence and polarizing microscopy App. A.16 Summary of X-ray diffraction and interference effects App. A.17 Optical analog of electron double diffraction to produce Moire patterns.

Thermal Characterization of Polymeric Materials

Author : Edith Turi
Publisher : Elsevier
Page : 987 pages
File Size : 53,5 Mb
Release : 2012-12-02
Category : Technology & Engineering
ISBN : 9780323141888

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Thermal Characterization of Polymeric Materials by Edith Turi Pdf

Thermal Characterization of Polymeric Materials is a critical review and a concise evaluation of the application of thermal analysis in polymer science and engineering. This book is divided into nine chapters that specifically tackle the instrumentation, theory, and a wide variety of applications of thermal characterization. The introductory chapters provide an overview of all aspects of thermal analytical methods and apparatus and the theory underlying the basic principles of thermal analysis. These chapters also examine the theories and functions of state for thermometry, dilatometry, thermomechanical analysis, calorimetry, thermogravimetry. These topics are followed by a discussion on single-component and multicomponent systems and their phase transitions, as influenced by concentration, pressure, deformation, molecular weight, and copolymerization. The subsequent chapters explore the influence of important chemical and physical parameters on the glass transition, crystallization, and melting of thermoplastic materials. The discussion then shifts to the theoretical aspects of polymer-polymer compatibility, phase separation, and miscibility in mixed polymer systems. This book further considers the thermal analysis in thermosets, elastomers, and fibers. The concluding chapters present the methods of obtaining information on the relative flammability properties of polymers, for screening fire retardant additives, and for studying the mechanism of flame inhibition. These chapters also look into the thermal analysis of antioxidants, stabilizers, lubricants, plasticizers, impact modifiers, and fire retardants. Polymer scientists and researchers will find this book invaluable.

Thermal Analysis of Polymeric Materials

Author : Bernhard Wunderlich
Publisher : Springer Science & Business Media
Page : 894 pages
File Size : 49,9 Mb
Release : 2005-12-06
Category : Technology & Engineering
ISBN : 9783540263609

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Thermal Analysis of Polymeric Materials by Bernhard Wunderlich Pdf

Thermal analysis is an old technique. It has been neglected to some degree because developments of convenient methods of measurement have been slow and teaching of the understanding of the basics of thermal analysis is often wanting. Flexible, linear macromolecules, also not as accurately simply called polymers, make up the final, third, class of molecules which only was identified in 1920. Polymers have neverbeenfullyintegratedintothedisciplinesofscienceandengineering. Thisbook is designed to teach thermal analysis and the understanding of all materials, flexible macromolecules, as well as those of the small molecules and rigid macromolecules. The macroscopic tool of inquiry is thermal analysis, and the results are linked to microscopic molecular structure and motion. Measurements of heat and mass are the two roots of quantitative science. The macroscopic heat is connected to the microscopic atomic motion, while the macroscopic mass is linked to the microscopic atomic structure. The macroscopic unitsofmeasurementofheatandmassarethejouleandthegram,chosentobeeasily discernable by the human senses. The microscopic units of motion and structure are 12 10 the picosecond (10 seconds) and the ångstrom (10 meters), chosen to fit the atomic scales. One notes a factor of 10,000 between the two atomic units when expressed in “human” units, second and gram—with one gram being equal to one cubic centimeter when considering water. Perhaps this is the reason for the much better understanding and greater interest in the structure of materials, being closer to human experience when compared to molecular motion.

Thermal Analysis of Polymers

Author : Joseph D. Menczel,R. Bruce Prime
Publisher : John Wiley & Sons
Page : 607 pages
File Size : 42,5 Mb
Release : 2014-07-09
Category : Science
ISBN : 9781118995990

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Thermal Analysis of Polymers by Joseph D. Menczel,R. Bruce Prime Pdf

Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Thermal Analysis of Polymeric Materials

Author : Krzysztof Pielichowski,Kinga Pielichowska
Publisher : John Wiley & Sons
Page : 878 pages
File Size : 51,7 Mb
Release : 2022-06-01
Category : Technology & Engineering
ISBN : 9783527828708

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Thermal Analysis of Polymeric Materials by Krzysztof Pielichowski,Kinga Pielichowska Pdf

An all-in-one reference work covering the essential principles and techniques on thermal behavior and response of polymeric materials This book delivers a detailed understanding of the thermal behavior of polymeric materials evaluated by thermal analysis methods. It covers the most widely applied principles which are used in method development to substantiate what happens upon heating of polymers. It also reviews the key application areas of polymers in materials science. Edited by two experts in the field, the book covers a wide range of specific topics within the aforementioned categories of discussion, such as: Crucial thermal phenomena - glass transition, crystallization behavior and curing kinetics Polymeric materials that have gained considerable interest over the last decade The latest advancements in techniques related to the field, such as modulated temperature DSC and fast scanning calorimetry The recent advances in hyphenated techniques and their applications Polymer chemists, chemical engineers, materials scientists, and process engineers can use this comprehensive reference work to gain clarity on the topics discussed within and learn how to harness them in practical applications across a wide range of disciplines.

Thermal Analysis of Polymers

Author : M. P. Sepe
Publisher : iSmithers Rapra Publishing
Page : 130 pages
File Size : 49,5 Mb
Release : 1997
Category : Technology & Engineering
ISBN : 1859571077

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Thermal Analysis of Polymers by M. P. Sepe Pdf

The techniques which are particularly relevant to polymer characterisation are evaluated in this new report. For each technique the author describes the method of operation and the output obtained, and then considers its application to polymer characterisation. An additional indexed section containing several hundred abstracts from the Rapra Polymer Library database provides useful references for further reading.

Reactions and Mechanisms in Thermal Analysis of Advanced Materials

Author : Atul Tiwari,Baldev Raj
Publisher : John Wiley & Sons
Page : 616 pages
File Size : 40,6 Mb
Release : 2015-07-29
Category : Technology & Engineering
ISBN : 9781119117704

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Reactions and Mechanisms in Thermal Analysis of Advanced Materials by Atul Tiwari,Baldev Raj Pdf

Strong bonds form stronger materials. For this reason, the investigation on thermal degradation of materials is a significantly important area in research and development activities. The analysis of thermal stability can be used to assess the behavior of materials in the aggressive environmental conditions, which in turn provides valuable information about the service life span of the materiel. Unlike other books published so far that have focused on either the fundamentals of thermal analysis or the degradation pattern of the materials, this book is specifically on the mechanism of degradation of materials. The mechanism of rapturing of chemical bonds as a result of exposure to high-temperature environment is difficult to study and resulting mechanistic pathway hard to establish. Limited information is available on this subject in the published literatures and difficult to excavate. Chapters in this book are contributed by the experts working on thermal degradation and analysis of the wide variety of advanced and traditional materials. Each chapter discusses the material, its possible application, behavior of chemical entities when exposed to high-temperature environment and mode and the mechanistic route of its decomposition. Such information is crucial while selecting the chemical ingredients during the synthesis or development of new materials technology.

Polymers and Multicomponent Polymeric Systems

Author : Jose James,Pramoda Kumari Pallathadka,Sabu Thomas
Publisher : CRC Press
Page : 301 pages
File Size : 51,9 Mb
Release : 2019-12-06
Category : Science
ISBN : 9780429943461

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Polymers and Multicomponent Polymeric Systems by Jose James,Pramoda Kumari Pallathadka,Sabu Thomas Pdf

In recent years, multicomponent polymers have generated much interest due to their excellent properties, unique morphology and high-end applications. Book focusses on thermal, thermo-mechanical and dielectric analysis of polymers and multicomponent polymeric systems like blends, interpenetrating polymeric networks (IPNs), gels, polymer composites, nanocomposites. Through these analyses, it provides an insight into the stability of polymer systems as a function of time, processing and usage. Aimed at polymer chemists, physicists and engineers, it also covers ASTM /ISO and other standards of various measurement techniques for systematic analysis in materials science.

Thermal Characterization of Polymeric Materials, Two-Volume Set

Author : Robert Shanks
Publisher : Academic Press
Page : 0 pages
File Size : 45,7 Mb
Release : 2015-03-01
Category : Science
ISBN : 0123972167

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Thermal Characterization of Polymeric Materials, Two-Volume Set by Robert Shanks Pdf

This is a source book for all aspects of thermal analysis as applied to polymeric material characterization. It includes theory, current instrumentation, and how to use the techniques for different types of polymers. It provides up to date reviews of current scientific findings for thermal analysis of polymeric materials, as well as insights into how the techniques can be used for practical and basic research. It consolidates a very wide field of knowledge into one book with insight on what all the information means. The book provides a clear overview of how thermal analysis can be used for material development, how to interpret thermal analysis data, and limitations of the techniques. Most of the knowledge generated for the reader will be practical in nature, but by understanding the basics and fundamentals, the readers may also see ways to apply these techniques to problems outside of polymeric materials. The work will be used as a training tool for professionals, research scientists and lab technicians, whether new to thermal analysis, as well as those needing to apply the techniques to their respective projects. Readers need to have at least BS degree in physical sciences and a general knowledge of polymeric materials. Last edition was published in 1997 - so assuming knowledge in the book is from 1995/96, we have about 15 years worth of new data and information to share with the reader in updating this book to a 3rd edition. This field has expanded considerably since the last edition. This book is therefore overdue for an update. The major changes in this revision compared to the 2nd edition The work will be updated 30-50% - many changes have occurred in thermal analysis and specifically in how these techniques are used for specific materials (or new materials - e.g. nanocomposites) a section on the use of thermal analysis for materials fire safety has been added each author includes a section attempting to predict the future and anticipate changes that may occur in the field. Consolidates knowledge in a wide field encompassing polymer and materials science, solid state physics, and an understanding of mechanical properties and chemical stability, presenting an all-in-one proposition, reducing time spent to acquire or disseminate quality information Written by practitioners, for practitioners, exploring current usage and applications, not theoretical techniques Techniques for thermal analysis for materials fire safety discusses rarely synthesized new coverage. Coverage extends to nanocomposites and other complex, recently discovered polymeric nanomaterials, representing a new class of content rarely afforded full breathing space in the literature Predicts future and anticipated changes in thermal calorimetry, meaning for the practitioner and institution the book sustains value over time rather than being outdated by events

Handbook of Thermal Analysis and Calorimetry

Author : Stephen Z.D. Cheng
Publisher : Elsevier
Page : 859 pages
File Size : 55,8 Mb
Release : 2002-12-09
Category : Technology & Engineering
ISBN : 9780080527406

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Handbook of Thermal Analysis and Calorimetry by Stephen Z.D. Cheng Pdf

As a new and exciting field of interdisciplinary macromolecular science and engineering, polymeric materials will have a profound presence in 21st century chemical, pharmaceutical, biomedical, manufacturing, infrastructure, electronic, optical and information technologies. The origin of this field derived from an area of polymer science and engineering encompassing plastic technologies. The field is rapidly expanding to incorporate new interdisciplinary research areas such as biomaterials, macromolecular biology, novel macromolecular structures, environmental macromolecular science and engineering, innovative and nano-fabrications of products, and is translating discoveries into technologies. · Unique in combining scientific concepts with technological aspects · Provides a comprehensive and broad coverage of thermodynamic and thermal behaviours of various polymeric materials as well as methodologies of thermal analysis and calorimetry · Contributions are from both pioneering scientists and the new generation of researchers

Thermal Degradation of Polymeric Materials

Author : Krzysztof Pielichowski,James Njuguna
Publisher : iSmithers Rapra Publishing
Page : 324 pages
File Size : 42,8 Mb
Release : 2005
Category : Science
ISBN : 185957498X

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Thermal Degradation of Polymeric Materials by Krzysztof Pielichowski,James Njuguna Pdf

Understanding the thermal degradation of polymers is of paramount importance for developing a rational technology of polymer processing and higher-temperature applications. Controlling degradation requires understanding of many different phenomena, including chemical mechanisms, the influence of polymer morphology, the complexities of oxidation chemistry, and the effects of stabilisers, fillers and other additives. This book offers a wealth of information for polymer researchers and processors requiring an understanding of the implications of thermal degradation on material and product performance.

Handbook of Thermal Analysis and Calorimetry

Author : Anonim
Publisher : Elsevier
Page : 860 pages
File Size : 42,7 Mb
Release : 2018-03-12
Category : Science
ISBN : 9780444640635

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Handbook of Thermal Analysis and Calorimetry by Anonim Pdf

Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications