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Author : Wallace S. Brey
Publisher : Unknown
Page : 0 pages
File Size : 47,5 Mb
Release : 1988
Category : Electronic
ISBN : OCLC:830702320
Author : Wallace S. Brey
Publisher : Elsevier
Page : 572 pages
File Size : 51,9 Mb
Release : 2012-12-02
Category : Science
ISBN : 9780080917030
FROM THE PREFACE: Pulse Methods in 1D and 2D Liquid-Phase NMR is written to enable the practicing NMR spectroscopist to understand and apply the varied and powerful new techniques developed in the past few years for obtaining spectra with greatly increased information content and from smaller and smaller samples. The intent is to describe both theory and practice in simple and detailed fashion so that the methods may be critically evaluated and effectively used in any potential application. As methods become more complex they require more instrument time, and it is important to be able to judge whether the investment of this time is justified. It is also essential for the spectroscopist to be in a position to evaluate the capabilities of the instrumentation available, as well as the additional requirements for utilization of particular new methods. The material in this book assumes a knowledge of continuous-wave NMR methods as well as an elementary understanding of the normal pulsed Fourier-transform spectroscopic procedures, together with a knowledge of such related phenomena as the nuclear Overhauser effect. Although much of the treatment is necessarily methematical, this aspect of the presentation has been simplified as much as possible.
Author : Gareth A. Morris,James W. Emsley
Publisher : John Wiley & Sons
Page : 877 pages
File Size : 52,7 Mb
Release : 2012-12-19
Category : Science
ISBN : 9781118589083
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here
Author : Edwin D. Becker
Publisher : Elsevier
Page : 424 pages
File Size : 55,8 Mb
Release : 1999-10-08
Category : Science
ISBN : 0080508065
High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate" level, with mathematics used to augment, rather than replace, clear verbal descriptions of the phenomena. The book is intended to allow a graduate student, advanced undergraduate, or researcher to understand NMR at a fundamental level, and to see illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The presentation is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. Likewise, no previous background in NMR is assumed, since the book begins with a description of the basic physics, together with a brief account of the historical development of the field. This third edition of High Resolution NMR preserves the "conversational" approach of the previous editions that has been well accepted as a teaching tool. However, more than half the material is new, and the remainder has been revised extensively. Problems are included to reinforce concepts in the book. Uses mathematics to augment, not replace, verbal explanations Written in a clear and conversational style Follows the successful format and approach of two previous editions Revised and updated extensively--about 70 percent of the text is new Includes problems and references to additional reading at the end of each chapter
Author : Helmut Duddeck,Wolfgang Dietrich
Publisher : Springer Science & Business Media
Page : 273 pages
File Size : 46,6 Mb
Release : 2012-12-06
Category : Science
ISBN : 9783642977879
For several years, we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us two years later to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in English version. Now, after the rapid development of basic multipulse NMR me thods in the early 1980s, the avantgarde in modem NMR is concentrating on the invention and optimi zation of advanced techniques, e. g. , three-dimensional experiments. For the beginners, however, the situation has not changed markedly since the appearence of the first edition of this book. Therefore, we decided not to add new techniques to this second edition, but rather to increase the number of exerci ses from 23 to 33, the new ones being basically single-spectrum-problems.
Author : Harald Günther
Publisher : John Wiley & Sons
Page : 739 pages
File Size : 42,6 Mb
Release : 2013-11-04
Category : Science
ISBN : 9783527330003
Auch die komplett überarbeitete 3. Auflage dieses bewährten Lehrbuchs überzeugt durch Klarheit, eine didaktisch gelungene Aufbereitung des Stoffes und ein hohes Maß an Praxisbezug. Das komplexe Thema wird mit einem Mindestmaß an Mathematik erklärt - ideal für Studenten, die die Grundlagen der NMR-Spektroskopie verstehen und das Verfahren effizient und präzise anwenden möchten. Die neue Auflage ist vollständig überarbeitet und aktualisiert. So sind rund 25% der Inhalte neu, darunter auch Kapitel zur biologischen NMR-Spektroskopie sowie viele Beispiele aus der organischen Chemie. Daher stellt dieses Fachbuch auch für Studenten in Grund- und Hauptstudium verwandter Fachrichtungen wie der Biochemie, Medizinischen Chemie, Pharmazeutischen Chemie und Materialwissenschaften einen wertvollen Leitfaden dar. Außerdem findet der Leser eine Vielzahl von Übungsaufgaben mit zugehörigen Lösungen.
Author : Igor N. Serdyuk,Nathan R. Zaccai,Joseph Zaccai,Giuseppe Zaccai
Publisher : Cambridge University Press
Page : 709 pages
File Size : 43,9 Mb
Release : 2017-05-18
Category : Medical
ISBN : 9781107056374
A comprehensive graduate textbook explaining key physical methods in biology, reflecting the very latest research in this fast-moving field.
Author : G A Webb
Publisher : Royal Society of Chemistry
Page : 650 pages
File Size : 45,5 Mb
Release : 2007-10-31
Category : Science
ISBN : 9781847553751
As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.
Author : G¿nter Gauglitz,David S. Moore
Publisher : John Wiley & Sons
Page : 2011 pages
File Size : 50,9 Mb
Release : 2014-06-09
Category : Science
ISBN : 9783527321506
This second, thoroughly revised, updated and enlarged edition provides a straightforward introduction to spectroscopy, showing what it can do and how it does it, together with a clear, integrated and objective account of the wealth of information that may be derived from spectra. It also features new chapters on spectroscopy in nano-dimensions, nano-optics, and polymer analysis. Clearly structured into sixteen sections, it covers everything from spectroscopy in nanodimensions to medicinal applications, spanning a wide range of the electromagnetic spectrum and the physical processes involved, from nuclear phenomena to molecular rotation processes. In addition, data tables provide a comparison of different methods in a standardized form, allowing readers to save valuable time in the decision process by avoiding wrong turns, and also help in selecting the instrumentation and performing the experiments. These four volumes are a must-have companion for daily use in every lab.
Author : T. R. Steinheimer,Martin G. Ondrus
Publisher : Unknown
Page : 498 pages
File Size : 49,8 Mb
Release : 1990
Category : Atrazine
ISBN : UOM:39015022546728
Author : Joseph B. Lambert,Eugene P. Mazzola,Clark D. Ridge
Publisher : John Wiley & Sons
Page : 485 pages
File Size : 45,7 Mb
Release : 2019-01-04
Category : Science
ISBN : 9781119295235
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Author : Chariklia I. Stassinopoulou
Publisher : Springer Science & Business Media
Page : 367 pages
File Size : 54,6 Mb
Release : 2013-06-29
Category : Science
ISBN : 9783642791581
Provided here are the latest techniques of NMR as applied to the study of proteins, carbohydrates and nucleic acids. The first chapters are devoted to an introduction to NMR and parameters related to molecular structure and molecular interactions. NMR experiments from basic 1D to 2D, 3D and 4D, used in combination with isotopically labelled molecules, are described and a general strategy is presented for biomacromolecular structure determination. Subsequent chapters deal with more advanced principles and techniques and their applications to structural and dynamic processes involving biomacromolecules in solution. Advanced results on peptide, protein, oligosaccharide and nucleic acid structure and recognition are presented.
Author : Anonim
Publisher : Academic Press
Page : 8607 pages
File Size : 41,7 Mb
Release : 2010-04-09
Category : Science
ISBN : 9780080922171
The Second Edition of the Encyclopedia of Spectroscopy and Spectrometry pulls key information into a single source for quick access to answers and/or in-depth examination of topics. "SPEC-2" covers theory, methods, and applications for researchers, students, and professionals—combining proven techniques and new insights for comprehensive coverage of the field. The content is available in print and online via ScienceDirect, the latter of which offers optimal flexibility, accessibility, and usability through anytime, anywhere access for multiple users and superior search functionality. No other work gives analytical and physical (bio)chemists such unprecedented access to the literature. With 30% new content, SPEC-2 maintains the "authoritative, balanced coverage" of the original work while also breaking new ground in spectroscopic research. Incorporates more than 150 color figures, 5,000 references, and 300 articles (30% of which are new), for a thorough examination of the field Highlights new research and promotes innovation in applied areas ranging from food science and forensics to biomedicine and health Features a new co-editor: David Koppenaal of Pacific Northwest National Laboratory, Washington, USA, whose work in atomic mass spectrometry has been recognized internationally
Author : George R. Waller,Kazuo Yamasaki
Publisher : Springer Science & Business Media
Page : 433 pages
File Size : 46,6 Mb
Release : 2012-12-06
Category : Science
ISBN : 9781461304135
''A wealth of information...these two volumes will be immensely valuable to anyone having to deal with this difficult group of compounds.'' ---Biochemical Systematics and Ecology, from a review of Saponins Used in Traditional and Modern Medicine and Saponins Used in Food and Agriculture ''A valuable contribution to the literature.'' ---The Quarterly Review of Biology, December 1997
Author : J.W. Akitt,B. E. Mann
Publisher : CRC Press
Page : 400 pages
File Size : 45,6 Mb
Release : 2017-12-21
Category : Science
ISBN : 9781482268379
Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.